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JP2018161354A - Filter material for food - Google Patents

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JP2018161354A
JP2018161354A JP2017061097A JP2017061097A JP2018161354A JP 2018161354 A JP2018161354 A JP 2018161354A JP 2017061097 A JP2017061097 A JP 2017061097A JP 2017061097 A JP2017061097 A JP 2017061097A JP 2018161354 A JP2018161354 A JP 2018161354A
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nonwoven fabric
filter material
food
basis weight
layer
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JP6836439B2 (en
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裕也 藤本
Yuya Fujimoto
裕也 藤本
祥吾 池田
Shogo Ikeda
祥吾 池田
留美名 小尾
Rumina Koo
留美名 小尾
一史 加藤
Kazufumi Kato
一史 加藤
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Asahi Kasei Corp
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Abstract

PROBLEM TO BE SOLVED: To provide while retaining conventional powder leakage property and heat sealability, a nonwoven fabric which is excellent in bag-making suitability of preventing slip-down from a conveyance arm in packaging and collapse in overlapping, caused by the low basis weight of a nonwoven fabric, aiming at improvement of an extraction speed, reduction of a cost, and improvement of beauty of exterior appearance such as transparency and glossiness during a general bag-making step of food filter application or the like.SOLUTION: A filter material for food has an average fiber diameter of a thermoplastic synthetic fiber constituting a nonwoven fabric of 10-30 μm, and a total basis weight of 10-50 g/m, and comprises a laminated nonwoven fabric whose flexural rigidity index obtained by following formula of [a flexural rigidity index {(gf cm)/(g/m)}×10={flexural rigidity (gf cm) with a KES flexural rigidity test machine/total basis weight (g/m)}×10] is 54-206.SELECTED DRAWING: Figure 1

Description

本発明は、食品用フィルター材、特に飲料用の抽出、出汁の抽出に用いて、抽出速度の向上やコスト低減などを目的とした低目付化に伴う曲げ剛性の低下により発生する一般的な製袋工程における問題を解消する不織布からなる食品用フィルター材に関する。   The present invention is used in food filter materials, particularly for beverage extraction and soup extraction, and is a general product that occurs due to a decrease in flexural rigidity accompanying a reduction in weight per unit for the purpose of improving extraction speed and reducing costs. It is related with the filter material for foodstuffs which consists of a nonwoven fabric which eliminates the problem in a bag process.

従来から、食品用のフィルター材として、緑茶、紅茶、麦茶、烏龍茶、レギュラーコーヒー、鰹出汁、鰯出汁などの抽出材料の成分抽出のために熱可塑性合成繊維の不織布が広く使用されている。近年、特に抽出用シートの抽出性の向上やコスト低減、さらには透明感や光沢感といった外観の美しさの向上のために、低目付の不織布が必要とされる傾向にある。   Conventionally, nonwoven fabrics of thermoplastic synthetic fibers have been widely used as filter materials for foods for extracting components of extraction materials such as green tea, black tea, barley tea, oolong tea, regular coffee, koji soup and koji soup. In recent years, nonwoven fabrics with a low basis weight tend to be required in order to improve the extractability of the extraction sheet, reduce costs, and improve the beauty of the appearance such as transparency and gloss.

しかしながら、低目付の不織布からなる商品用フィルター材は、一般に薄く、剛性が低下するため、一般的な製袋機械における取扱いが難しく、機械適正が低いという問題がある。例えば、茶葉などの抽出材料を封入した抽出用バッグは、それがピロー型である場合には、一般に抽出材料によって不均一に膨らんだ形状となってしまうため、複数個重ねた際には不安定になりやすい。特に低目付の不織布からなる抽出用バッグの場合は、それがより顕著となり、梱包時搬送アームからのずり落ちや積み重ね時に崩れてしまい、取扱い性が低いという問題がある。   However, a commercial filter material made of a nonwoven fabric having a low basis weight is generally thin and has a low rigidity, so that it is difficult to handle in a general bag-making machine and has low mechanical suitability. For example, an extraction bag containing an extraction material such as tea leaves generally has a shape that bulges unevenly due to the extraction material when it is a pillow type. It is easy to become. In particular, in the case of an extraction bag made of a non-woven fabric with a low basis weight, this becomes more prominent, and there is a problem that the handleability is low due to slippage from the transport arm during packing or collapse during stacking.

他方で、一般に紙製の抽出シートは低目付においても曲げ剛性が高く、抽出用バッグの保型性が高くなるため、抽出用バッグなどの製造の際に取扱い性が高い。しかしながら、紙は透明度が低く、抽出速度が遅い。さらには抽出時に紙由来の苦み成分が溶出し、風味を害してしまうといった問題があり、これらの点が、紙を抽出用バッグとして使用するデメリットとなっている。   On the other hand, generally an extraction sheet made of paper has high bending rigidity even at a low basis weight, and the shape retaining property of the extraction bag becomes high, so that it is easy to handle when manufacturing an extraction bag or the like. However, paper is low in transparency and extraction speed is slow. Furthermore, there is a problem that the bitter component derived from paper is eluted at the time of extraction, and the flavor is impaired. These points are disadvantages of using paper as an extraction bag.

以下の特許文献1には、不織布として、粉漏れが少なく、ヒートシール性、成分抽出性、曲げ剛性などに優れた食品用フィルター材、及びそれを用いた食品封入風袋の製法が開示されている。しかしながら目付に対する曲げ剛性が小さく、抽出性向上やコスト低減などを目的とした低目付化、特に、目付15g/m以下においては、製袋適正を顕著に満たさなくなってしまう。 The following Patent Document 1 discloses a filter material for food that has less powder leakage and is excellent in heat sealability, component extractability, bending rigidity, and the like, and a method for producing a food-filled tare using the same as a non-woven fabric. . However, the bending rigidity with respect to the fabric weight is small, and when the fabric weight is lowered for the purpose of improving the extractability and reducing the cost, in particular, when the fabric weight is 15 g / m 2 or less, the bag-making suitability is not sufficiently satisfied.

また、以下の特許文献2には、ポリ乳酸系樹脂の繊維からなるメルトブロウン不織布の結晶性を低くすることで折れ目が付き易くなる性質を利用し、折れ目線をつける、あるいは屈曲させるなどして、ぴんと張ったまっすぐな状態とし、抽出用バッグの保型性を向上させることが開示されている。しかしながら、結晶性の低いメルトブロウン繊維は低融点側にブロードな融解ピークを有し、一般的な製袋工程におけるヒートシール時に、ヒートシールバーへ樹脂が付着しやすくなってしまう。特にPLA樹脂はPP樹脂やPET樹脂と比べて熱に対する分解性が非常に高く、抽出用バッグへの分解物付着による品位の低下、さらには一定の時間毎に汚れの拭き取りが必要となり、生産量の低下にも繋がる。   In addition, Patent Document 2 below uses a property that a crease is easily formed by lowering the crystallinity of a melt-blown nonwoven fabric made of polylactic acid resin fibers, and makes a crease line or bends. In addition, it is disclosed that a tight and straight state is provided to improve the shape retention of the extraction bag. However, melt-blown fibers having low crystallinity have a broad melting peak on the low melting point side, and the resin tends to adhere to the heat seal bar during heat sealing in a general bag making process. In particular, PLA resin has a very high heat decomposability compared to PP resin and PET resin, and the quality is reduced due to degradation products adhering to the extraction bag, and it is necessary to wipe off the dirt at regular intervals. It also leads to a decline.

さらに、以下の特許文献3には、曲げ剛性というパラメータに特化し、風合いに優れたスパンボンド不織布が開示されている。しかしながら、風合いの確保のために、曲げ剛性を小さくするという技術思想が開示されているにすぎない。   Furthermore, the following Patent Document 3 discloses a spunbonded nonwoven fabric specializing in a parameter called bending rigidity and having an excellent texture. However, only the technical idea of reducing the bending rigidity in order to ensure the texture is disclosed.

