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JP2018062006A - Method of estimating hardness of casting of nodular graphite cast iron - Google Patents

Method of estimating hardness of casting of nodular graphite cast iron Download PDF

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JP2018062006A
JP2018062006A JP2017185591A JP2017185591A JP2018062006A JP 2018062006 A JP2018062006 A JP 2018062006A JP 2017185591 A JP2017185591 A JP 2017185591A JP 2017185591 A JP2017185591 A JP 2017185591A JP 2018062006 A JP2018062006 A JP 2018062006A
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cooling rate
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義弘 中道
Yoshihiro Nakamichi
義弘 中道
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Abstract

PROBLEM TO BE SOLVED: To provide a method of accurately estimating a hardness of a casting of nodular graphite cast iron by simulation.SOLUTION: A method of estimating a hardness of a casting of nodular graphite cast iron comprises an element creating step (S1) that creates an analytic model, a cooling history analysis step (S2) that chronologically analyzes a heat transmission in a casting element during a period from when a molten metal flows a casting element to be filled until when it is cooled and obtains a set of data of time and temperature of the casting element, a chemical composition value setting step (S3), a temperature setting step (S4) that gives a preset temperature for calculating a cooling rate, a maximum temperature calculation step (S5) that determines a maximum temperature of the casting element, a cooling rate calculation step (S6) that includes a process of calculating a cooling rate of eutectic solidification, a cooling rate after eutectic solidification and a cooling rate of eutectoid transformation on the basis of the preset temperature and the set of data, and a hardness calculation step (S7) that calculates a hardness of the casting element by a hardness estimation formula on the basis of the maximum temperature, the cooling rate of eutectic solidification, the cooling rate after eutectic solidification, the cooling rate of eutectoid transformation and chemical composition values.SELECTED DRAWING: Figure 1

Description

本発明は、球状黒鉛鋳鉄鋳物の硬度を予測する方法に関するものである。   The present invention relates to a method for predicting the hardness of a spheroidal graphite cast iron casting.

金属材料の強度その他の機械的特性は、硬度と強い相関があることが知られている。自動車向けの構造用部材として多用される球状黒鉛鋳鉄鋳物の硬度をシミュレーションによって予測する方法に関しては、例えば特許文献1に、解析モデルの鋳物要素における共晶凝固開始付近の冷却速度と鋳物の硬度とが比例関係にあることが記載されており、冷却速度を解析で求めることによって硬度を予測することが可能であることが示唆されている。   It is known that the strength and other mechanical properties of a metal material have a strong correlation with hardness. Regarding the method of predicting the hardness of spheroidal graphite cast iron castings frequently used as structural members for automobiles by simulation, for example, Patent Document 1 describes the cooling rate near the start of eutectic solidification in the casting element of the analytical model, the hardness of the casting, Are proportional to each other, suggesting that the hardness can be predicted by obtaining the cooling rate by analysis.

特開2008−155230号公報JP 2008-155230 A

球状黒鉛鋳鉄鋳物の各部位の硬度を精度よく予測できれば、引張強さや耐力、伸びなどの自動車部品として必要な機械的特性を、実際の鋳造を行わずに精度よく予測することが可能となって、試作工数の削減による開発期間の短縮などが期待できる。しかし、特許文献1に記載のような、ある一つの温度範囲の冷却速度のみをシミュレーションで求めて硬度を予測する方法では、精度が不十分であることがわかった。   If the hardness of each part of the spheroidal graphite cast iron casting can be accurately predicted, it is possible to accurately predict the mechanical properties necessary for automobile parts such as tensile strength, proof stress, and elongation without performing actual casting. The development period can be shortened by reducing the number of prototypes. However, it has been found that the accuracy as described in Patent Document 1 is insufficient in the method of predicting the hardness by calculating only the cooling rate in a certain temperature range by simulation.

このため、本発明は球状黒鉛鋳鉄鋳物の硬度をシミュレーションにより精度よく予測する方法を提供することを目的としている。   Therefore, an object of the present invention is to provide a method for accurately predicting the hardness of a spheroidal graphite cast iron casting by simulation.

本発明者は実際に測定した球状黒鉛鋳鉄鋳物の硬度と、硬度を測定した部位の近傍で実測した凝固冷却温度曲線及び化学成分値との関係を丹念に調べたところ、球状黒鉛鋳鉄鋳物の硬度は共晶凝固付近の冷却速度以外の冷却速度や黒鉛粒数、化学成分値などにも強い相関があることを見出し、本発明に想到した。なお、本発明において、共晶凝固付近の冷却速度を「共晶凝固の冷却速度」と、共析変態温度付近の冷却速度を「共析変態の冷却速度」ということがある。   The inventor carefully examined the relationship between the hardness of the spheroidal graphite cast iron casting actually measured and the solidification cooling temperature curve and chemical component value measured in the vicinity of the portion where the hardness was measured. Has found that there is a strong correlation with the cooling rate other than the cooling rate in the vicinity of eutectic solidification, the number of graphite grains, the chemical component value, and the like, and has reached the present invention. In the present invention, the cooling rate near eutectic solidification may be referred to as “eutectic solidification cooling rate” and the cooling rate near eutectoid transformation temperature may be referred to as “eutectoid transformation cooling rate”.

すなわち本発明は、球状黒鉛鋳鉄鋳物の硬度を予測する方法であって、
鋳物要素を含む解析モデルを作成する要素作成工程(S1)と、
球状黒鉛鋳鉄からなる溶湯が前記鋳物要素を流動し充填されて前記球状黒鉛鋳鉄の共析変態温度よりも低い温度に冷却されるまでの期間の前記鋳物要素の伝熱を経時的に解析して、前記鋳物要素の時刻と温度との組データを取得する冷却履歴解析工程(S2)と、
前記球状黒鉛鋳鉄の化学成分値を与える化学成分値設定工程(S3)と、
前記鋳物要素の冷却速度を計算するための設定温度を与える温度設定工程(S4)と、
前記鋳物要素の組データに基づいて前記鋳物要素の最高温度を求める最高温度計算工程(S5)と、
前記設定温度と前記組データとに基づいて、共晶凝固の冷却速度を計算する第1の冷却速度計算工程(S61)、共晶凝固後の冷却速度を計算する第2の冷却速度計算工程(S62)及び共析変態の冷却速度を計算する第3の冷却速度計算工程(S63)を含む冷却速度計算工程(S6)と、
前記最高温度、前記共晶凝固の冷却速度、前記共晶凝固後の冷却速度、前記共析変態の冷却速度及び前記化学成分値に基づいて、硬度予測式により前記鋳物要素の硬度を計算する硬度計算工程(S7)と
を有する球状黒鉛鋳鉄鋳物の硬度を予測する方法である。
That is, the present invention is a method for predicting the hardness of a spheroidal graphite cast iron casting,
An element creation step (S1) for creating an analysis model including a casting element;
Analyzing the heat transfer of the casting element over time during the period from when the molten metal made of spheroidal graphite cast iron flows and fills the casting element and is cooled to a temperature lower than the eutectoid transformation temperature of the spheroidal graphite cast iron. , A cooling history analysis step (S2) for acquiring set data of time and temperature of the casting element;
A chemical component value setting step (S3) for giving a chemical component value of the spheroidal graphite cast iron;
A temperature setting step (S4) for providing a set temperature for calculating the cooling rate of the casting element;
A maximum temperature calculation step (S5) for obtaining a maximum temperature of the casting element based on the set data of the casting element;
Based on the set temperature and the set data, a first cooling rate calculation step (S61) for calculating a cooling rate for eutectic solidification, and a second cooling rate calculation step for calculating a cooling rate after eutectic solidification ( A cooling rate calculation step (S6) including S62) and a third cooling rate calculation step (S63) for calculating the cooling rate of the eutectoid transformation;
Based on the maximum temperature, the cooling rate of the eutectic solidification, the cooling rate after the eutectic solidification, the cooling rate of the eutectoid transformation, and the chemical component value This is a method for predicting the hardness of a spheroidal graphite cast iron casting having a calculation step (S7).

本発明において、前記化学成分値設定工程(S3)で与える化学成分値は元素として少なくともC、Si、Cu及びMnを含むことが好ましい。   In the present invention, the chemical component value given in the chemical component value setting step (S3) preferably includes at least C, Si, Cu and Mn as elements.

また、本発明において、前記硬度計算工程(S7)は、前記最高温度、前記共晶凝固の冷却速度及び少なくとも元素としてCとSiを含む化学成分値に基づいて前記鋳物要素の黒鉛粒数を計算する黒鉛粒数計算工程(S71)を含むことが好ましい。   In the present invention, the hardness calculation step (S7) calculates the number of graphite grains of the casting element based on the maximum temperature, the cooling rate of the eutectic solidification, and the chemical component value including at least C and Si as elements. It is preferable to include a graphite particle number calculating step (S71).

