JPH0580445B2 - - Google Patents
Info
- Publication number
- JPH0580445B2 JPH0580445B2 JP61297808A JP29780886A JPH0580445B2 JP H0580445 B2 JPH0580445 B2 JP H0580445B2 JP 61297808 A JP61297808 A JP 61297808A JP 29780886 A JP29780886 A JP 29780886A JP H0580445 B2 JPH0580445 B2 JP H0580445B2
- Authority
- JP
- Japan
- Prior art keywords
- cockroaches
- repellent
- cockroach
- present
- oil
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 241001674044 Blattodea Species 0.000 claims description 37
- 239000005871 repellent Substances 0.000 claims description 33
- 230000002940 repellent Effects 0.000 claims description 33
- 239000010617 anise oil Substances 0.000 claims description 8
- 239000010620 bay oil Substances 0.000 claims description 8
- 239000004480 active ingredient Substances 0.000 claims description 6
- 230000000694 effects Effects 0.000 description 12
- 241000238657 Blattella germanica Species 0.000 description 5
- 239000003205 fragrance Substances 0.000 description 5
- 239000000341 volatile oil Substances 0.000 description 5
- OOCCDEMITAIZTP-QPJJXVBHSA-N (E)-cinnamyl alcohol Chemical compound OC\C=C\C1=CC=CC=C1 OOCCDEMITAIZTP-QPJJXVBHSA-N 0.000 description 4
- 230000009471 action Effects 0.000 description 4
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 description 4
- 238000000034 method Methods 0.000 description 4
- ZMQAAUBTXCXRIC-UHFFFAOYSA-N safrole Chemical compound C=CCC1=CC=C2OCOC2=C1 ZMQAAUBTXCXRIC-UHFFFAOYSA-N 0.000 description 4
- 241000607479 Yersinia pestis Species 0.000 description 3
- 235000013305 food Nutrition 0.000 description 3
- 230000000384 rearing effect Effects 0.000 description 3
- NOOLISFMXDJSKH-UTLUCORTSA-N (+)-Neomenthol Chemical compound CC(C)[C@@H]1CC[C@@H](C)C[C@@H]1O NOOLISFMXDJSKH-UTLUCORTSA-N 0.000 description 2
- ODZVUHGEGIBWOY-FMIVXFBMSA-N (2e)-n,n,3,7-tetramethylocta-2,6-dien-1-amine Chemical compound CN(C)C\C=C(/C)CCC=C(C)C ODZVUHGEGIBWOY-FMIVXFBMSA-N 0.000 description 2
- SDOFMBGMRVAJNF-KVTDHHQDSA-N (2r,3r,4r,5r)-6-aminohexane-1,2,3,4,5-pentol Chemical compound NC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO SDOFMBGMRVAJNF-KVTDHHQDSA-N 0.000 description 2
- ODZVUHGEGIBWOY-XFXZXTDPSA-N (2z)-n,n,3,7-tetramethylocta-2,6-dien-1-amine Chemical compound CN(C)C\C=C(\C)CCC=C(C)C ODZVUHGEGIBWOY-XFXZXTDPSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 description 2
- NOOLISFMXDJSKH-UHFFFAOYSA-N DL-menthol Natural products CC(C)C1CCC(C)CC1O NOOLISFMXDJSKH-UHFFFAOYSA-N 0.000 description 2
- ROSDSFDQCJNGOL-UHFFFAOYSA-N Dimethylamine Chemical compound CNC ROSDSFDQCJNGOL-UHFFFAOYSA-N 0.000 description 2
- 239000005770 Eugenol Substances 0.000 description 2
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- OOCCDEMITAIZTP-UHFFFAOYSA-N allylic benzylic alcohol Natural products OCC=CC1=CC=CC=C1 OOCCDEMITAIZTP-UHFFFAOYSA-N 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- -1 bennite Chemical compound 0.000 description 2
- WJSDHUCWMSHDCR-VMPITWQZSA-N cinnamyl acetate Natural products CC(=O)OC\C=C\C1=CC=CC=C1 WJSDHUCWMSHDCR-VMPITWQZSA-N 0.000 description 2
- 229960002217 eugenol Drugs 0.000 description 2
- 239000002917 insecticide Substances 0.000 description 2
- 229940041616 menthol Drugs 0.000 description 2