特開2008−54840号公報JP 2008-54840 A 国際公開第2016/147978号International Publication No. 2016/147978 特開2014−141752号公報JP 2014-141752 A

前記した従来技術の問題点に鑑み、本発明が解決しようとする課題は、食品フィルター用途等の一般的な製袋工程において抽出速度の向上やコストの低減、さらには透明感や光沢感といった外観の美しさの向上を目的とした不織布の低目付化により生じる梱包時搬送アームからのずり落ちや積み重ね時の崩れを発生させない製袋適正に優れた不織布を、従来の粉漏れ性、ヒートシール性を維持したまま提供することである。   In view of the above-described problems of the prior art, the problem to be solved by the present invention is to improve the extraction speed and reduce the cost in a general bag making process such as food filter use, and further, the appearance such as transparency and gloss. Non-woven fabrics with excellent bag-making properties that do not cause slippage from the transfer arm during packing or collapse during stacking due to the low weight of nonwoven fabrics for the purpose of improving the beauty of the fabric. It is to provide while maintaining.

本発明者らは、前記課題を解決するため鋭意検討した結果、エンボスロールによる熱接着方法を工夫し、非エンボス箇所の糸-糸接着点数を増やすこと、さらには厚みを維持することにより不織布の曲げ剛性が飛躍的に向上することを見出し、本発明を完成するに至ったものである。
すなわち、本発明は、以下の通りのものである。
As a result of intensive studies to solve the above problems, the present inventors have devised a heat bonding method using an embossing roll, increasing the number of yarn-thread bonding points at non-embossed portions, and further maintaining the thickness of the nonwoven fabric. The present inventors have found that the bending rigidity is dramatically improved and have completed the present invention.
That is, the present invention is as follows.

[1]不織布を構成する熱可塑性合成繊維の平均繊維径が10〜30μmであり、総目付が10〜50g/mであり、かつ、以下の式:
曲げ剛性指数{(gf・cm)/(g/m2.5}×106={KES曲げ剛性試験機による曲げ剛性(gf・cm)/総目付(g/m2.5}×106
で求められる曲げ剛性指数{(gf・cm)/(g/m2.5}×106が54〜206であることを特徴とする積層不織布からなる食品用フィルター材。
[2]前記積層不織布のエンボス端部から0.3mm地点までの糸同士の接着点数が10個以上ある、前記[1]に記載の食品用フィルター材。
[3]前記積層不織布の厚みが0.06mm以上である、前記[1]又は[2]に記載の食品用フィルター材。
[4]前記積層不織布の結晶化度が30%以上である、前記[1]〜[3]のいずれかに記載の食品用フィルター材。
[5]前記積層不織布が複数の層で構成され、該複数の層の内少なくとも1層が熱可塑性合成樹脂の繊維から構成される不織布層であり、他の1の層が、該少なくとも1層の熱可塑性剛性樹脂の融点より30℃〜150℃低い融点を有する熱可塑性合成樹脂の繊維から構成される不織布層である、前記[1]〜[4]のいずれかに記載の食品用フィルター材。
[6]シール強度が2〜50N/25mmである、前記[1]〜[5]のいずれかに記載の食品用フィルター材。
[1] The average fiber diameter of the thermoplastic synthetic fibers constituting the nonwoven fabric is 10 to 30 μm, the total basis weight is 10 to 50 g / m 2 , and the following formula:
Bending stiffness index {(gf · cm) / (g / m 2 ) 2.5 } × 10 6 = {Bending stiffness (gf · cm) / total basis weight (g / m 2 ) by KES bending stiffness tester 2.5 } × 10 6
A food filter material comprising a laminated nonwoven fabric, wherein the flexural rigidity index {(gf · cm) / (g / m 2 ) 2.5 } × 10 6 determined by the formula ( 1 ) is 54 to 206.
[2] The food filter material according to [1], wherein the number of adhesion points between yarns from the embossed end of the laminated nonwoven fabric to a point of 0.3 mm is 10 or more.
[3] The food filter material according to [1] or [2], wherein the thickness of the laminated nonwoven fabric is 0.06 mm or more.
[4] The food filter material according to any one of [1] to [3], wherein the laminated nonwoven fabric has a crystallinity of 30% or more.
[5] The laminated nonwoven fabric is composed of a plurality of layers, at least one of the plurality of layers is a nonwoven fabric layer composed of fibers of thermoplastic synthetic resin, and the other layer is the at least one layer. The food filter material according to any one of [1] to [4], wherein the filter material is a nonwoven fabric layer composed of fibers of a thermoplastic synthetic resin having a melting point lower by 30 ° C to 150 ° C than the melting point of the thermoplastic rigid resin. .
[6] The food filter material according to any one of [1] to [5], wherein the seal strength is 2 to 50 N / 25 mm.

本発明の積層不織布からなる食品用フィルター材は、抽出速度の向上やコスト低減などを目的とする低目付化、さらには透明感や光沢感といった外観の美しさの向上を目的とした不織布の低目付化において、従来の食品フィルター用不織布に対し、粉漏れ性、ヒートシール性を維持したまま、製袋時に発生する梱包時搬送アームからのずり落ちや積み重ね時の崩れを解消する。   The filter material for foods comprising the laminated nonwoven fabric of the present invention is a low-weight nonwoven fabric for the purpose of improving the extraction rate and lowering the weight for the purpose of cost reduction, and further improving the appearance of the appearance such as transparency and gloss. In weighting, the conventional food filter non-woven fabric retains powder leakage and heat sealability, and eliminates slipping from the transport arm during packing and collapse during stacking.

曲げ剛性指数{(gf・cm)/(g/m2.5}×106と目付との関係を示すグラフである。It is a graph which shows the relationship between bending rigidity index {(gf * cm) / (g / m < 2 >) 2.5 } * 10 < 6 > and a fabric weight. 目付15g/mにおける曲げ剛性(gf・cm)と厚み(mm)との関係を示すグラフである。It is a graph which shows the relationship between the bending rigidity (gf * cm) in 15 g / m < 2 > of fabric weight, and thickness (mm). 糸同士の接着点数が多いことを示すSEM写真である。It is a SEM photograph which shows that there are many adhesion points of thread | yarns. 糸同士の接着点数が無いことを示すSEM写真である。It is a SEM photograph which shows that there is no number of adhesion points of yarns.