また、本発明において、前記硬度計算工程(S7)は、前記共析変態の冷却速度と前記共晶凝固後の冷却速度との相対値の計算を含むのが好ましい。   In the present invention, the hardness calculation step (S7) preferably includes calculation of a relative value between the cooling rate of the eutectoid transformation and the cooling rate after eutectic solidification.

さらに本発明は、前記硬度計算工程(S7)で計算される鋳物要素の硬度を画像として出力する硬度出力工程(S8)を有するのが好ましい。   Furthermore, the present invention preferably includes a hardness output step (S8) for outputting the hardness of the casting element calculated in the hardness calculation step (S7) as an image.

本発明により、球状黒鉛鋳鉄鋳物の各部位の硬度をシミュレーションによって精度よく予測する方法が提供される。これにより球状黒鉛鋳鉄鋳物の引張強さや耐力など、特に自動車用鋳物部品として設計するために必要となる機械的特性を、実際の鋳造を行わずに精度よく予測することができるようになり、試作工数の削減による開発期間の短縮などを図ることが可能となる。   The present invention provides a method for accurately predicting the hardness of each part of a spheroidal graphite cast iron casting by simulation. This makes it possible to accurately predict the mechanical properties necessary for designing cast parts for automobiles, such as the tensile strength and proof stress of spheroidal graphite cast iron castings, without performing actual casting. It becomes possible to shorten the development period by reducing man-hours.

本発明の全体構成を示す流れ図である。It is a flowchart which shows the whole structure of this invention. 本発明を構成する冷却履歴解析工程(S2)を示す流れ図である。It is a flowchart which shows the cooling history analysis process (S2) which comprises this invention. 本発明を構成する冷却速度計算工程(S6)を示す流れ図である。It is a flowchart which shows the cooling rate calculation process (S6) which comprises this invention. 本発明を構成する冷却速度計算工程(S6)の構成要素の一つである第1の冷却速度計算工程(S61)を示す流れ図である。It is a flowchart which shows the 1st cooling rate calculation process (S61) which is one of the components of the cooling rate calculation process (S6) which comprises this invention. 本発明を構成する硬度計算工程(S7)を示す流れ図である。It is a flowchart which shows the hardness calculation process (S7) which comprises this invention. 本発明の実施例による硬度の予測値と実物の硬度の実測値とを比較する図である。It is a figure which compares the predicted value of the hardness by the Example of this invention, and the actual value of the hardness of a real thing. 球状黒鉛鋳鉄の冷却履歴を示す凝固冷却曲線の模式図である。It is a schematic diagram of the solidification cooling curve which shows the cooling history of spheroidal graphite cast iron. 球状黒鉛鋳鉄鋳物の冷却速度とブリネル硬度との関係を実測した例であって、(a)は共析変態温度付近の冷却速度とブリネル硬度との関係、(b)は共析変態温度付近の冷却速度と共晶凝固後の冷却速度との比とブリネル硬度との関係を示す図である。It is the example which measured the relationship between the cooling rate of a spheroidal graphite cast iron casting, and Brinell hardness, (a) is the relationship between the cooling rate near eutectoid transformation temperature and Brinell hardness, (b) is the eutectoid transformation temperature neighborhood. It is a figure which shows the relationship between ratio of a cooling rate and the cooling rate after eutectic solidification, and Brinell hardness. 球状黒鉛鋳鉄鋳物の黒鉛粒数とブリネル硬度との関係を実測した例を示す図である。It is a figure which shows the example which measured the relationship between the graphite particle number of a spheroidal graphite cast iron casting, and Brinell hardness. 球状黒鉛鋳鉄鋳物の鋳型内に注湯された溶湯の段階での最高到達温度と黒鉛粒数との関係を実測した例を示す図である。It is a figure which shows the example which measured the relationship between the highest attained temperature in the stage of the molten metal poured in the casting mold of the spheroidal graphite cast iron, and the number of graphite grains. 球状黒鉛鋳鉄鋳物の共晶凝固温度付近の冷却速度と黒鉛粒数との関係を実測した例を示す図である。It is a figure which shows the example which measured the relationship between the cooling rate of the eutectic solidification temperature vicinity of a spheroidal graphite cast iron casting, and the number of graphite grains. 共析変態の冷却速度のみを考慮した比較例による硬度の予測値と実物の硬度の実測値とを比較する図である。It is a figure which compares the predicted value of the hardness by the comparative example which considered only the cooling rate of eutectoid transformation, and the actual value of the hardness of a real thing.

前述のように、本発明者は実際の球状黒鉛鋳鉄鋳物(以下、鋳物ともいう。)の各部位の硬度と、その部位における実測した凝固冷却温度曲線及び化学成分値との関係を丹念に調べた。その結果、硬度はその部位の冷却履歴、化学成分値及び黒鉛粒数との関数であり、冷却履歴の代表値である冷却速度と化学成分値に基づく成分パラメータを適切に設定することにより、実験データから精度のよい硬度予測式と黒鉛粒数予測式を作ることができることがわかった。そしてこの知見から、CAE(Computer−aided Engineering)を用いたシミュレーションによって得られる鋳物要素の冷却履歴と、化学成分値と、実験データに基づいて予め作成した硬度予測式及び黒鉛粒数予測式とを用いることにより、鋳物の各部位の硬度を精度よく予測する方法に想到した。   As described above, the present inventor has carefully studied the relationship between the hardness of each part of an actual spheroidal graphite cast iron casting (hereinafter also referred to as a casting) and the measured solidification cooling temperature curve and chemical component value at that part. It was. As a result, the hardness is a function of the cooling history, chemical component value, and number of graphite grains of the part, and by setting the component parameters based on the cooling rate and the chemical component value, which are representative values of the cooling history, the experiment was performed. From the data, it was found that the hardness prediction formula and the graphite grain number prediction formula can be made with high accuracy. And from this knowledge, the cooling history of the casting element obtained by the simulation using CAE (Computer-aided Engineering), the chemical component value, the hardness prediction formula and the graphite grain number prediction formula created in advance based on the experimental data. As a result, the inventors have come up with a method for accurately predicting the hardness of each part of the casting.

本発明は球状黒鉛鋳鉄鋳物の硬度を予測する方法であって、鋳物要素を含む解析モデルを作成する要素作成工程(S1)と、球状黒鉛鋳鉄からなる溶湯が前記鋳物要素を流動し充填されて前記球状黒鉛鋳鉄の共析変態温度よりも低い温度に冷却されるまでの期間の前記鋳物要素の伝熱を経時的に解析して、前記鋳物要素の時刻と温度との組データを取得する冷却履歴解析工程(S2)と、前記球状黒鉛鋳鉄の化学成分値を与える化学成分値設定工程(S3)と、前記鋳物要素の冷却速度を計算するための設定温度を与える温度設定工程(S4)と、前記鋳物要素の組データに基づいて前記鋳物要素の最高温度を求める最高温度計算工程(S5)と、前記設定温度と前記組データとに基づいて、共晶凝固の冷却速度を計算する第1の冷却速度計算工程(S61)、共晶凝固後の冷却速度を計算する第2の冷却速度計算工程(S62)及び共析変態の冷却速度を計算する第3の冷却速度計算工程(S63)を含む冷却速度計算工程(S6)と、前記最高温度、前記共晶凝固の冷却速度、前記共晶凝固後の冷却速度、前記共析変態の冷却速度及び前記化学成分値に基づいて、硬度予測式により前記鋳物要素の硬度を計算する硬度計算工程(S7)とを有する。以下、本発明の詳細を図面を参照しつつ説明するが、これに限定されない。   The present invention is a method for predicting the hardness of a spheroidal graphite cast iron casting, wherein an element creating step (S1) for creating an analysis model including a cast element, and a molten metal made of spheroidal graphite cast iron flows and fills the cast element. Cooling that analyzes the heat transfer of the casting element over time until it is cooled to a temperature lower than the eutectoid transformation temperature of the spheroidal graphite cast iron, and obtains time and temperature set data of the casting element A history analysis step (S2), a chemical component value setting step (S3) for giving a chemical component value of the spheroidal graphite cast iron, and a temperature setting step (S4) for giving a set temperature for calculating the cooling rate of the casting element A first temperature calculating step (S5) for obtaining a maximum temperature of the casting element based on the set data of the casting element, and a first rate of calculating a cooling rate for eutectic solidification based on the set temperature and the set data. Cooling rate meter Cooling rate calculation including a step (S61), a second cooling rate calculation step (S62) for calculating the cooling rate after eutectic solidification, and a third cooling rate calculation step (S63) for calculating the cooling rate of the eutectoid transformation Based on the step (S6), the maximum temperature, the cooling rate of the eutectic solidification, the cooling rate after the eutectic solidification, the cooling rate of the eutectoid transformation, and the chemical component value, the casting element according to the hardness prediction formula And a hardness calculation step (S7) for calculating the hardness. Hereinafter, although the detail of this invention is demonstrated, referring drawings, it is not limited to this.