- 239000000843 powder Substances 0.000 description 2
- 230000001846 repelling effect Effects 0.000 description 2
- 238000005507 spraying Methods 0.000 description 2
- 241000251468 Actinopterygii Species 0.000 description 1
- 239000005995 Aluminium silicate Substances 0.000 description 1
- 241000238662 Blatta orientalis Species 0.000 description 1
- 241000257226 Muscidae Species 0.000 description 1
- 241000238675 Periplaneta americana Species 0.000 description 1
- 241000048273 Periplaneta japonica Species 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000000853 adhesive Substances 0.000 description 1
- 230000001070 adhesive effect Effects 0.000 description 1
- 239000000443 aerosol Substances 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 235000012211 aluminium silicate Nutrition 0.000 description 1
- 230000000844 anti-bacterial effect Effects 0.000 description 1
- 239000003429 antifungal agent Substances 0.000 description 1
- 229940121375 antifungal agent Drugs 0.000 description 1
- 239000005667 attractant Substances 0.000 description 1
- 239000003899 bactericide agent Substances 0.000 description 1
- 239000000969 carrier Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 230000031902 chemoattractant activity Effects 0.000 description 1
- 239000004927 clay Substances 0.000 description 1
- 239000011248 coating agent Substances 0.000 description 1
- 238000000576 coating method Methods 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000002270 dispersing agent Substances 0.000 description 1
- 239000003995 emulsifying agent Substances 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 235000013312 flour Nutrition 0.000 description 1
- 239000010794 food waste Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000000422 nocturnal effect Effects 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 230000002085 persistent effect Effects 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 230000008569 process Effects 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 230000007480 spreading Effects 0.000 description 1
- 239000003381 stabilizer Substances 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- 239000003826 tablet Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
- 239000000080 wetting agent Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Description
(A) 産業上の利用分野
本発明は、人体に対して安全なゴキブリ忌避剤
に関する。
更に詳しくは、本発明は、古くから香料として
利用されている天然精油であるアニス油及び／又
はベイ油を有効成分として含有することを特徴と
するゴキブリ忌避剤に関する。
(B) 従来の技術
ゴキブリ類は、熱帯地方を中心に世界に約44種
類ほど分布しているが、日本の家住性のゴキブリ
としては、例えばチヤバネゴキブリ、クロゴキブ
リ、ヤマトゴキブリ、ワモンゴキブリなどが良く
知られている。
このゴキブリは、食品害虫としてばかりでな
く、病害の伝播者としてイエバエとならんで衛生
上、極めて不潔な害虫である。これらのゴキブリ
は、水分、食物の摂取に好都合な場所の間隙に集
合し、隠れ、夜間台所の食物の残りとかに歩き回
る雑食性の害虫である。
近年、ゴキブリ類の分布地域及び棲息数が著し
く増加する傾向にある。これらの現象は家庭及び
ビルの暖房設備の普及と豊富な食物等により冬季
の棲息活動、増殖活動を助長させたために生じた
ものである。
これらのゴキブリの防除方法としては、夜間活
動性などの性質を利用して残効性の高い殺虫剤を
ゴキブリの潜伏場所や通路等の噴霧して又は塗布
した容器あるいは、その集合性を利用して粘着剤
と誘引剤とを併用した容器を用いて捕獲する方
法、更にゴキブリに対する忌避作用を利用して忌
避剤を塗布した容器を用いて忌避させる方法など
が知られている。
ゴキブリの忌避作用を利用した忌避剤の例とし
ては、例えばメントール（特開昭55−104202）、
Ｎ−ゲラニルジメチルアミン、Ｎ−シトロネルジ
メチルアミン、Ｎ−ネリルジメチルアミン（特開
昭58−113105）、シンナミルアルコール、オイゲ
ノール、サフロール、シンナミルアセテート（特
開昭50−105821）などが知られている。
(C) 発明が解決しようとする問題点
従来、ゴキブリの忌避剤として報告のある例え
ば、上記のメントール、Ｎ−ゲラニルジメチルア
ミン、Ｎ−シトロネリルジメチルアミン、Ｎ−ネ
リルジメチルアミン、シンナミルアルコール、オ
イゲノール、サフロール、シンナミルアセテート
などによるゴキブリに対する忌避作用は、必ずし