以下、本発明の実施形態を詳細に説明する。
本実施形態の食品用フィルター材は、不織布を構成する熱可塑性合成繊維の平均繊維径が10〜30μmであり、総目付が10〜30g/mであり、かつ、以下の式:
曲げ剛性指数{(gf・cm)/(g/m2.5}×106={KES曲げ剛性試験機による曲げ剛性(gf・cm)/総目付(g/m2.5}×106
で求められる曲げ剛性指数{(gf・cm)/(g/m2.5}×106が54〜206であることを特徴とする積層不織布からなる食品用フィルター材である。
積層不織布は、例えば、第1層が高融点の熱可塑性繊維(S)、第2層が第1層を構成する樹脂を芯側、該樹脂の融点より30℃以上低融点の樹脂を鞘側とする熱可塑性鞘芯剛性繊維(W)を積層し、熱圧着で一体化したS/Wの構造を有する積層不織布であることができる。
特に、第2層の鞘芯繊維極細繊維(W)では、1層と第2層の融点差を設けることで、熱圧着により、層間の接合が強固にでき、熱シール強度及び温度範囲が広くできるなどの特徴が得られる。
Hereinafter, embodiments of the present invention will be described in detail.
The filter material for food of this embodiment has an average fiber diameter of 10 to 30 μm, a total basis weight of 10 to 30 g / m 2 , and the following formula:
Bending stiffness index {(gf · cm) / (g / m 2 ) 2.5 } × 10 6 = {Bending stiffness (gf · cm) / total basis weight (g / m 2 ) by KES bending stiffness tester 2.5 } × 10 6
Is a food filter material comprising a laminated nonwoven fabric, wherein the flexural rigidity index {(gf · cm) / (g / m 2 ) 2.5 } × 10 6 determined by the formula ( 1 ) is 54 to 206.
In the laminated nonwoven fabric, for example, the first layer is a thermoplastic fiber (S) having a high melting point, the second layer is a resin constituting the first layer, the core side, and a resin having a melting point lower by 30 ° C. or more than the melting point of the resin is the sheath side. A laminated nonwoven fabric having an S / W structure in which the thermoplastic sheath-core rigid fibers (W) are laminated and integrated by thermocompression bonding.
In particular, in the second-layer sheath-core fiber ultra-fine fiber (W), by providing a difference in melting point between the first layer and the second layer, the bonding between the layers can be strengthened by thermocompression bonding, and the heat seal strength and temperature range are wide. Features such as can be obtained.

積層不織布としては、第1層と第2層の間に粉漏れ性の向上を目的とし、これらの層間に極細繊維を積層させたものでもよい。   The laminated nonwoven fabric may be obtained by laminating ultrafine fibers between these layers for the purpose of improving powder leakage between the first layer and the second layer.

第1層の高融点の熱可塑性合成繊維層は、通常、繊維径が10〜30μm、好ましくは12〜20μmの太い繊維から成り、強度、通気性に優れ、磨耗強度が大きいことが好ましい。このような構成繊維としては、例えば、ポリエチレンテレフタレート、ポリブチレンテレフタレート、共重合ポリエステルなどのポリエステル系繊維、ナイロン6、ナイロン66、共重合ポリアミド繊維などのポリアミド系繊維などの合成繊維が挙げられる。   The high-melting thermoplastic synthetic fiber layer of the first layer is usually composed of thick fibers having a fiber diameter of 10 to 30 μm, preferably 12 to 20 μm, and is preferably excellent in strength and breathability and has high wear strength. Examples of such constituent fibers include synthetic fibers such as polyester fibers such as polyethylene terephthalate, polybutylene terephthalate, and copolyester, and polyamide fibers such as nylon 6, nylon 66, and copolyamide fibers.

第2層の熱可塑性合成繊維層は、第1層の繊維より30℃以上、好ましくは50℃以上低融点の繊維からなり、袋構造体の熱シール面となる。繊維径は10〜30μm、好ましくは12〜20μmmの太い繊維が好ましい。構成繊維としては、例えば、低密度ポリエチレン、高密度ポリエチレン、ポリプロピレン、共重合ポリエチレン、共重合ポリプロピレンなどのオレフイン系繊維、ポリエチレンテレフタレートにフタル酸、イソフタル酸、セバシン酸、アジピン酸、ジエチレングリコール、1,4-ブタンジオールの1種又は2種以上の化合物を共重合した芳香族ポリエステル共重合体、脂肪族ポリエステルなどのポリエステル系繊維、共重合ポリアミド繊維などの合成繊維が用いられる。さらに、芯鞘構造、サイドバイサイドなどの2成分からなる複合繊維、例えば、芯が高融点で鞘が低融点の複合繊維で、具体的には、芯がポリエチレンテレフタレート、ポリブチレンテレフタレート、共重合ポリエステル、ナイロン6、ナイロン66、共重合ポリアミドなどの高融点繊維、鞘が低密度ポリエチレン、高密度ポリエチレン、ポリプロピレン、共重合ポリエチレン、共重合ポリプロピレン、共重合ポリエステル、脂肪族ポリエステルなどの低融点繊維が好ましい。   The thermoplastic synthetic fiber layer of the second layer is made of fibers having a melting point lower than that of the fibers of the first layer by 30 ° C. or more, preferably 50 ° C. or more, and serves as a heat seal surface of the bag structure. A thick fiber having a fiber diameter of 10 to 30 μm, preferably 12 to 20 μm is preferable. Examples of the constituent fiber include olefin fibers such as low density polyethylene, high density polyethylene, polypropylene, copolymer polyethylene, copolymer polypropylene, polyethylene terephthalate, phthalic acid, isophthalic acid, sebacic acid, adipic acid, diethylene glycol, 1,4 -Synthetic fibers such as aromatic polyester copolymers obtained by copolymerizing one or more butanediol compounds, polyester fibers such as aliphatic polyesters, and copolymerized polyamide fibers are used. Furthermore, a composite fiber composed of two components such as a core-sheath structure and side-by-side, for example, a composite fiber having a high melting point in the core and a low melting point in the sheath, specifically, the core is polyethylene terephthalate, polybutylene terephthalate, copolymer polyester, High melting point fibers such as nylon 6, nylon 66, copolymerized polyamide, and the like, and low melting point fibers such as low density polyethylene, high density polyethylene, polypropylene, copolymerized polyethylene, copolymerized polypropylene, copolymerized polyester, and aliphatic polyester as the sheath are preferable.

積層不織布の製法は特に限定しないが、好ましくは第1層、第2層はスパンボンド法、極細繊維層はメルトブロウン法であることができる。   Although the manufacturing method of a laminated nonwoven fabric is not specifically limited, Preferably a 1st layer and a 2nd layer can be a spunbond method, and an ultrafine fiber layer can be a meltblown method.

積層不織布の結晶化度は、30%以上であることが、好ましくは35%以上である。結晶化度が30%を下回るとヒートシール時の熱収縮が大きくなり、シール不良による粉漏れ、品位の低下に繋がる。また、低温度側にブロードな融解ピークを有し、製袋工程におけるヒートシール時にヒートシールバーへ樹脂が付着しやすくなってしまう。それにより、熱分解物が抽出用バッグに付着することで品位の低下に繋がる。   The crystallinity of the laminated nonwoven fabric is 30% or more, preferably 35% or more. When the degree of crystallinity is less than 30%, thermal shrinkage at the time of heat sealing increases, leading to powder leakage and poor quality due to poor sealing. Moreover, it has a broad melting peak on the low temperature side, and the resin tends to adhere to the heat seal bar during heat sealing in the bag making process. As a result, the pyrolyzate adheres to the extraction bag, leading to a reduction in quality.

極細繊維の繊維径は7μm以下であることが好ましく、より好ましくは1〜5μmであり、繊維間隙、及び最大開口径を小さくし、粉漏れ性を少なくする役目を有する。特に太い繊維間隙に、極細繊維が被覆するように積層されることにより、少ない極細繊維比率で繊維間隙を小さくできる。繊維径が7μmを超えると繊維間隙の被覆効果が低下する。   The fiber diameter of the ultrafine fiber is preferably 7 μm or less, more preferably 1 to 5 μm, and serves to reduce the fiber gap and the maximum opening diameter, thereby reducing powder leakage. In particular, by laminating the fine fiber gaps so that the fine fibers are covered, the fiber gaps can be reduced with a small fine fiber ratio. When the fiber diameter exceeds 7 μm, the effect of covering the fiber gap decreases.

極細繊維の目付は、1g/m以上が好ましく、より好ましくは1.5〜10g/m、さらに好ましくは2〜7g/mである。極細繊維の目付が1g/m未満では、極細繊維層の分散性が不充分となる。 Basis weight of the microfibers, 1 g / m 2 or more, more preferably 1.5~10g / m 2, more preferably from 2~7g / m 2. When the basis weight of the ultrafine fiber is less than 1 g / m 2 , the dispersibility of the ultrafine fiber layer becomes insufficient.