図1は本発明の全体構成を示す流れ図である。本発明は要素作成工程S1、冷却履歴解析工程S2、化学成分設定工程S3、温度設定工程S4、最高温度計算工程S5、冷却速度計算工程S6、硬度計算工程S7を有する。本発明は、さらに硬度出力工程S8を有してもよい。硬度予測の手順については要素作成工程S1から順を追って後述するが、先に硬度計算工程S7で用いる硬度予測式について詳細を説明する。   FIG. 1 is a flowchart showing the overall configuration of the present invention. The present invention includes an element creation step S1, a cooling history analysis step S2, a chemical component setting step S3, a temperature setting step S4, a maximum temperature calculation step S5, a cooling rate calculation step S6, and a hardness calculation step S7. The present invention may further include a hardness output step S8. The procedure of hardness prediction will be described later in order from the element creation step S1, but the details of the hardness prediction formula used in the hardness calculation step S7 will be described first.

(1)硬度予測式と黒鉛粒数予測式
本発明者は実際の鋳物の硬度と、その部位において実測した凝固冷却曲線及び化学成分値との関係を丹念に調べて、以下のような相関があることを見出した。
(1) Hardness Prediction Formula and Graphite Grain Number Prediction Formula The inventor carefully examined the relationship between the actual casting hardness, the solidification cooling curve and the chemical component value measured at the site, and the following correlation was found. I found out.

図7は球状黒鉛鋳鉄鋳物の冷却履歴を示す凝固冷却曲線1の模式図である。凝固冷却曲線1において時刻tに伴う温度Tの推移をみると、鋳型に注湯された球状黒鉛鋳鉄の溶湯は、最高到達温度Tmaxから時間の経過に伴って鋳型に抜熱されて温度が降下していくが、その過程で共晶凝固温度Tで黒鉛を晶出しながら凝固し、共析変態温度TA1では組織中へのパーライト相の析出を伴う。この共晶凝固温度T付近と共析変態温度TA1付近では潜熱を放出するために温度降下が緩やかになる。冷却速度とはある温度区間をそれに要した時間で除した値で一般に定義されるものであるが、凝固冷却曲線1に示すように、冷却速度は温度区間によって異なる。このため、本発明者は実験データを解析し、硬度と強い相関を示す冷却速度が得られる温度区間を調べた。 FIG. 7 is a schematic diagram of the solidification cooling curve 1 showing the cooling history of the spheroidal graphite cast iron casting. Looking at the transition of the temperature T with time t in the solidification cooling curve 1, the molten spheroidal graphite cast iron poured into the mold is extracted from the maximum temperature T max as the time elapses and the temperature rises. In the process, it solidifies while crystallization of graphite at the eutectic solidification temperature T E , and the eutectoid transformation temperature T A1 is accompanied by precipitation of a pearlite phase in the structure. In the vicinity of the eutectic solidification temperature T E and in the vicinity of the eutectoid transformation temperature T A1 , since the latent heat is released, the temperature drop becomes gentle. The cooling rate is generally defined by a value obtained by dividing a certain temperature section by the time required for it, but as shown in the solidification cooling curve 1, the cooling rate varies depending on the temperature section. For this reason, the present inventor analyzed the experimental data and examined the temperature interval in which the cooling rate showing a strong correlation with the hardness was obtained.

図8は球状黒鉛鋳鉄鋳物の冷却速度とブリネル硬度との関係を実測した例である。図8(a)は、共析変態温度TA1付近の冷却速度とブリネル硬度H(以下、硬度ともいう。)との関係である。この例では、硬度の測定部位近傍における共析変態温度TA1付近の740℃から710℃の温度区間の冷却速度V740−710が増加するに伴って硬度Hも増加していく強い相関がみられた。本発明者は、球状黒鉛鋳鉄鋳物の硬度は、その組織中へのパーライト相の析出を伴う共析変態温度付近の冷却速度の影響を強く受けるものと推察していたが、図8(a)に示すようにその推察が妥当であることが確認された。 FIG. 8 shows an example in which the relationship between the cooling rate of the spheroidal graphite cast iron casting and the Brinell hardness is measured. FIG. 8A shows the relationship between the cooling rate near the eutectoid transformation temperature T A1 and the Brinell hardness H B (hereinafter also referred to as hardness). In this example, there is a strong correlation in which the hardness H B increases as the cooling rate V 740-710 in the temperature range from 740 ° C. to 710 ° C. near the eutectoid transformation temperature T A1 near the hardness measurement site increases. It was seen. The present inventor presumed that the hardness of the spheroidal graphite cast iron casting was strongly influenced by the cooling rate in the vicinity of the eutectoid transformation temperature accompanied by the precipitation of the pearlite phase in the structure. It was confirmed that the inference was valid as shown in.

また、図8(b)は、図7で示す共析変態温度TA1付近の冷却速度V740−710と共晶凝固後の1100℃から1000℃の温度区間の冷却速度V1100−1000との相対的な値である比V740−710/V1100−1000と硬度との関係を実測した例である。この例では、V740−710/V1100−1000が増加するに伴って硬度Hは減少していく関係がみられたが、この相関は特に鋳物の薄肉部分について強いことがわかった。このように、共析変態温度付近の冷却速度だけでなく、共晶凝固後の冷却速度も硬度に大きく影響することがわかった。 Further, FIG. 8 (b), the cooling rate V 1100-1000 of eutectoid transformation temperature T A1 near the cooling rate V 740-710 and the temperature zone of 1000 ° C. from 1100 ° C. after eutectic solidification shown in Figure 7 This is an example in which the relationship between the relative value ratio V 740-710 / V 1100-1000 and hardness is measured. In this example, it was found that the hardness H B decreased as V 740-710 / V 1100-1000 increased, but this correlation was found to be particularly strong for the thin portion of the casting. Thus, it was found that not only the cooling rate near the eutectoid transformation temperature but also the cooling rate after eutectic solidification greatly affects the hardness.

また、図9は鋳物の黒鉛粒数と硬度との関係を実測した例を示す図である。黒鉛粒数Nが多くなると硬度Hも増加する傾向がみられ、鋳物の硬度は上記のような冷却速度だけでなく黒鉛粒数にも相関があることがわかった。また図10は、鋳型内における溶湯の段階での最高到達温度Tmax(以下、最高温度ともいう。)と黒鉛粒数との関係を実測した例を示す図である。すなわち図7で示す最高温度Tmaxが大きくなると黒鉛粒数Nが減少する傾向が顕著にみられたことから、黒鉛粒数は最高温度と相関が強いことがわかった。さらに、図11は共晶凝固温度付近の冷却速度と黒鉛粒数との関係を実測した例を示す図である。図7に示す共晶凝固温度T付近の1160℃から1100℃の区間の冷却速度V1160−1100が増加するに伴って黒鉛粒数Nも増加する傾向が強いことがわかった。以上のように、硬度は黒鉛粒数にも相関があり、さらに黒鉛粒数は最高温度と共晶凝固温度付近の冷却速度と強い相関を持つことも見出した。 Moreover, FIG. 9 is a figure which shows the example which measured the relationship between the graphite particle number of a casting, and hardness. As the number of graphite grains NG increases, the hardness H B tends to increase, and it has been found that the hardness of the casting has a correlation not only with the cooling rate as described above but also with the number of graphite grains. FIG. 10 is a diagram showing an example in which the relationship between the maximum temperature T max (hereinafter also referred to as the maximum temperature) at the stage of the molten metal in the mold and the number of graphite grains is actually measured. That is, the tendency for the number of graphite grains NG to decrease as the maximum temperature T max shown in FIG. 7 increases was found to be significant, indicating that the number of graphite grains has a strong correlation with the maximum temperature. Further, FIG. 11 is a diagram showing an example in which the relationship between the cooling rate near the eutectic solidification temperature and the number of graphite grains is measured. The number of graphite grains N G with the eutectic solidification temperature T E cooling rate V 1160-1100 from 1160 ° C. interval of 1100 ° C. vicinity shown in FIG. 7 increases also found that a strong tendency to increase. As described above, the hardness was also correlated with the number of graphite grains, and the number of graphite grains was also found to have a strong correlation with the maximum temperature and the cooling rate near the eutectic solidification temperature.

そして鋳物の硬度及び黒鉛粒数は含有する化学成分値によっても影響される。例えば、CuとMnは、硬度の高いパーライト相の析出を促進させるので鋳物の硬度を高める成分元素であることが知られている。また、CとSiは黒鉛の晶出を促進する成分元素であることも知られている。したがって、特にこれらの元素の化学成分値に基づく成分パラメータも変数として考慮することが好ましい。   And the hardness of a casting and the number of graphite grains are influenced also by the chemical component value to contain. For example, Cu and Mn are known to be component elements that increase the hardness of a casting because they promote the precipitation of a pearlite phase having a high hardness. It is also known that C and Si are component elements that promote crystallization of graphite. Therefore, it is preferable to consider the component parameters based on the chemical component values of these elements as variables.