も満足できるものではないという不利益乃至欠点
がある。
(D) 問題点を解決するための手段
本発明者らは、上述のごとき不利益乃至欠点を
解決すべく多数の香料類についてゴキブリに対す
る忌避作用について鋭意研究を行つてきた。その
結果、古くから香料として使用されている天然精
油である、アニス油及び／又はベイ油が、ゴキブ
リに対する忌避作用が極めて優れ、且つその作用
の持続性が優れていることを発見した。
本発明ゴキブリ忌避剤の有効成分として使用す
る天然精油であるアニス油及びベイ油は、市場で
容易に入手することができる。本発明ゴキブリ忌
避剤においては、このような天然精油類を単独又
は併用して、そのままゴキブリの忌避剤として用
いることもできるが、適当な担体に吸着、混合ま
たは分散させて用いることができる。担体の例と
しては、例えば圭藻土、アルミナ、酸性白土、木
粉、カオリン、ベンナイト、活性炭、シリカなど
をあげることができる。これら担体は、１種また
は２種以上の混合物として用いることもできる。
また、各種の合成樹脂に含浸又は混練して用いる
こともできる。更に必要により、乳化剤、分散
剤、懸濁剤、展着剤、浸透剤、湿潤剤、安定剤な
どを添加し、油剤、乳剤、水和剤、粉剤、錠剤、
噴霧剤などの剤型で使用することもできる。ま
た、本発明のゴキブリ忌避剤は、アニス油及び／
又はベイ油の他に殺虫剤、共力剤、他の忌避剤、
香料、殺菌剤、防カビ剤などを配合して使用する
こともできる。
上述のようにして得ることのできる本発明のゴ
キブリ忌避剤は、例えばゴキブリの棲息場所、潜
伏場所または通路などに直接、噴霧したり、散布
したり、あるいは塗布したりなどの方法によつて
ゴキブリをある一定地域から逃避させ、ゴキブリ
からの被害を有効に防除することができる。
本発明のゴキブリ忌避剤の有効成分であるアニ
ス油及び／又はベイ油の使用量には特別な制約は
なく、適宜選択利用できる。少量で忌避効果を示
すために、とくに多量に用いる必要はないが、例
えば、塗布、エアゾールなどにより忌避区域を作
る場合、表面に有効成分として例えば、0.0001
ｇ／cm2以上または空気中に有効成分として
0.5ppm以上で存在させることが望ましい。
(E) 作用
本発明ゴキブリ忌避剤で用いる有効成分である
アニス油及びベイ油からえらばれる天然精油類
が、ゴキブリに対して忌避作用を示すことは、本
発明によつて初めて見出されたが、その作用及び
効果について下記の実施例により示す。
(F) 実施例
(1) 10cm×4.5cmのロ紙をゴキブリが侵入できる
程度の大きさの波型に折り、このロ紙に本発明
品及び対照品を一定濃度で0.05ml塗布する。次
に縦40cm、横25cm、高さ28cmのゴキブリ飼育用
の透明プラスチツクケースの四隅に同種のゴキ
ブリ忌避剤を塗布した上記の波型のロ紙２ケと
ブランクの波型の口紙２ケを交互に設置し、忌
避効果を観察した。（ゴキブリ類はその習性と
して飼育ケースの隅の暗所に集まり易い）
忌避効果の判定は、上記の飼育ケース中にチ
ヤバネコゴキブリの成虫を雌雄10匹ずつ計20匹
を放し、３時間後にゴキブリ忌避剤を塗布した
波型のロ紙中に居るゴキブリの数を調べて判定
した。その結果は表−１及び表−２に示した通
りで、本発明の忌避剤は、対照品と比較してチ
ヤバネコゴキブリの雄成虫および雌成虫に対し
て、優れた忌避効果を示した。
(A) Industrial Application Field The present invention relates to a cockroach repellent that is safe for the human body. More specifically, the present invention relates to a cockroach repellent characterized by containing as an active ingredient anise oil and/or bay oil, which are natural essential oils that have been used as fragrances since ancient times. (B) Conventional technology There are approximately 44 types of cockroaches distributed around the world, mainly in tropical regions, but examples of domestic cockroaches in Japan include the German cockroach, black cockroach, Yamato cockroach, and American cockroach. well known. These cockroaches are not only food pests, but also pests that are extremely unclean in terms of hygiene, along with houseflies as disease propagators. These cockroaches are omnivorous pests that congregate and hide in crevices where they have favorable access to water and food, and wander around at night on food scraps in the kitchen. In recent years, the distribution area and number of cockroaches have been increasing significantly. These phenomena have occurred because the spread of heating equipment in homes and buildings and the abundance of food have encouraged winter habitat and multiplication activities. Methods for controlling these cockroaches include spraying or applying highly persistent insecticides to cockroaches' hiding places and passageways, taking advantage of their nocturnal activity, and using containers that have been sprayed or applied, or by using their aggregation properties. A method of capturing cockroaches using a container containing both an adhesive and an attractant, and a method of repelling cockroaches by using a container coated with a repellent to take advantage of its repellent action are known. Examples of repellents that utilize the action of repelling cockroaches include menthol (Japanese Patent Application Laid-open No. 104202-1983),