極細繊維の結晶化度は、10%以上が好ましく、より好ましくは20%以上、さらに好ましくは30%以上である。結晶化度が10%を下回ると融点が低温度側にブロードな融解ピークを有し、製袋工程におけるヒートシール時に樹脂がシールバ―へ付着し、熱分解物が抽出用バッグに付着することで品位の低下に繋がる。   The crystallinity of the ultrafine fibers is preferably 10% or more, more preferably 20% or more, and further preferably 30% or more. When the crystallinity is less than 10%, the melting point has a broad melting peak on the low temperature side, the resin adheres to the seal bar during heat sealing in the bag making process, and the thermal decomposition product adheres to the extraction bag. This leads to a decline in quality.

積層不織布全体に対する極細繊維の含有比率は、通常、5〜50wt%、好ましくは7〜30wt%である。極細繊維としては、例えば、ポリエチレン、ポリプロピレンなどのポリオレフィン系繊維、ナイロン6、ナイロン66などのポリアミド系繊維、ポリエチレンテレフタレート、ポリブチレンテレフタレート、共重合ポリエステル、脂肪族ポリエステルなどである。   The content ratio of the ultrafine fibers with respect to the entire laminated nonwoven fabric is usually 5 to 50 wt%, preferably 7 to 30 wt%. Examples of the ultrafine fibers include polyolefin fibers such as polyethylene and polypropylene, polyamide fibers such as nylon 6 and nylon 66, polyethylene terephthalate, polybutylene terephthalate, copolymerized polyester, and aliphatic polyester.

積層不織布は、第1層と第2層の繊維に融点差を有することであるが、第2層を構成する繊維の融点は、好ましくは30℃以上、より好ましくは50〜150℃の範囲で第1層を構成する繊維の融点より低温であることが好ましい。かかる融点差により、部分熱圧着時のロール温度範囲が広く設定できる。熱圧着ロール温度の上下差が150℃を超える場合は、高融点側のロール温度の影響を受けて低融繊維の劣化が生じ易くなる。他方、第1層と第2層との融点差が30℃未満の場合は、熱圧着温度範囲が狭くなり、ロール温度の条件により強度、摩擦毛羽強度が影響を受け易くなる。   The laminated nonwoven fabric has a melting point difference between the fibers of the first layer and the second layer, but the melting point of the fibers constituting the second layer is preferably 30 ° C. or higher, more preferably in the range of 50 to 150 ° C. The temperature is preferably lower than the melting point of the fibers constituting the first layer. The roll temperature range at the time of partial thermocompression bonding can be set wide due to such a melting point difference. When the difference between the upper and lower sides of the thermocompression-bonding roll temperature exceeds 150 ° C., the low-melting fiber tends to deteriorate due to the influence of the roll temperature on the high melting point side. On the other hand, when the melting point difference between the first layer and the second layer is less than 30 ° C., the thermocompression bonding temperature range becomes narrow, and the strength and the friction fluff strength are easily affected by the roll temperature conditions.

積層不織布を熱圧着で一体化するとは、例えば、公知のエンボスロールと平滑ロール間で加熱、圧着して接合することである。加熱温度は、繊維の軟化温度以上の温度〜融点以下の温度範囲である。しかしながら、低融点繊維の熱劣化を考慮した場合、上下ロールの温度差を150℃以下とすることが好ましく、130℃以下がより好ましい。熱圧着の圧力は、好ましくは10〜1000kPa/cm、より好ましくは50〜700kPa/cmである。   The integration of the laminated nonwoven fabric by thermocompression bonding means, for example, heating and pressure bonding between a known embossing roll and a smooth roll to join them. The heating temperature is in the temperature range from the temperature above the softening temperature of the fiber to the melting point. However, in consideration of thermal degradation of the low melting point fiber, the temperature difference between the upper and lower rolls is preferably 150 ° C. or less, and more preferably 130 ° C. or less. The pressure for thermocompression bonding is preferably 10 to 1000 kPa / cm, more preferably 50 to 700 kPa / cm.

本実施形態の食品用フィルター材を構成する積層不織布では、エンボスロールの柄、ピッチ、リピート、深さ、接着面積率を制御することで、エンボス端部から0.3mm地点以内の糸同士の接着点数を増やし、さらには厚みを維持することで、図1に示すように、従来の不織布よりも、総目付当たりの曲げ剛性、すなわち、曲げ剛性指数(cm−1)の値を一段階向上させている。具体的にはピッチ、リピートを小さくすることで糸同士の接着点数を増加させ、さらには深さを大きくすることで厚みを維持し、曲げ剛性を飛躍的に向上させている。 In the laminated nonwoven fabric constituting the food filter material of the present embodiment, by controlling the pattern, pitch, repeat, depth, and adhesion area ratio of the embossing roll, the yarns within 0.3 mm from the embossed end can be bonded to each other. By increasing the number of points and maintaining the thickness, as shown in FIG. 1, the bending stiffness per unit weight, that is, the value of the bending stiffness index (cm −1 ) is improved by one step as compared with the conventional nonwoven fabric. ing. Specifically, the number of adhesion points between yarns is increased by decreasing the pitch and repeat, and the thickness is maintained by increasing the depth, thereby greatly improving the bending rigidity.

積層不織布では、エンボス端部から0.3mm地点以内の糸同士の接着点数は、好ましくは10個以上であり、より好ましくは15個以上である。10個以下であると、曲げ剛性向上の効果が小さくなってしまう。なお、糸同士の接着点とは、図3において囲んでいる箇所である。図3は、接着点数が多い例、図4は接着点数が無い例を示している。   In the laminated nonwoven fabric, the number of adhesion points between yarns within 0.3 mm from the embossed end is preferably 10 or more, more preferably 15 or more. If it is 10 or less, the effect of improving the bending rigidity is reduced. In addition, the adhesion | attachment point of thread | yarns is the location enclosed in FIG. FIG. 3 shows an example in which the number of adhesion points is large, and FIG. 4 shows an example in which there is no number of adhesion points.

積層不織布の厚みは、好ましくは0.06mm以上であり、より好ましくは0.07mm以上である。厚みが0.06mm以下であると、曲げ剛性向上の効果が小さくなってしまう。   The thickness of the laminated nonwoven fabric is preferably 0.06 mm or more, more preferably 0.07 mm or more. When the thickness is 0.06 mm or less, the effect of improving the bending rigidity is reduced.

KES曲げ剛性(準曲げ試験気 KES FB2―AUTOA)は、被抽出物を入れたテトラパックなどの袋体に製袋した場合、輸送、保管及び抽出時の形状保持するために必要な特性である。本実施形態の食品用フィルター材のKES曲げ剛性は、好ましくは0.03〜0.5(gf・cm)であり、より好ましくは、0.045〜0.22(gf・cm)、さらに好ましくは、0.065〜0.22(gf・cm)である。KES曲げ剛性が0.03(gf・cm)未満では、剛性が低く、製袋加工時に加工性が低下する。他方、曲げ剛性の高い側は、製袋加工性、形状保持性が良好となり、0.5(gf・cm)以下であれば、食品用袋体に用いた場合、被抽出物のお湯による膨潤、拡大などを拘束するなどの問題が生じない。   KES flexural rigidity (quasi-bending test air KES FB2-AUTOA) is a characteristic necessary to maintain the shape during transportation, storage, and extraction when the bag is made into a bag such as a Tetra Pak containing the extract. . The KES bending rigidity of the food filter material of the present embodiment is preferably 0.03 to 0.5 (gf · cm), more preferably 0.045 to 0.22 (gf · cm), and still more preferably. Is 0.065 to 0.22 (gf · cm). If the KES bending rigidity is less than 0.03 (gf · cm), the rigidity is low, and the workability deteriorates during bag making. On the other hand, the side with high bending rigidity has good bag-making processability and shape retention, and if it is 0.5 (gf · cm) or less, it will swell due to hot water of the extractable when used in food bags. , Problems such as restraining expansion do not occur.