以上の知見により、球状黒鉛鋳鉄鋳物の硬度予測式は、これらの複数の冷却速度、黒鉛粒数及び化学成分値を変数とする関数Fとして、概念的に次のように表すことができる。
=F(E,N,V,V) (式1)
ここで、H:硬度
:化学成分値に基づく第1の変数
:黒鉛粒数
:共晶凝固後の冷却速度
:共析変態の冷却速度
である。
Based on the above knowledge, the hardness prediction formula of the spheroidal graphite cast iron casting can be conceptually expressed as the following function F 1 using the plurality of cooling rates, the number of graphite grains, and the chemical component value as variables.
H B = F 1 (E 1 , N G , V 2 , V 3 ) (Formula 1)
Where H B : Hardness
E 1 : First variable based on chemical component values
N G : Number of graphite grains
V 2 : Cooling rate after eutectic solidification
V 3 is the cooling rate of the eutectoid transformation.

ところで、黒鉛粒数Nについてはその予測式を関数Fとして、概念的に次のように表すことができる。
=F(E,V,Tmax) (式2)
ここで、E:化学成分値に基づく第2の変数
:共晶凝固の冷却速度
max:最高温度
である。
Incidentally, for the number of graphite grains N G the prediction equation as a function F 2, it can be conceptually represented as follows.
N G = F 2 (E 2 , V 1 , T max ) (Formula 2)
Where E 2 : second variable based on chemical component value
V 1 : Cooling rate of eutectic solidification
T max : Maximum temperature.

なお、上記のように関数Fで表される黒鉛粒数Nは、関数Fの変数にもなっているので、硬度Hは、化学成分値に基づく第1の変数E及び第2の変数E、最高温度Tmax、共晶凝固の冷却速度V、共晶凝固後の冷却速度V及び共析変態の冷却速度Vを変数とする関数Fとして一括して次のように表記することも可能である。
=F(E,E,Tmax,V,V,V) (式3)
Since the number of graphite grains NG represented by the function F 2 is also a variable of the function F 1 as described above, the hardness H B is determined by the first variable E 1 and the first variable based on the chemical component value. Next, the function F 1 having the variables E 2 , the maximum temperature T max , the cooling rate V 1 of eutectic solidification, the cooling rate V 2 after eutectic solidification, and the cooling rate V 3 of eutectoid transformation as a variable It is also possible to express as follows.
H B = F 1 (E 1 , E 2 , T max , V 1 , V 2 , V 3 ) (Formula 3)

上記の(式1)〜(式3)は概念的な表記であるが、実際の鋳物についての化学成分値、硬度測定部位近傍の冷却履歴(凝固冷却曲線)、硬度及び黒鉛粒数の実測データを十分に採取し、上記の各変数について、例えば重回帰分析などの回帰分析や試行錯誤的な反復計算などの解析を行うことにより、具体的な関数F及び関数Fの式を作成することが可能である。 The above (Formula 1) to (Formula 3) are conceptual notations, but actual measurement data of chemical component values, cooling history (solidification cooling curve) in the vicinity of the hardness measurement site, hardness, and number of graphite grains for actual castings. Are collected, and a specific expression of the function F 1 and the function F 2 is created by performing regression analysis such as multiple regression analysis or trial and error iterative calculation for each of the above variables. It is possible.

本発明者は図8〜図11に示したような実験データを十分に採取し、解析を行うことにより、以下に示す精度の高い関数形を有する硬度予測式(式4)及び黒鉛粒数予測式(式5)を作成した。但し本発明の硬度予測式及び黒鉛粒数予測式はこの関数形に限定されない。なお、硬度予測式(式4)のNの項は、必ずしも黒鉛粒数予測式(式5)により求まるNの値でなくてもよく、一定値として黒鉛粒数Nを設定してもよい。

=F(Cueq,N,V,V
=ω+αCueq+α+α+α/V (式4)

=F(DCE,V,Tmax
=ψ+DCE(β−ψ)+β+βmax (式5)
The inventor sufficiently collects experimental data as shown in FIG. 8 to FIG. 11 and performs analysis to thereby obtain a hardness prediction formula (formula 4) and a graphite particle number prediction having a highly accurate function form shown below. Formula (Formula 5) was created. However, the hardness prediction formula and the graphite grain number prediction formula of the present invention are not limited to this function form. Note that the NG term in the hardness prediction formula (Formula 4) does not necessarily have to be the value of NG determined by the graphite grain number prediction formula (Formula 5), and the graphite grain number NG is set as a constant value. Also good.

H B = F 1 (Cu eq , NG , V 2 , V 3 )
= Ω + α 1 Cu eq + α 2 V 3 + α 3 NG + α 4 V 3 / V 2 (Formula 4)

N G = F 2 (D CE , V 1 , T max )
= Ψ 1 + D CE1 V 1 −ψ 2 ) + β 2 V 1 + β 3 T max (Formula 5)

ここで、(式4)のCueqはここではCu当量と称する成分パラメータであって、化学成分値に基づく第1の変数Eに相当し、Cueq=Cu%+ξMn%としている。ここでCu%はCuの、Mn%はMnの質量%を示す。また、ξはMnの寄与度を示す定数である。 Here, Cu eq in (Equation 4) is a component parameter referred to herein as Cu equivalent, which corresponds to the first variable E 1 based on the chemical component value, and is set to Cu eq = Cu% + ξ 2 Mn%. Here, Cu% represents Cu, and Mn% represents mass% of Mn. Ξ 2 is a constant indicating the contribution of Mn.

また、(式4)のV/Vの項、すなわち共析変態の冷却速度Vと共晶凝固後の冷却速度Vとの比は、図8(b)に例示したような結果に基づくものである。前述したように、特に薄肉部の硬度の予測精度を高めることができるので、V/Vはこれを求める工程として関数Fに組み込んでおくことが好ましい。なお、(式4)の例ではV/Vとしているが、VとVとの相対的な関係の指標であるので、逆数V/Vを用いてもよい。なお、(式4)のV/Vの項は必須ではなく、この項を除く、またはV/Vに替えて共晶凝固後の冷却速度Vのみをαとして組み込んでもよい。 Further, the term of V 3 / V 2 in (Equation 4), that is, the ratio of the cooling rate V 3 of the eutectoid transformation and the cooling rate V 2 after eutectic solidification is the result as illustrated in FIG. 8B. It is based on. As described above, since the accuracy of predicting the hardness of the thin-walled portion can be particularly improved, V 3 / V 2 is preferably incorporated in the function F 1 as a process for obtaining this. In the example of (Equation 4), V 3 / V 2 is used, but since it is an indicator of the relative relationship between V 2 and V 3 , the reciprocal number V 2 / V 3 may be used. Note that the term V 3 / V 2 in (Equation 4) is not essential, and this term is excluded, or only the cooling rate V 2 after eutectic solidification is incorporated as α 4 V 2 instead of V 3 / V 2. But you can.

また、DCEはここでは過共晶度と称し、球状黒鉛鋳鉄の共晶組成からの過共晶側への偏差を示す成分パラメータであって、化学成分値に基づく第2の変数Eに相当する、過共晶度DCEは、DCE=Ceq−φ=C%+ξSi%−φとしている。ここでCeqは一般にはCE値と称される炭素当量であり、ξはSiの寄与度を示す定数であって、ξ=1/3(0.33)が広く用いられている。なお、C%はCの、Si%はSiの質量%を示す。また定数φは炭素当量Ceqでみたときの共晶組成に相当する値で、一般にはφ=4.5とされている。 DCE is referred to herein as the hypereutectic degree, and is a component parameter indicating a deviation from the eutectic composition of the spheroidal graphite cast iron to the hypereutectic side, and is a second variable E 2 based on the chemical component value. The corresponding hypereutectic degree D CE is set to D CE = C eq −φ = C% + ξ 1 Si% −φ. Here, C eq is a carbon equivalent generally referred to as a CE value, ξ 1 is a constant indicating the contribution of Si, and ξ 1 = 1/3 (0.33) is widely used. C% indicates C and Si% indicates mass% of Si. The constant φ is a value corresponding to the eutectic composition when viewed in terms of carbon equivalent C eq , and generally φ = 4.5.

また、ω、α〜α、β〜β及びψ〜ψは定数であって、硬度や黒鉛粒数に対する上記の各変数の重み(寄与度)を与えるものである。これらの定数は、鋳物の製造条件等で最適な値が異なる場合が多い。したがってこれらの定数は、硬度を予測しようとする対象の鋳物を製造する製造ラインや鋳物工場、あるいは製造する製品毎に、実測データを十分に採取し解析を適切に行うことによって、できるだけ確からしい値を求めておくことが好ましい。 Further, ω, α 1 to α 4 , β 1 to β 3, and ψ 1 to ψ 2 are constants, and give weights (contributions) of the above variables to the hardness and the number of graphite grains. These constants often have different optimum values depending on the casting production conditions. Therefore, these constants are as probable as possible by sufficiently collecting actual measurement data and conducting appropriate analysis for each production line, foundry factory, or product to be manufactured for which the hardness is to be predicted. Is preferably obtained.