Known examples include N-geranyl dimethylamine, N-citronel dimethylamine, N-neryl dimethylamine (Japanese Patent Publication No. 58-113105), cinnamyl alcohol, eugenol, safrole, cinnamyl acetate (Japanese Patent Application Publication No. 50-105821), etc. There is. (C) Problems to be solved by the invention Examples of the above-mentioned menthol, N-geranyldimethylamine, N-citronellyldimethylamine, N-neryldimethylamine, cinnamyl alcohol, which have been reported as cockroach repellents in the past. The repellent action of eugenol, safrole, cinnamyl acetate, etc. against cockroaches has the disadvantage that it is not always satisfactory. (D) Means for Solving the Problems In order to solve the above-mentioned disadvantages and disadvantages, the present inventors have conducted extensive research on the repellent effects of a large number of fragrances on cockroaches. As a result, it was discovered that anise oil and/or bay oil, which are natural essential oils that have been used as fragrances since ancient times, have an extremely excellent repellent effect on cockroaches and have an excellent long-lasting effect. Anise oil and bay oil, which are natural essential oils used as active ingredients in the cockroach repellent of the present invention, are easily available on the market. In the cockroach repellent of the present invention, such natural essential oils can be used alone or in combination as a cockroach repellent as they are, but they can also be used after being adsorbed, mixed or dispersed on a suitable carrier. Examples of the carrier include geriatric earth, alumina, acid clay, wood flour, kaolin, bennite, activated carbon, and silica. These carriers can also be used singly or as a mixture of two or more.
It can also be used by impregnating or kneading various synthetic resins. Furthermore, if necessary, emulsifiers, dispersants, suspending agents, spreading agents, penetrants, wetting agents, stabilizers, etc. may be added to produce oils, emulsions, wettable powders, powders, tablets, etc.
It can also be used in the form of a spray. The cockroach repellent of the present invention also includes anise oil and/or
Or insecticides, synergists, other repellents in addition to bay oil,
It can also be used in combination with fragrances, bactericides, antifungal agents, etc. The cockroach repellent of the present invention, which can be obtained as described above, can be used to repel cockroaches by, for example, directly spraying, dispersing, or applying the cockroach habitat, hiding place, or passageway. It is possible to effectively prevent damage caused by cockroaches by forcing them to escape from a certain area. There is no particular restriction on the amount of anise oil and/or bay oil to be used, which are the active ingredients of the cockroach repellent of the present invention, and they can be selected and used as appropriate. It is not necessary to use a particularly large amount in order to show a repellent effect in a small amount, but for example, when creating a repellent area by coating, aerosol, etc.