本実施形態の食品用フィルター材を構成する積層不織布では、以下の式:
曲げ剛性指数{(gf・cm)/(g/m2.5}×106={KES曲げ剛性試験機による曲げ剛性(gf・cm)/総目付(g/m2.5}×106
で求められる曲げ剛性指数は、54〜206であり、好ましくは66〜206、より好ましくは66〜150である。
In the laminated nonwoven fabric constituting the food filter material of the present embodiment, the following formula:
Bending stiffness index {(gf · cm) / (g / m 2 ) 2.5 } × 10 6 = {Bending stiffness (gf · cm) / total basis weight (g / m 2 ) by KES bending stiffness tester 2.5 } × 10 6
The flexural rigidity index determined by is from 54 to 206, preferably from 66 to 206, more preferably from 66 to 150.

前記したKES曲げ剛性、及び曲げ剛性指数は、目付を上げることにより、あるいはエンボス面積率を増加させていくことにより達成可能であるが、これらの手法では、通気度や開孔径を必要以上に小さくしてしまうことに繋がり、抽出速度や透明度の低下は避けられない。本実施形態の食品用フィルター材では、糸同士の接着点数や厚みといった、抽出速度に影響を与えない因子を制御することによって、通気度や開孔径、すなわち抽出速度や透明度を変えないまま曲げ剛性の向上を狙うものである。   The above-mentioned KES bending stiffness and bending stiffness index can be achieved by increasing the basis weight or increasing the embossed area ratio. However, in these methods, the air permeability and the aperture diameter are made smaller than necessary. This leads to a decrease in extraction speed and transparency. In the food filter material of this embodiment, by controlling factors that do not affect the extraction speed, such as the number of adhesion points and thickness between yarns, the bending rigidity and the pore diameter, that is, the bending rigidity without changing the extraction speed and transparency are maintained. It aims to improve.

本実施形態の食品用フィルター材では、糸同士の接着点数を増やし、さらには厚みを維持することで飛躍的に曲げ剛性を向上させ、特に15g/m以下の薄目付においても製袋に必要な曲げ剛性を確保できるものである。 In the food filter material of this embodiment, the number of adhesive points between yarns is increased and the thickness is maintained to dramatically improve the bending rigidity. Especially, it is necessary for bag making even with a light weight of 15 g / m 2 or less. Can ensure high bending rigidity.

本実施形態の食品用フィルター材の通気度は、好ましくは50〜700cm/cm/s、より好ましくは200〜600cm/cm/s、さらに好ましくは300〜600cm/cm/sである。700cm/cm/sを超えると抽出速度は向上するが、粉漏れし易くなり、シール強度、剛性などが低下する。他方、50cm/cm/s未満では粉漏れがし難くなり、シール強度、剛性が大きくなり、成分抽出性が低下するなどがある。 The air permeability of the food filter material of the present embodiment is preferably 50 to 700 cm 3 / cm 2 / s, more preferably 200 to 600 cm 3 / cm 2 / s, and even more preferably 300 to 600 cm 3 / cm 2 / s. It is. If it exceeds 700 cm 3 / cm 2 / s, the extraction speed is improved, but powder leakage is liable to occur, and the seal strength, rigidity, etc. are reduced. On the other hand, if it is less than 50 cm 3 / cm 2 / s, powder leakage is difficult, seal strength and rigidity increase, and component extractability decreases.

本実施形態の食品用フィルター材の開孔径は、好ましくは60〜200μm、より好ましくは100〜200μm、さらに好ましくは140〜200μmである。200μmを超えると粉漏れし易くなり、シール強度、剛性などが低下する。他方、60μm未満では粉漏れがし難くなり、シール強度、剛性が大きくなり、成分抽出性が低下する。   The pore diameter of the food filter material of the present embodiment is preferably 60 to 200 μm, more preferably 100 to 200 μm, and still more preferably 140 to 200 μm. If it exceeds 200 μm, powder leakage is liable to occur, and the sealing strength, rigidity, etc. decrease. On the other hand, if it is less than 60 μm, it is difficult for powder to leak, seal strength and rigidity increase, and component extractability decreases.

積層不織布の製造において、エンボスロールピンのロール面とのなす角度は、大きいほど糸同士の接着点数が増加するという特徴があるが、隣り合うエンボスとの距離により、耐久上の限度があるため、ピッチ、リピート、接着面積率に応じ、最適な角度を選定してよい。   In the production of laminated nonwoven fabrics, the angle formed with the roll surface of the embossed roll pin is characterized by the fact that the greater the number of adhesion points between the yarns, the greater the durability, depending on the distance to the adjacent embossed pitch. The optimum angle may be selected according to the repeat and adhesion area ratio.

エンボスロール柄は、織目柄でも絹目柄でも、亀甲柄でもポイント柄でもよく、特に限定しない。
熱圧着時に、ロール間にギャップを設けることで、より厚みを維持できるクリアランスロールを使用してもよい。また、エンボスロールを用いる以外に、熱風をウェブに通過させることで糸同士を熱で圧着するエアスルー法を後加工として行ってもよい。
The embossing roll pattern may be a texture pattern, a silk pattern, a turtle shell pattern, or a point pattern, and is not particularly limited.
You may use the clearance roll which can maintain thickness more by providing a gap between rolls at the time of thermocompression bonding. In addition to using an embossing roll, an air-through method in which hot air is passed through the web and the yarns are heat-bonded may be performed as post-processing.

本実施形態の食品用フィルター材を用いたその袋体の製袋加工は、前記フィルター材の第2層を内側にして重ね合わせて、端部をシールとして、公知のシール法によりシールすることによって行われる。例えば、3包シール機、4包シール機などの熱シール法、超音波シール機などの超音波シール法などで行うことができる。さらに、2個以上の多数個連続の連包袋状に製袋加工することもできる。   The bag making process using the food filter material of the present embodiment is performed by stacking with the second layer of the filter material on the inside, and sealing the end portion as a seal by a known sealing method. Done. For example, it can be performed by a heat sealing method such as a three-pack sealing machine or a four-pack sealing machine, or an ultrasonic sealing method such as an ultrasonic sealing machine. Furthermore, it is possible to form a bag into two or more continuous continuous bags.

袋体は、例えば、袋内に充填した充填物が落下や、重量物が載った時に破袋しないため、高いシール強度が必要である。従って、袋体のシール強度は、1N/25mm以上、好ましくは1.5N/25mm以上、より好ましくは2〜50N/25mmである。シール強度が1N/25mm未満では、シール部分が剥離し易くなり、内容物が外部に漏れるなどの問題が生じる。   For example, the bag body needs to have a high sealing strength because the filling material filled in the bag does not drop or breaks when a heavy material is loaded. Therefore, the sealing strength of the bag body is 1 N / 25 mm or more, preferably 1.5 N / 25 mm or more, more preferably 2 to 50 N / 25 mm. When the seal strength is less than 1 N / 25 mm, the seal portion is easily peeled off, causing problems such as leakage of contents to the outside.