以上のような方法によって、精度の高い硬度予測式を作成することができる。以下、本発明の工程について、図面を参照しつつ順に説明する。   A highly accurate hardness prediction formula can be created by the above method. Hereinafter, the steps of the present invention will be described in order with reference to the drawings.

(2)要素作成工程(S1)
要素作成工程S1は解析モデルを作成する工程である。この工程では、製品となる鋳物の形状データを3次元CADデータとして作成し、または予め作製された形状データを取り込んで、また、鋳造に必要な湯口、湯道、押湯、堰などの鋳造方案部の形状データ、さらに鋳物の周囲に鋳型の形状データを作成し、これらの各形状データを多面体からなる複数の微小要素(以下、要素ともいう。)に分割した後、これらの要素を鋳物または鋳型と定義し、硬度予測の対象とするn個の鋳物要素及び硬度予測の対象としない鋳物要素並びに鋳型要素を含む解析モデルを作成する。
(2) Element creation process (S1)
Element creation step S1 is a step of creating an analysis model. In this process, the shape data of the casting that is the product is created as three-dimensional CAD data, or the shape data prepared in advance is taken in, and the casting plan for the gate, runner, feeder, weir, etc. necessary for casting The shape data of the part and the shape data of the mold around the casting are created, and each of these shape data is divided into a plurality of microelements (hereinafter also referred to as elements) made of a polyhedron, and then these elements are cast or An analysis model is defined that includes n casting elements to be hardness-predicted, casting elements that are not to be hardness-predicted, and mold elements.

複数の要素の作成には、部位毎に要素に分割する位置を座標として与える方法や、所望の要素の大きさを与えれば自動で要素を生成する要素作成プログラムなどを用いてもよい。また鋳型要素の作成では、鋳物の形状データのみから鋳型の厚さを定義した簡易的な鋳型要素を鋳物要素の周囲に配してもよい。   To create a plurality of elements, a method of giving the position where the element is divided for each part as coordinates, an element creation program for automatically generating elements if a desired element size is given, or the like may be used. In creating the mold element, a simple mold element in which the thickness of the mold is defined only from the shape data of the casting may be arranged around the casting element.

予め作成された鋳物の形状を取り込むための3次元CADデータの形式は、様々な形式を用いることができる。例えば、国際規格IGES(Initial Graphics Exchange Specification)形式やSTL(Stereo Lithography)形式などを利用できる。   Various formats can be used as the format of the three-dimensional CAD data for taking in the shape of the casting created in advance. For example, an international standard IGES (Initial Graphics Exchange Specification) format, STL (Stereo Lithography) format, or the like can be used.

(3)冷却履歴解析工程(S2)
図2に冷却履歴解析工程S2の流れ図を示す。冷却履歴解析工程S2は、解析上の溶湯(以下、溶湯ともいう。)が流動している段階では第1の冷却履歴解析工程S21を、次いで溶湯が流動を停止した後から、図7に示す共析変態温度TA1以下である所定の温度TENDに到達するまでの段階は第2の冷却履歴解析工程S22を実行する工程であり、公知の湯流れ・凝固シミュレーションの手法を用いることができる。
(3) Cooling history analysis step (S2)
FIG. 2 shows a flowchart of the cooling history analysis step S2. The cooling history analysis step S2 is shown in FIG. 7 after the first cooling history analysis step S21 at the stage where the analytical molten metal (hereinafter also referred to as molten metal) flows, and then after the molten metal stops flowing. The stage until reaching a predetermined temperature T END that is equal to or lower than the eutectoid transformation temperature T A1 is a step of executing the second cooling history analysis step S22, and a known hot water flow / solidification simulation method can be used. .

冷却履歴解析工程S2では、鋳物要素間と、鋳物要素と鋳型要素との間の伝熱を経時的に解析し、n個の鋳物要素毎に解析上の時刻tと、時刻tにおける解析上の温度Tの組データ(t,T)を取得して、電磁的な記憶手段(以下、記憶手段ともいう。)に格納する。ここで添字mは経時的な解析上の時間ステップを表し、時刻tは初期時刻tからm番目の時間ステップの時刻を意味する。 In the cooling history analysis step S2, and between the casting elements, analysis over time was analyzed, and time t m on analysis for each n-number of the casting element, at time t m heat transfer between the casting elements and the mold elements The set data (t m , T m ) of the upper temperature T m is acquired and stored in electromagnetic storage means (hereinafter also referred to as storage means). Here, the subscript m represents a time step in analysis over time, and the time t m means the time of the mth time step from the initial time t 0 .

(3−1)第1の冷却履歴解析工程(S21)
第1の冷却履歴解析工程S21は、溶湯が鋳物要素に充填される挙動を計算する湯流れ解析を用いる工程である。第1の冷却履歴解析工程S21では、上記要素作成工程S1で作成した鋳物要素の一部をなす湯口要素には溶湯の流入量または流入圧力を、各要素には密度、比熱、熱伝導率及び粘性係数などの物性値、初期温度及び初期圧力を、また、鋳物要素と鋳型要素間の伝熱条件として熱伝達係数を付与した後、例えばナビエストークスの式などを利用して、鋳物要素における溶湯の位置、温度、圧力などを経時的に求める。この工程において、n個の鋳物要素について時間ステップ毎の時刻と温度との組データ(t,T)を得ることができる。
(3-1) First cooling history analysis step (S21)
The first cooling history analysis step S21 is a step using a molten metal flow analysis for calculating a behavior in which a molten metal is filled in a casting element. In the first cooling history analysis step S21, the inflow amount or the inflow pressure of the molten metal is applied to the gate element forming part of the casting element created in the element creation step S1, and the density, specific heat, thermal conductivity and After assigning physical properties such as viscosity coefficient, initial temperature and initial pressure, and heat transfer coefficient as the heat transfer condition between the casting element and the mold element, for example, using the Naviestokes formula, the molten metal in the casting element The position, temperature, pressure, etc. are obtained over time. In this process, the set data (t m , T m ) of time and temperature for each time step can be obtained for n casting elements.

(3−2)第2の冷却履歴解析工程(S22)
第2の冷却履歴解析工程S22は、溶湯の流動が停止した後から共析変態温度TA1以下の所定の温度TENDに温度が低下するまで、各要素に対して熱伝導解析を用いる工程である。第2の冷却履歴解析工程S22では、鋳物要素と鋳型要素に、密度、比熱、熱伝導率、凝固潜熱などの物性値及び第1の冷却履歴解析工程S21で得られた流動完了時点の時刻と温度の組データを付与し、鋳物要素と鋳型要素間の伝熱条件として熱伝達係数などを付与した後、すべての鋳物要素に溶湯が充填された直後からの、n個の鋳物要素の時刻と温度との組データ(t,T)を経時的に求める。
(3-2) Second cooling history analysis step (S22)
The second cooling history analysis step S22 is a step of using heat conduction analysis for each element until the temperature drops to a predetermined temperature T END equal to or lower than the eutectoid transformation temperature T A1 after the flow of the molten metal stops. is there. In the second cooling history analysis step S22, the casting element and the mold element are provided with physical properties such as density, specific heat, thermal conductivity, latent heat of solidification, and the time when the flow is completed obtained in the first cooling history analysis step S21. After giving temperature set data and giving heat transfer coefficient etc. as a heat transfer condition between casting elements and mold elements, the time of n casting elements immediately after all the casting elements are filled with molten metal The set data (t m , T m ) with temperature is obtained over time.

第2の冷却履歴解析工程S22は、鋳物の引け巣予測を目的に広く行われている手法と同様であり、引け巣予測を目的とする場合、通常は鋳物の凝固が終了した時点で解析を終了すればよい。しかし本発明においては、鋳物の温度が十分に低下したときの鋳物の硬度を求めることを目的としているため、凝固が終了した後も所定の温度TENDに降下するまで解析を継続する。 The second cooling history analysis step S22 is the same as a technique widely used for the purpose of predicting shrinkage cavities of castings. When aiming at shrinkage cavities, the analysis is usually performed at the time when solidification of the casting is completed. Just finish. However, in the present invention, since the object is to determine the hardness of the casting when the temperature of the casting is sufficiently lowered, the analysis is continued until the temperature falls to the predetermined temperature T END even after the solidification is completed.