g/ cm2 or more or as an active ingredient in the air
It is desirable to have it present at 0.5 ppm or more. (E) Effect It was discovered for the first time by the present invention that the natural essential oils selected from anise oil and bay oil, which are the active ingredients used in the cockroach repellent of the present invention, exhibit a repellent effect against cockroaches. , its action and effects will be illustrated by the following examples. (F) Example (1) A piece of 10 cm x 4.5 cm square paper is folded into a corrugated shape large enough for cockroaches to penetrate, and 0.05 ml of the present invention product and the control product are applied to the paper at a constant concentration. Next, place two pieces of corrugated paper coated with the same type of cockroach repellent and two pieces of blank corrugated opening paper on the four corners of a transparent plastic case for rearing cockroaches, measuring 40 cm long, 25 cm wide, and 28 cm high. They were placed alternately and the repellent effect was observed. (Due to their habit, cockroaches tend to gather in dark places in the corners of rearing cases.) To determine the repellent effect, a total of 20 adult German cockroaches (10 male and 10 male) were released into the above rearing case, and 3 hours later. The number of cockroaches present in a corrugated piece of paper coated with a cockroach repellent was determined. The results are shown in Tables 1 and 2, and the repellent of the present invention showed superior repellent effects against male and female adult German cockroaches compared to the control product. .
【表】【table】
【表】
表中の数字は、忌避剤を塗布した波型のロ
紙の中に残つていたチヤバネゴキブリの数を
示す。
(2) 実施例(1)で用いた忌避剤を塗布した波型のロ
紙を全部ブランクにした波型のロ紙に変えた他
は、実施例(1)と同様に行つて、ロ紙中に居るチ
ヤバネゴキブリの数を観察した。その結果、４
ケのロ紙中に居るチヤバネゴキブリの合計数は
19匹であつた。
(G) 発明の効果
本発明のゴキブリ忌避剤として利用できる、ア
ニス油及びベイ油は、古くから香料として使用さ
れていて人体に対して安全であるためその使用場
所に制限されることなく利用できる。又本発明の
ゴキブリ忌避剤は、従来知られている忌避剤に比
べて、その忌避効果ならびに持続性が優れ、且つ
工業的に容易に製造することができる。[Table] The numbers in the table indicate the number of German cockroaches remaining in the corrugated paper coated with repellent.
(2) The process was carried out in the same manner as in Example (1), except that the repellent-coated corrugated paper used in Example (1) was replaced with a blank corrugated paper. The number of German cockroaches inside was observed. As a result, 4
The total number of cockroaches in the paper is
There were 19 fish. (G) Effects of the invention Anise oil and bay oil, which can be used as the cockroach repellent of the present invention, have been used as fragrances since ancient times and are safe for the human body, so they can be used without being restricted to where they can be used. . Furthermore, the cockroach repellent of the present invention has superior repellent effect and durability compared to conventionally known repellents, and can be easily manufactured industrially.
Claims (1)
含有することを特徴とするゴキブリ忌避剤。1. A cockroach repellent characterized by containing anise oil and/or bay oil as an active ingredient.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61297808A JPS63150206A (en) | 1986-12-16 | 1986-12-16 | cockroach repellent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP61297808A JPS63150206A (en) | 1986-12-16 | 1986-12-16 | cockroach repellent |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| JPS63150206A JPS63150206A (en) | 1988-06-22 |
| JPH0580445B2 true JPH0580445B2 (en) | 1993-11-09 |
Family
ID=17851435
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| JP61297808A Granted JPS63150206A (en) | 1986-12-16 | 1986-12-16 | cockroach repellent |
Country Status (1)
| Country | Link |
|---|---|
| JP (1) | JPS63150206A (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5688509A (en) * | 1996-02-20 | 1997-11-18 | Tenneco Packaging | Controlled-release insect repellent device |
| JP2004182704A (en) * | 2002-12-06 | 2004-07-02 | S T Chem Co Ltd | Insect repellents for cereals and dry matter and methods for controlling cereals and dry matter pests |
| JP2005255664A (en) * | 2004-02-12 | 2005-09-22 | Tomoko Hayase | Food pest repellent and repelling method |
-
1986
- 1986-12-16 JP JP61297808A patent/JPS63150206A/en active Granted
Also Published As
| Publication number | Publication date |
|---|---|
| JPS63150206A (en) | 1988-06-22 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| LAPS | Cancellation because of no payment of annual fees |