製袋加工を安定に行うためには、シール温度範囲が広いことが必要である。例えば、温度範囲が50℃以上150℃以下が好ましい。これは、シール機のシール部の温度が開始時から少しずつ上昇し、さらに環境温度により変化するなど、一定温度にコントロールすることが難しいからである。温度範囲が50℃未満の狭い範囲の設定が必要な場合には、環境温度、ヒーター部の蓄熱などの影響でシール強度が変化するなどの問題が生じる。他方、150℃を超える温度範囲では、低融点繊維の熱劣化などで物性低下などを生じる。   In order to carry out the bag making process stably, it is necessary that the sealing temperature range is wide. For example, the temperature range is preferably 50 ° C. or higher and 150 ° C. or lower. This is because it is difficult to control the temperature of the sealing portion of the sealing machine to a constant temperature, for example, the temperature gradually increases from the start and further changes depending on the environmental temperature. When the temperature range needs to be set in a narrow range of less than 50 ° C., there arises a problem that the seal strength changes due to the influence of the environmental temperature, the heat storage of the heater portion, and the like. On the other hand, in a temperature range exceeding 150 ° C., physical properties are reduced due to thermal deterioration of the low melting point fiber.

本実施形態の食品用フィルター材では、シール温度範囲を広くとることができ、且つ、高く安定したシール強度を得ることができる。これは、例えば、第1層と第2層の繊維の層間で融点差を30℃以上設けているため、低融点層の繊維が軟化または融解しても、高融点繊維が所定の繊維形状を維持しているためである。従って、製袋加工時にヒートシールバーに繊維の融解物が付着することがなくなる。   In the food filter material of this embodiment, a wide sealing temperature range can be obtained, and a high and stable sealing strength can be obtained. This is because, for example, a difference in melting point of 30 ° C. or more is provided between the fibers of the first layer and the second layer, so even if the fibers of the low melting point layer soften or melt, the high melting point fibers have a predetermined fiber shape. This is because it is maintained. Accordingly, the fiber melt does not adhere to the heat seal bar during bag making.

本実施形態の食品用フィルター材では、積層不織布が極細繊維を含む積層シートである場合であっても、結晶化度が高く、融点が低融点側へブロードとならないため、ヒートシールバ―に繊維の融解物が付着することはない。   In the filter material for food of the present embodiment, even when the laminated nonwoven fabric is a laminated sheet containing ultrafine fibers, the crystallinity is high and the melting point does not broaden to the low melting point. Things do not stick.

本実施形態の食品用フィルター材及びその袋体は、シール強度高く、剛性、成分抽出性に優れている。積層不織布の総目付は、10〜30g/m、好ましくは10〜20g/m、より好ましくは10〜16g/mである。総目付が10g/m未満では、粉漏れし易くなり、シール強度、剛性などが低下する。他方、総目付が30g/mを超えると、粉漏れがし難くなり、シール強度、剛性が大きくなり、成分抽出性が低下するなどがある。 The food filter material and the bag of the present embodiment have high sealing strength, and are excellent in rigidity and component extractability. The total basis weight of the laminated nonwoven fabric is 10 to 30 g / m 2 , preferably 10 to 20 g / m 2 , more preferably 10 to 16 g / m 2 . When the total basis weight is less than 10 g / m 2 , powder leakage is likely to occur, and the seal strength, rigidity, and the like are reduced. On the other hand, when the total basis weight exceeds 30 g / m 2 , powder leakage becomes difficult, seal strength and rigidity increase, and component extractability decreases.

袋体に充填する被抽出物は、粉末形状、粒形状シート状物などの固形物であれば特に制限ない。例えば、嗜好性飲料用の緑茶、烏龍茶、麦茶、紅茶、などの茶葉、レギュラーコーヒーの細挽、中細挽き、粗挽き等の粉末、鰹、いりこ、鰯、昆布、煮干などの一種又は二種以上の混合粉末などである。   The extract to be filled in the bag body is not particularly limited as long as it is a solid substance such as a powder shape or a granular sheet. For example, tea leaves such as green tea, oolong tea, barley tea, black tea, etc. for taste drinks, regular coffee fine ground, medium fine ground, coarse ground powder, etc. Such mixed powders.

以下、実施例により本発明を具体的に説明するが、本発明は、これらにより何ら限定されるものではない。尚、用いた測定方法、評価方法等は下記の通りであった。   Hereinafter, the present invention will be specifically described by way of examples. However, the present invention is not limited to these examples. The measurement method and evaluation method used were as follows.

(1)目付(g/m
縦20cm×横25cmの試料を3カ所切り取り、重量を測定し、その平均値を単位当たりの質量に換算して求める。(JIS−L−1906)
(1) Weight per unit area (g / m 2 )
A sample of 20 cm in length and 25 cm in width is cut out at three places, the weight is measured, and the average value is calculated by converting it into mass per unit. (JIS-L-1906)

(2)平均繊維径(μm)
顕微鏡で500倍の拡大写真を取り、10本の平均値で求める。
(2) Average fiber diameter (μm)
Take a 500 times magnified photograph with a microscope and obtain the average value of 10 pieces.

(3)KES曲げ剛性(gf・cm):測定装置は、カトーテック(株)社製KES・FB2−AUTO−Aを用いる。試料は、20cm×20cmであり、KES曲げ剛性を測定する。 (3) KES bending rigidity (gf · cm): As a measuring device, KES · FB2-AUTO-A manufactured by Kato Tech Co., Ltd. is used. The sample is 20 cm × 20 cm and the KES bending stiffness is measured.

(4)糸同士の接着点数
顕微鏡で試料を観察し、エンボス端部から0.3mm地点までの糸同士の融着点数を数える。1試料につきランダムでエンボスを3か所選定し、N=3の平均値を試料の糸同士の接着点数とする。倍率は適当に選択してよいが、本発明では糸同士の融着判断がし易い350倍とし、1エンボスにつき、6枚撮影した画像をつなぎ合わせて端部から0.3mm地点までの糸同士の接着点数を数えている。尚、図3、4は正面から撮影しているが、糸同士の融着が見にくい場合には少し傾けて撮影してもよい。
(4) Number of adhesion points between yarns A sample is observed with a microscope, and the number of fusion points between yarns from the embossed end to the 0.3 mm point is counted. Three embosses are selected at random for each sample, and the average value of N = 3 is defined as the number of adhesion points between the yarns of the sample. The magnification may be selected appropriately, but in the present invention, it is 350 times that makes it easy to determine the fusion between the yarns. The number of adhesion points is counted. 3 and 4 are taken from the front, but if it is difficult to see the fusion between the yarns, they may be taken slightly tilted.

(5)通気度(cm/cm/s)
JIS−L−1906フラジュール法に準拠。
(5) Air permeability (cm 3 / cm 2 / s)
Conforms to JIS-L-1906 Fraule Law.

(6)開孔径(μm)
顕微鏡で白金蒸着したサンプルの100倍の拡大写真をとり、撮影した画像を二値化することで見られる空隙の面積を計算し、全面積の2.3%の面積となるときの円相当経を算出する。
(6) Opening diameter (μm)
Take a 100x magnified photograph of the platinum-deposited sample with a microscope, calculate the area of the voids seen by binarizing the captured image, and calculate the equivalent circle when the area is 2.3% of the total area Is calculated.

(7)厚み(mm)
Mitsutoyo社製の厚み計を用いて100g荷重時の厚みを測定。
(7) Thickness (mm)
Measure thickness at 100 g load using a thickness gauge manufactured by Mitsutoyo.