解析を終了する所定の温度TENDは、球状黒鉛鋳鉄の共析変態温度TA1よりも低い温度とする。その理由は、硬度に大きな影響を及ぼすパーライト相が共析変態温度TA1を通過する過程で鋳物の組織中に析出するからである。共析変態温度TA1よりも低い温度域では球状黒鉛鋳鉄鋳物の硬度はあまり変化しないので、少なくとも共析変態温度TA1よりも低い温度に低下するまで解析を実施する。球状黒鉛鋳鉄の共析変態温度TA1は約730℃であるが、球状黒鉛鋳鉄の共析変態は共析変態温度付近のある温度幅で進行するので、解析を終了する所定の温度TENDは、共析変態温度よりも100℃以上低い温度である630℃以下とすることが好ましい。 The predetermined temperature T END for ending the analysis is set to a temperature lower than the eutectoid transformation temperature T A1 of the spheroidal graphite cast iron. This is because the great influence pearlite hardness is deposited on tissue of the casting in the process of passing through the eutectoid transformation temperature T A1. In the temperature range lower than the eutectoid transformation temperature T A1, the hardness of the spheroidal graphite cast iron casting does not change so much. Therefore, the analysis is performed until the hardness is lowered to at least a temperature lower than the eutectoid transformation temperature T A1 . The eutectoid transformation temperature T A1 of the spheroidal graphite cast iron is about 730 ° C. However, since the eutectoid transformation of the spheroidal graphite cast iron proceeds in a certain temperature range near the eutectoid transformation temperature, the predetermined temperature T END for ending the analysis is The temperature is preferably 630 ° C. or lower, which is 100 ° C. or lower than the eutectoid transformation temperature.

時間ステップの間隔τの値は通常の湯流れ・凝固シミュレーションで設定する値でもよい。τの値が小さいほど冷却履歴を精度よく解析できる一方で、解析時間は増大する。このため、冷却履歴の各段階に応じてτの値を変えてもよい。例えば、時間当たりの温度変化が大きい段階ではτの値を小さくし、温度変化が小さい段階ではτの値を大きくすれば、解析精度と解析時間とのバランスが良好になるので好ましい。   The value of the time step interval τ may be a value set in a normal molten metal flow / solidification simulation. The smaller the value of τ, the more accurately the cooling history can be analyzed, while the analysis time increases. For this reason, the value of τ may be changed according to each stage of the cooling history. For example, it is preferable to decrease the value of τ when the temperature change per time is large and increase the value of τ when the temperature change is small because the balance between the analysis accuracy and the analysis time is improved.

(4)化学成分値設定工程S3
球状黒鉛鋳鉄鋳物の硬度は、その化学成分値によっても変化する。これは、化学成分値によって鋳物の組織が変化するからである。球状黒鉛鋳鉄鋳物の組織は、軟質のフェライト相と硬質のパーライト相とからなる基地と、基地に分散する球状黒鉛とからなる。組織を構成するこれらの相は化学成分によってその占める割合が変化し、また特にフェライト相はそれ自身の硬度も変化する。化学成分値設定工程S3では、これらの構成相の性質に特に大きく影響する元素として、少なくともC、Si、Cu及びMnの化学成分値を与えることが好ましい。これらの化学成分値は予め記憶手段に格納しておくことが好ましく、後述する硬度計算工程S7で読み込まれる。
(4) Chemical component value setting step S3
The hardness of the spheroidal graphite cast iron casting also varies depending on its chemical component value. This is because the structure of the casting changes depending on the chemical component value. The structure of the spheroidal graphite cast iron casting is composed of a base composed of a soft ferrite phase and a hard pearlite phase, and spheroidal graphite dispersed in the base. The proportion of these phases constituting the structure varies depending on chemical components, and in particular, the ferrite phase also varies in its own hardness. In the chemical component value setting step S3, it is preferable to give chemical component values of at least C, Si, Cu, and Mn as elements that greatly affect the properties of these constituent phases. These chemical component values are preferably stored in the storage means in advance, and are read in the hardness calculation step S7 described later.

(5)温度設定工程S4
温度設定工程S4は、後述の冷却速度計算工程S6において、共晶凝固の冷却速度V(以下、第1の冷却速度ともいう。)、共晶凝固後の冷却速度V(以下、第2の冷却速度ともいう。)及び共析変態の冷却速度V(以下、第3の冷却速度ともいう。)で使用される温度区間を区画するために温度を設定する工程である。以下、再度、図7を参照しつつ説明する。
(5) Temperature setting step S4
In the temperature setting step S4, a cooling rate V 1 for eutectic solidification (hereinafter also referred to as a first cooling rate) and a cooling rate V 2 after eutectic solidification (hereinafter referred to as a second rate) in the cooling rate calculation step S6 described later. And a eutectoid transformation cooling rate V 3 (hereinafter also referred to as a third cooling rate), and a temperature setting step for defining a temperature section. Hereinafter, description will be made again with reference to FIG.

(5−1)第1の温度T1及び第2の温度T2
図7に示す第1の温度T1と第2の温度T2は第1の冷却速度Vを計算するためのものであり、T1>T2を満たすものとする。球状黒鉛鋳鉄の共晶凝固温度Tは1150℃付近であるので、第1の温度T1は1150℃以上の値とするが、過度に高い値とすると硬度や黒鉛粒数の予測精度が低下するので、1150℃以上1200℃以下とする。第1の温度T1は、好ましくは1155℃以上1180℃以下、より好ましくは1155℃以上1165℃以下である。一方、共晶凝固温度Tは化学成分や接種の有無、周囲からの抜熱状態などの製造条件により若干低下したり、図7中に示す若干の過冷却2を生じたりすることがある。このため、第2の温度T2は過冷却2の温度よりも低い温度である1145℃以下とすることが好ましいが、過度に低い値であると硬度や黒鉛粒数の予測精度が低下するので1145℃以下1080℃以上とする。第2の温度T2は、好ましくは1145℃以下1095℃以上である。
(5-1) First temperature T1 and second temperature T2
The first temperature T1 and the second temperature T2 shown in FIG. 7 are for calculating the first cooling rate V1, and satisfy T1> T2. Since the eutectic solidification temperature T E of the spherical graphite cast iron is around 1150 ° C., the first temperature T1 is a value equal to or greater than 1150 ° C., when excessively high value prediction accuracy of the hardness and the number of graphite grains decreases Therefore, it shall be 1150 degreeC or more and 1200 degrees C or less. The first temperature T1 is preferably 1155 ° C. or higher and 1180 ° C. or lower, more preferably 1155 ° C. or higher and 1165 ° C. or lower. On the other hand, the presence of the eutectic solidification temperature T E chemical composition and inoculation slightly or decreased by the production conditions such as heat removal conditions from ambient, it may or cause a slight supercooling 2 shown in FIG. For this reason, it is preferable that the second temperature T2 is 1145 ° C. or lower, which is a temperature lower than the temperature of the supercooling 2, but if it is an excessively low value, the accuracy of predicting the hardness and the number of graphite grains decreases, so 1145 C. or lower and 1080 C or higher. The second temperature T2 is preferably 1145 ° C. or lower and 1095 ° C. or higher.

(5−2)第3の温度T3及び第4の温度T4
第3の温度T3と第4の温度T4は第2の冷却速度Vを計算するためのものであり、T3>T4を満たすものとする。第3の温度T3は共晶凝固完了後の温度であればよいが。好ましくは第2の温度T2以下とする。第4の温度T4は共析変態温度TA1よりも大きい値とする。第3の温度T3及び第4の温度T4は、T3>T4を満足したうえで、好ましくはT2(℃)以下950℃以上、好ましくはT2(℃)以下1000℃以上である。
(5-2) Third temperature T3 and fourth temperature T4
The third temperature T3 and the fourth temperature T4 are for calculating the second cooling rate V2, and satisfy T3> T4. The third temperature T3 may be a temperature after completion of eutectic solidification. The second temperature is preferably equal to or lower than the second temperature T2. The fourth temperature T4 to a value larger than the eutectoid transformation temperature T A1. The third temperature T3 and the fourth temperature T4 satisfy T3> T4, and are preferably T2 (° C.) or lower and 950 ° C. or higher, preferably T2 (° C.) or lower and 1000 ° C. or higher.

(5−3)第5の温度T5及び第6の温度T6
第5の温度T5と第6の温度T6は第3の冷却速度Vを計算するためのものであり、T5>T6を満たすものとする。第5の温度T5は共析変態温度TA1よりも高い温度とし、第6の温度T6は共析変態温度TA1よりも低い温度とする。第5の温度T5が過度に高い値である場合や、第6の温度T6が過度に低い値である場合は硬度の予測精度が低下するので、第5の温度T5は735℃以上755℃以下とすることが好ましく、第6の温度T6は720℃以下700℃以上とすることが好ましい。
(5-3) Fifth temperature T5 and sixth temperature T6
The fifth temperature T5 and the sixth temperature T6 are for calculating the third cooling rate V3, and satisfy T5> T6. The fifth temperature T5 is a temperature higher than the eutectoid transformation temperature T A1 , and the sixth temperature T6 is a temperature lower than the eutectoid transformation temperature T A1 . When the fifth temperature T5 is an excessively high value, or when the sixth temperature T6 is an excessively low value, the accuracy of predicting hardness decreases, so the fifth temperature T5 is 735 ° C. or more and 755 ° C. or less. The sixth temperature T6 is preferably 720 ° C. or lower and 700 ° C. or higher.

前述した解析終了の設定温度TENDを含めた上記の設定温度T1〜T6は、T1≧T>T2≧T3>T4≧T5>TA1>T6>TENDを満たすように設定する。TEND、T1〜T6の各設定温度は、予め記憶手段に格納しておくことが好ましい。 The above set temperature T1~T6 including the set temperature T END of the foregoing analysis end is set so as to satisfy the T1 ≧ T E> T2 ≧ T3 > T4 ≧ T5> T A1>T6> T END. Each set temperature of T END and T1 to T6 is preferably stored in the storage means in advance.

(6)最高温度計算工程S5
最高温度計算工程S5は、冷却履歴解析工程S2で得られた時刻と温度との組データから、その鋳物要素が到達する最高温度Tmaxを求める工程である。冷却履歴解析工程S2で取得し、記憶手段に格納された時刻と温度の組データ(t,T)を読み込み、Tmの最大値をその要素の最高温度Tmaxとして、その時刻tmaxの組データ(tmax,Tmax)を記憶手段に格納する。
(6) Maximum temperature calculation step S5
The maximum temperature calculation step S5 is a step of obtaining the maximum temperature Tmax that the casting element reaches from the set data of the time and temperature obtained in the cooling history analysis step S2. The time and temperature set data (t m , T m ) acquired in the cooling history analysis step S2 and stored in the storage means is read, and the maximum value of T m is set as the maximum temperature T max of the element, and the time t max The set data (t max , T max ) is stored in the storage means.

(7)冷却速度計算工程S6
次いで、冷却速度計算工程S6を実行する。図3は冷却速度計算工程S6を示す流れ図である。冷却速度計算工程S6は、第1の冷却速度計算工程S61、第2の冷却速度計算工程S62及び第3の冷却速度計算工程S63からなり、冷却履歴解析工程S2で得られた時刻と温度との組データ(t,T)と、温度設定工程S4で設定した設定温度T1〜T6とを読み込みつつ、S61、S62、S63の順に実行される。これら第1〜第3の冷却速度計算工程S61〜S63はいずれも同様の流れとなるので、第1の冷却速度計算工程S61のみを図4を用いて詳細に説明し、他は簡潔な記載とする。
(7) Cooling rate calculation step S6
Next, the cooling rate calculation step S6 is executed. FIG. 3 is a flowchart showing the cooling rate calculation step S6. The cooling rate calculation step S6 includes a first cooling rate calculation step S61, a second cooling rate calculation step S62, and a third cooling rate calculation step S63, and includes the time and temperature obtained in the cooling history analysis step S2. While reading the set data (t m , T m ) and the set temperatures T1 to T6 set in the temperature setting step S4, the processes are executed in the order of S61, S62, and S63. Since the first to third cooling rate calculation steps S61 to S63 all have the same flow, only the first cooling rate calculation step S61 will be described in detail with reference to FIG. To do.

(7−1)第1の冷却速度計算工程S61
図4に第1の冷却速度計算工程S61の流れ図を示す。冷却履歴解析工程S2では時間ステップ毎に飛び飛びの温度Tを取得しているので、取得された温度Tは、温度設定工程S4で設定した第1の温度T1や第2の温度T2に完全に一致する値が存在しない場合がある。したがって、第1の冷却速度Vの計算に用いる温度として、第1の温度T1と第2の温度T2に替えて、第1の解析温度T1と第2の解析温度T2を用いる。第1の解析温度T1は、第1の温度T1に最も近い温度であり、第1の温度T1に到達する直前または直後の時刻における温度である。第2の解析温度T2についても同様とし、後述する第3〜第6の解析温度T3〜T6についても同様とする。
(7-1) First cooling rate calculation step S61
FIG. 4 shows a flowchart of the first cooling rate calculation step S61. In the cooling history analysis step S2, the jumping temperature Tm is acquired for each time step, so the acquired temperature Tm is completely equal to the first temperature T1 and the second temperature T2 set in the temperature setting step S4. There may be no value that matches. Accordingly, as the temperature used in the first calculation of the cooling rate V 1, a first temperature T1 in place to a second temperature T2, using the first analysis temperature T1 A second analysis temperature T2 A. The first analysis temperature T1 A is a temperature closest to the first temperature T1, and is a temperature at a time immediately before or immediately after reaching the first temperature T1. Also the same for the second analysis temperature T2 A, and similarly for the third to sixth analysis temperature T3 A to T6 A to be described later.

先ず、第1の解析温度T1を取得する工程を示す。冷却履歴解析工程S2で得られた組データのうち、第1の冷却速度計算工程S61で読み込む最初の組データ(t,T)は、直前の工程である最高温度計算工程S6で求められた最高温度Tmaxを示す組データ(tmax,Tmax)=(t,T)の次の時間ステップの(tm+1,Tm+1)とする。すなわち、m=m+1として(t,T)を読み込む。 First, a step of obtaining the first analysis temperature T1 A is shown. Of the set data obtained in the cooling history analysis step S2, the first set data (t m , T m ) read in the first cooling rate calculation step S61 is obtained in the maximum temperature calculation step S6 which is the immediately preceding step. The set data (t max , T max ) = (t m , T m ) indicating the maximum temperature T max is set to (t m + 1 , T m + 1 ) of the next time step. That is, (t m , T m ) is read with m = m + 1.

次いで、温度Tと温度設定工程S4で設定した第1の温度T1との大小関係を比較し、T1<Tの場合はさらにm=m+1として順次これを繰り返す。そしてT≦T1となったとき、次の操作により、第1の解析温度T1とその時刻t1との組データ(t1,T1)として記憶手段に格納する。すなわちT<T1の場合は、TとT1との差(T1−T)と1つ前の時刻tm−1におけるTm−1とT1との差(Tm−1−T1)が、(Tm−1−T1)≦(T1−T)であるときは組データ(tm−1,Tm−1)を(t1,T1)として記憶手段に格納する。これに対し、T=T1の場合及び(Tm−1−T1)>(T1−T)場合は時刻tにおける組データ(t,T)を(t1,T1)として記憶手段に格納する。つまり、温度Tのうち第1の温度T1に最も近い温度を第1の解析温度T1とするのである。 Then, by comparing the magnitude relation between the first temperature T1 set in a temperature T m and the temperature setting step S4, successively repeating this as further m = m + 1 in the case of T1 <T m. When T m ≦ T1, the following operation is performed to store in the storage means as set data (t1, T1 A ) of the first analysis temperature T1 A and the time t1. That is, in the case of T m <T1, the difference between T m and T1 (T1−T m ) and the difference between T m−1 and T1 at the previous time t m−1 (T m−1 −T1) but stored in the storage unit set data (t m-1, T m -1) as (t1, T1 a) when a (T m-1 -T1) ≦ (T1-T m). On the other hand, when T m = T 1 and (T m−1 −T 1 )> (T 1 −T m ), the set data (t m , T m ) at time t m is stored as (t 1, T 1 A ). Store in the means. That is, to the closest temperature to the first temperature T1 first analysis temperature T1 A of the temperature T m.

次いで実行される第2の解析温度T2を取得する工程も、第1の解析温度T1を取得する工程と同様である。すなわち、m=m+1、すなわち第1の解析温度T1を取得する工程で記憶手段に格納した組データの1つ後の時間ステップにおける組データを記憶手段より読み込み、温度設定工程S4で設定した第2の温度T2との大小関係を比較しつつ、T2≦Tとなるまでこれを順次繰り返し、第1の解析温度T1を取得する方法と同様の方法で第2の解析温度T2における組データ(t2,T2)を取得して、記憶手段に格納する。つまり、温度Tのうち第2の温度T2に最も近い温度を第2の解析温度T2とする。 Obtaining a second analysis temperature T2 A to be executed and then also the same as obtaining a first analysis temperature T1 A. That is, m = m + 1, that is, the set data in the time step immediately after the set data stored in the storage means in the step of acquiring the first analysis temperature T1 A is read from the storage means, and set in the temperature setting step S4. while comparing the magnitude relation between the second temperature T2, successively repeating this until T2 ≦ T m, set in the second analysis temperature T2 a by the same method as for obtaining the first analysis temperature T1 a Data (t2, T2 A ) is acquired and stored in the storage means. In other words, the closest temperature to the second temperature T2 and the second analysis temperature T2 A of the temperature T m.

そして、第1の冷却速度Vを計算する。記憶手段に格納された組データ(t1,T1)と(t2,T2)を読み込み、V=(T1−T2)/(t2−t1)の計算式により第1の冷却速度Vを求めて、記憶手段に格納する。 Then, calculating a first cooling rate V 1. The set data (t1, T1 A ) and (t2, T2 A ) stored in the storage means are read, and the first cooling rate V is calculated by the calculation formula of V 1 = (T1 A −T2 A ) / (t2−t1). 1 is obtained and stored in the storage means.