(8)結晶化度(%)
示差走査熱量測定装置(DSC6000・パーキンエルマー製)にて測定を行う。測定プログラム:1)30℃で1分間保温、2)300℃まで10℃/分にて昇温。冷結晶部及び融解部の熱量を計算し、以下の式により、結晶化度を求める。
結晶量=融解部の熱量(J/g)−冷結晶部の熱量(J/g)
結晶化度(%)=結晶量(J/g)/126.4×100
(8) Crystallinity (%)
Measurement is performed with a differential scanning calorimeter (DSC6000, manufactured by PerkinElmer). Measurement program: 1) Incubate at 30 ° C for 1 minute, 2) Increase to 300 ° C at 10 ° C / min. The amount of heat in the cold crystal part and the melted part is calculated, and the crystallinity is obtained by the following equation.
Amount of crystals = calorie of melting part (J / g)-calorie of cold crystal part (J / g)
Crystallinity (%) = Crystal content (J / g) /126.4×100

(9)シール強度(N)
定長引張試験機を用い、試料幅25mm長さ200mmを切り取り、熱シール部分を約50mm上下型向に剥離し、180°剥離するように各々取り付け、つかみ間各100mm、引張速度10cm/minで、剥離強度をタテ、ヨコ各々3カ所測定し最大強度の平均値で示す。但し、シール温度120℃、時間1秒間、圧力5500kPa、シール面積7mm×25mmとする。
(9) Seal strength (N)
Using a constant-length tensile tester, cut a sample width of 25 mm and a length of 200 mm, peel off the heat seal part about 50 mm in the vertical direction, and attach each piece so as to peel 180 °. The peel strength was measured at three points each for length and width, and the average value of the maximum strengths is shown. However, the seal temperature is 120 ° C., the time is 1 second, the pressure is 5500 kPa, and the seal area is 7 mm × 25 mm.

[実施例1〜7]
第2層として、スパンボンド用の2成分紡糸口金から、芯がポリエチレンテレフタレート、鞘が芳香族ポリエステル共重合体(融点210℃)の芯鞘構造の平均繊維計14μmの複合繊維ウェブを作成し、その上に第1層として、一般的なポリエチレンテレフタレートをスパンボンド用紡糸口金から、紡糸温度300℃で平均繊径14μmの熱可塑性繊維ウェブを捕集ネット上に積層繊維ウェブとして積層し、総目付15g/mとなるよう搬送速度を調整し、任意のエンボス柄、接着面積率、ピッチ、リピート、深さのエンボスロールで、上下温度を210℃/110℃、線圧350N/cmで熱圧着して実施例1〜7の食品用フィルター材を得た。
[Examples 1-7]
As a second layer, a composite fiber web having an average fiber total of 14 μm in a core-sheath structure in which a core is polyethylene terephthalate and a sheath is an aromatic polyester copolymer (melting point 210 ° C.) is formed from a two-component spinneret for spunbond, On top of that, as a first layer, a general polyethylene terephthalate is spun from a spinneret for spunbond, a thermoplastic fiber web having an average diameter of 14 μm at a spinning temperature of 300 ° C. is laminated as a laminated fiber web on the collection net, and the total weight is obtained. Adjusting the conveyance speed to 15g / m 2 , thermocompression bonding with an embossing pattern of any embossed pattern, bonding area ratio, pitch, repeat, depth, up and down temperature of 210 ° C / 110 ° C, linear pressure of 350N / cm And the filter material for foodstuffs of Examples 1-7 was obtained.

得られたフィルター材の特性を以下の表1に示す。表1の結果から、比較例の不織布に対して、実施例1〜7の食品用フィルター材は、通気度、粉漏れ率、シール強度は維持したまま、エンボス端部から0.3mm地点までの糸同士の接着点数も増加し、曲げ剛性に優れたフィルター材であることが分かる。他方、同目付けである実施例5〜7のように、エンボスロールの深さを小さくしすぎると、厚みが減少し、糸同士の接着点数は増えているが、曲げ剛性の向上効果が若干低くなっている。つまり、図2に示すように、糸同士の接着点数増加による曲げ剛性向上の効果と、厚みの維持による曲げ剛性向上効果が複合され、飛躍的に曲げ剛性が向上する。   The characteristics of the obtained filter material are shown in Table 1 below. From the result of Table 1, the filter material for foodstuffs of Examples 1 to 7 with respect to the nonwoven fabric of the comparative example is from the embossed end to the 0.3 mm point while maintaining the air permeability, the powder leakage rate, and the seal strength. It can be seen that the number of adhesion points between the yarns is increased, and the filter material has excellent bending rigidity. On the other hand, when the depth of the embossing roll is made too small as in Examples 5-7, which are the same weight, the thickness decreases and the number of bonding points between the yarns increases, but the effect of improving the bending rigidity is slightly low. It has become. That is, as shown in FIG. 2, the bending rigidity improvement effect by increasing the number of adhesion points between yarns and the bending rigidity improvement effect by maintaining the thickness are combined, and the bending rigidity is dramatically improved.

[実施例8、9]
実施例1の繊維構成で目付を、それぞれ、10、20g/mとなるように搬送速度を変更し、実施例3のエンボスロールで同じ温度条件で熱圧着して実施例8、9の食品用フィルター材を得た。
[Examples 8 and 9]
The foods of Examples 8 and 9 were prepared by changing the conveyance speed so that the basis weight was 10 and 20 g / m 2 in the fiber configuration of Example 1, and thermocompression bonding with the embossing roll of Example 3 under the same temperature conditions. A filter material was obtained.

得られた食品用フィルター材の特性を、以下の表1に示す。以下の表1の結果から、本実施形態の食品用フィルター材は、低目付、高目付ともにエンボス端部から0.3mm地点までの糸同士の接着点数が増加し、さらには厚みも維持しており、曲げ剛性の向上効果が得られていることが分かる。   The characteristics of the obtained filter material for food are shown in Table 1 below. From the results of Table 1 below, the food filter material of the present embodiment has an increased number of bonding points between yarns from the embossed end to the 0.3 mm point for both the low weight and the high weight, and further maintains the thickness. Thus, it can be seen that the effect of improving the bending rigidity is obtained.

[実施例10、11]
実施例1の繊維構成で異なるエンボス柄、接着面積率、ピッチ、リピート、深さのエンボスロールで、上下温度を210℃/110℃、線圧350N/cmで熱圧着して実施例10、11の食品用フィルター材を得た。
[Examples 10 and 11]
Examples 10 and 11 were prepared by embossing rolls having different embossed patterns, bonding area ratios, pitches, repeats, and depths in the fiber configuration of Example 1 at a vertical temperature of 210 ° C./110° C. and a linear pressure of 350 N / cm. A filter material for food was obtained.

[実施例12]
実施例1の繊維層間に、メルトブロウン法による平均繊維径2μmのポリエチレンテレフタレートを、全重量の20wt%挿入し、目付15g/mとなるよう搬送速度を調整し、実施例3のエンボスロールで、同じ温度条件で熱圧着して実施例12の食品用フィルター材を得た。
[Example 12]
20 wt% of the total weight of polyethylene terephthalate having an average fiber diameter of 2 μm by the melt blown method was inserted between the fiber layers of Example 1, and the conveyance speed was adjusted so that the basis weight was 15 g / m 2. The food filter material of Example 12 was obtained by thermocompression bonding under the same temperature conditions.

実施例10〜12で得られた食品用フィルター材の特性を以下の表1に示す。表1の結果から、本実施形態の食品用フィルター材は、エンボスロール柄を変更してもエンボスピッチ、リピート、深さを適切に選択することで、エンボス端部から0.3mm地点までの糸同士の接着点数が増加し、さらには厚みも維持しており、曲げ剛性の向上効果が得られていることが分かる。   The characteristics of the food filter material obtained in Examples 10 to 12 are shown in Table 1 below. From the results shown in Table 1, the filter material for food according to the present embodiment is a yarn from the embossed end to the 0.3 mm point by appropriately selecting the embossed pitch, repeat, and depth even if the embossed roll pattern is changed. It can be seen that the number of adhesion points between each other increased and the thickness was also maintained, and an effect of improving the bending rigidity was obtained.

[比較例1〜7]
実施例1の繊維構成で種々目付となるよう搬送速度を変え、エンボス柄を織目柄、接着面席率14.4%、ピッチ2mm、リピートmm、深さ0.32mmのエンボスロールで、上下温度を210℃/110℃、線圧350N/cmで熱圧着して比較例1〜7の食品用フィルター材を得た。
[Comparative Examples 1-7]
The conveyance speed was changed so that various fabric weights were obtained in the fiber configuration of Example 1, the embossed pattern was a textured pattern, the bonding surface seating ratio was 14.4%, the pitch was 2 mm, the repeat mm, and the depth was 0.32 mm. The filter material for foodstuffs of Comparative Examples 1-7 was obtained by thermocompression bonding at a temperature of 210 ° C / 110 ° C and a linear pressure of 350 N / cm.

[比較例8]
実施例12の繊維構成で目付種々目付15g/mとなるよう搬送速度を調整し、比較例1〜7と同じエンボス条件で熱圧着して比較例8の食品用フィルター材を得た。
[Comparative Example 8]
The conveyance speed was adjusted so that the basis weight was 15 g / m 2 in the fiber configuration of Example 12, and thermocompression bonding was performed under the same embossing conditions as in Comparative Examples 1 to 7 to obtain a food filter material for Comparative Example 8.

比較例1〜8で得られた食品用フィルター材の特性を以下の表2に示す。表2の結果から、得られたフィルター材は、糸-糸接着点数が少なく、目付当たりの曲げ剛性(すなわち、曲げ剛性指数)が低い。   The characteristics of the food filter materials obtained in Comparative Examples 1 to 8 are shown in Table 2 below. From the results shown in Table 2, the obtained filter material has a small number of yarn-thread adhesion points, and has a low bending stiffness per unit weight (that is, a bending stiffness index).

本発明の食品用フィルター材は、粉漏れ性、熱シール加工性、シール強度、曲げ剛性などに優れているため、粉末、粒状物などの被抽出物の包装材として広い用途に用いることができる。例えば、嗜好飲料用、及び、出汁用成分抽出用フィルター材として好適に利用可能である。
特に、目付が低くても剛性が高く、製袋適正に優れるため、抽出用シートの抽出性の向上やコスト低減、さらには透明感や光沢感といった外観の美しさの向上のための低目付化に好適である。
The food filter material of the present invention is excellent in powder leakage, heat seal processability, seal strength, bending rigidity, etc., and can therefore be used in a wide range of applications as a packaging material for an extractable substance such as powder and granular materials. . For example, it can be suitably used as a filter material for extracting components for taste drinks and for soup stock.
In particular, even if the basis weight is low, the rigidity is high and the bag making is excellent, making it possible to improve the extractability of the extraction sheet, reduce the cost, and lower the basis weight to improve the beauty of the appearance such as transparency and gloss. It is suitable for.

Claims (6)

不織布を構成する熱可塑性合成繊維の平均繊維径が10〜30μmであり、総目付が10〜50g/mであり、かつ、以下の式:
曲げ剛性指数{(gf・cm)/(g/m2.5}×106={KES曲げ剛性試験機による曲げ剛性(gf・cm)/総目付(g/m2.5}×106
で求められる曲げ剛性指数が54〜206であることを特徴とする積層不織布からなる食品用フィルター材。
The average fiber diameter of the thermoplastic synthetic fiber constituting the nonwoven fabric is 10 to 30 μm, the total basis weight is 10 to 50 g / m 2 , and the following formula:
Bending stiffness index {(gf · cm) / (g / m 2 ) 2.5 } × 10 6 = {Bending stiffness (gf · cm) / total basis weight (g / m 2 ) by KES bending stiffness tester 2.5 } × 10 6
The foodstuff filter material which consists of a laminated nonwoven fabric characterized by the bending rigidity index calculated | required by 54-206 being characterized by the above-mentioned.
前記積層不織布のエンボス端部から0.3mm地点までの糸同士の接着点数が10個以上ある、請求項1に記載の食品用フィルター材。   The filter material for food according to claim 1, wherein the number of adhesion points between yarns from the embossed end of the laminated nonwoven fabric to a point of 0.3 mm is 10 or more. 前記積層不織布の厚みが0.06mm以上である、請求項1又は2に記載の食品用フィルター材。   The filter material for foodstuffs of Claim 1 or 2 whose thickness of the said laminated nonwoven fabric is 0.06 mm or more. 前記積層不織布の結晶化度が30%以上である、請求項1〜3のいずれか1項に記載の食品用フィルター材。   The filter material for foodstuffs of any one of Claims 1-3 whose crystallinity degree of the said laminated nonwoven fabric is 30% or more. 前記積層不織布が複数の層で構成され、該複数の層の内少なくとも1層が熱可塑性合成樹脂の繊維から構成される不織布層であり、他の1の層が、該少なくとも1層の熱可塑性剛性樹脂の融点より30℃〜150℃低い融点を有する熱可塑性合成樹脂の繊維から構成される不織布層である、請求項1〜4のいずれか1項に記載の食品用フィルター材。   The laminated nonwoven fabric is composed of a plurality of layers, at least one of the plurality of layers is a nonwoven fabric layer composed of thermoplastic synthetic resin fibers, and the other layer is the at least one thermoplastic layer. The filter material for foodstuffs of any one of Claims 1-4 which is a nonwoven fabric layer comprised from the fiber of a thermoplastic synthetic resin which has 30 to 150 degreeC melting | fusing point lower than melting | fusing point of rigid resin. シール強度が2〜50N/25mmである、請求項1〜5のいずれか1項に記載の食品用フィルター材。   The food filter material according to any one of claims 1 to 5, wherein the seal strength is 2 to 50 N / 25 mm.
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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2021171434A (en) * 2020-04-28 2021-11-01 大紀商事株式会社 Extraction sheet material and extraction bag
JP2022000545A (en) * 2020-06-19 2022-01-04 大紀商事株式会社 Extraction sheet material
JP2022060175A (en) * 2020-10-02 2022-04-14 大紀商事株式会社 Sheet material for extraction
JP2023013611A (en) * 2021-07-16 2023-01-26 株式会社エクスプロア Water quality and/or air quality control materials, and water quality and/or air quality control tools

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008054840A (en) * 2006-08-30 2008-03-13 Asahi Kasei Fibers Corp FILTER FILTER MATERIAL AND METHOD FOR PRODUCING FOOD-INCLOSED PAG
WO2016159266A1 (en) * 2015-04-03 2016-10-06 旭化成株式会社 Single-layer or multilayer nonwoven fabric of long polyester fibers, and filter comprising same for food

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2008054840A (en) * 2006-08-30 2008-03-13 Asahi Kasei Fibers Corp FILTER FILTER MATERIAL AND METHOD FOR PRODUCING FOOD-INCLOSED PAG
WO2016159266A1 (en) * 2015-04-03 2016-10-06 旭化成株式会社 Single-layer or multilayer nonwoven fabric of long polyester fibers, and filter comprising same for food

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2021171434A (en) * 2020-04-28 2021-11-01 大紀商事株式会社 Extraction sheet material and extraction bag
JP7174972B2 (en) 2020-04-28 2022-11-18 大紀商事株式会社 Extraction sheets and extraction bags
JP2022000545A (en) * 2020-06-19 2022-01-04 大紀商事株式会社 Extraction sheet material
JP2022060175A (en) * 2020-10-02 2022-04-14 大紀商事株式会社 Sheet material for extraction
JP7779505B2 (en) 2020-10-02 2025-12-03 大紀商事株式会社 Extraction sheet material
JP2023013611A (en) * 2021-07-16 2023-01-26 株式会社エクスプロア Water quality and/or air quality control materials, and water quality and/or air quality control tools
JP7753597B2 (en) 2021-07-16 2025-10-15 株式会社エクスプロア Water and/or air quality control materials and water and/or air quality control devices

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