(7−2)第2の冷却速度計算工程S62及び第3の冷却速度計算工程S63
引き続いて、第2の冷却速度計算工程S62と第3の冷却速度計算工程S63を実行する。第2の冷却速度計算工程S62及び第3の冷却速度計算工程S63ともに図示は省略するが、いずれもm=m+1として、直前の工程で記憶手段に格納した組データの1つ後の時間ステップにおける組データを記憶手段から読み込んで、第1の冷却速度計算工程S61と同様の方法で行う。第2の冷却速度計算工程S62により、第3の解析温度T3における組データ(t3,T3)及び第4の解析温度T4における組データ(t4、T4)が取得され、次いで第2の冷却速度Vが計算されて記憶手段に格納される。次いで、第3の冷却速度計算工程S63により、第5の解析温度T5における組データ(t5,T5)及び第6の解析温度T6における組データ(t6,T6)が取得され、第3の冷却速度Vが計算されて記憶手段に格納される。
(7-2) Second cooling rate calculation step S62 and third cooling rate calculation step S63
Subsequently, the second cooling rate calculation step S62 and the third cooling rate calculation step S63 are executed. Although both the second cooling rate calculation step S62 and the third cooling rate calculation step S63 are not shown, both m = m + 1 and in the time step after the set data stored in the storage means in the immediately preceding step. The set data is read from the storage means, and is performed in the same manner as in the first cooling rate calculation step S61. The second cooling speed calculation step S62, the set data in the third analysis temperature T3 A (t3, T3 A) and the fourth set data in the analysis temperature T4 A of (t4, T4 A) is obtained, then the second cooling rate V 2 of are stored in the computed and the storage means. Then, the third cooling rate calculation step S63, the set data in the fifth analysis temperature T5 A of (t5, T5 A) and a sixth set data in the analysis temperature T6 A of (t6, T6 A) is obtained, the The cooling rate V3 of 3 is calculated and stored in the storage means.

以上の最高温度計算工程S5と、これに続く冷却速度計算工程S6までの一連の工程を、n個の鋳物要素について実行する。   The above-described maximum temperature calculation step S5 and the subsequent series of steps up to the cooling rate calculation step S6 are executed for n casting elements.

(8)硬度計算工程S7
鋳物要素の硬度Hを予測する式は、前述のように実験データに基づき回帰計算等によって予め作成した硬度予測式を適用する。図5は硬度計算工程S7を示す流れ図である。図5では、黒鉛粒数予測式を実行する黒鉛粒数計算工程S71と硬度予測式を実行する工程S72とに工程を分けているが、黒鉛粒数予測式も含めた硬度予測式を計算する1つの工程で実行してもよい。以下、黒鉛粒数予測式として前述の(式5)を実行する黒鉛粒数計算工程S71と、硬度予測式として前述の(式4)を用いる硬度予測式を実行する工程S72とに工程を分ける例で説明するが、これに限定されない。例えば、硬度予測式(式4)のNの項は、一定値(例えば、300個/mm)として黒鉛粒数Nを設定してもよいが、黒鉛粒数予測式(式5)により黒鉛粒数計算工程S71を実行すれば、硬度の予測精度を向上できる。
(8) Hardness calculation step S7
As a formula for predicting the hardness H B of the casting element, a hardness prediction formula created in advance by regression calculation or the like based on experimental data as described above is applied. FIG. 5 is a flowchart showing the hardness calculation step S7. In FIG. 5, the process is divided into the graphite grain number calculation step S71 for executing the graphite grain number prediction formula and the step S72 for executing the hardness prediction formula, but the hardness prediction formula including the graphite grain number prediction formula is calculated. You may perform by one process. Hereinafter, the steps are divided into a graphite particle number calculation step S71 that executes the above-described (Equation 5) as a graphite particle number prediction equation, and a step S72 that executes a hardness prediction equation that uses the above-described (Equation 4) as a hardness prediction equation. This will be described with an example, but the present invention is not limited to this. For example, the NG term of the hardness prediction formula (Formula 4) may set the graphite grain number NG as a constant value (for example, 300 particles / mm 2 ), but the graphite grain count prediction formula (Formula 5) If the graphite particle number calculation step S71 is executed, the accuracy of predicting the hardness can be improved.

先に黒鉛粒数計算工程S71を実行する。すなわち、冷却速度計算工程S6までに取得され記憶手段に格納された最高温度Tmax、第1の冷却速度V及び化学成分設定工程S3で設定され記憶手段に格納されたC%とSi%を読み込んで、黒鉛粒数予測式(式5)を実行し、黒鉛粒数Nを得る。次いで、硬度予測式を実行する(S72)。すなわち、黒鉛粒数計算工程S71における黒鉛粒数予測式(式5)によって得られた黒鉛粒数N、冷却速度計算工程S6で取得され記憶手段に格納された第2の冷却速度Vと第3の冷却速度V及び化学成分設定工程S3で設定され記憶手段に格納されたCu%とMn%の値を読みこんで、硬度予測式(式4)により硬度Hを計算し、記憶手段に格納する。以上のS71〜S73の工程を、n個の鋳物要素すべて、またはn個のうちの必要な部位の鋳物要素について実行する。なお、硬度予測式(式4)において、共析変態の冷却速度(第3の冷却速度V)と共晶凝固後の冷却速度(第2の冷却速度V)との相対値は、必ずしも計算に含めなくともよいが、両者の冷却速度の相対値を、例えばV/Vとして計算に含めれば、特に薄肉部の硬度の予測精度を高めることができる。 First, the graphite particle number calculation step S71 is executed. That is, the maximum temperature T max acquired up to the cooling rate calculation step S6 and stored in the storage means, the first cooling rate V 1 and the C% and Si% set in the chemical component setting step S3 and stored in the storage means. Read and execute the graphite grain number prediction formula (Formula 5) to obtain the graphite grain number NG . Next, a hardness prediction formula is executed (S72). That is, the graphite particle number N G obtained by the graphite particle number prediction formula (Equation 5) in the graphite particle number calculation step S71, the second cooling rate V 2 obtained in the cooling rate calculation step S6 and stored in the storage means The values of Cu% and Mn% set in the third cooling rate V 3 and chemical component setting step S3 and stored in the storage means are read, and the hardness H B is calculated by the hardness prediction formula (formula 4) and stored. Store in the means. The above-described steps S71 to S73 are executed for all n casting elements or a casting element at a necessary portion of the n casting elements. In the hardness prediction formula (Formula 4), the relative value between the cooling rate of the eutectoid transformation (third cooling rate V 3 ) and the cooling rate after eutectic solidification (second cooling rate V 2 ) is not necessarily limited. Although not necessarily included in the calculation, if the relative value of both cooling rates is included in the calculation as, for example, V 3 / V 2 , the accuracy of predicting the hardness of the thin portion can be particularly improved.

(9)硬度出力工程S8
硬度計算工程S7で計算され、記憶手段に格納されたn個の鋳物要素すべて、またはn個のうちの必要な部位の鋳物要素の硬度は、例えばポストプロセッサを使用して要素毎に3次元モデルにマッピングされた画像として出力されることが好ましい。例えば市販のビュワーソフトを用いることにより、硬度を画像出力することができる。硬度を画像出力することで鋳物の部位ごとの硬度の分布を、視覚的に容易に認識することができる。
(9) Hardness output step S8
The hardness of all the n casting elements calculated in the hardness calculation step S7 and stored in the storage means, or the hardness of the casting elements in the necessary portions of the n casting parts, is determined by a three-dimensional model for each element using a post processor, for example. It is preferable to output as an image mapped to. For example, the hardness can be output as an image by using commercially available viewer software. By outputting the hardness as an image, the distribution of hardness for each part of the casting can be easily recognized visually.

以下、本発明を具体的に実施した例を図面及び表を用いて説明する。   Hereinafter, examples in which the present invention is specifically implemented will be described with reference to the drawings and tables.

(実施例1)鋳物工場A、製品A
実施例1は鋳物工場Aで製造される球状黒鉛鋳鉄からなる鋳物である製品A(ステアリングナックル)に本発明の硬度を予測する方法を適用した例である。硬度計算工程S7の硬度予測式を実行する工程S72で使用した硬度Hの予測式は(式4)に示した関数形の式、すなわち
=ω+αCueq+α+α+α/V (式6)
とし、
同じく硬度計算工程S7の黒鉛粒数計算工程S71で使用した黒鉛粒数予測式は(式5)の関数形の式、すなわち
=ψ+DCE(β−ψ)+β+βmax (式7)
とした。
(Example 1) Foundry A, product A
Example 1 is an example in which the method of predicting the hardness of the present invention is applied to a product A (steering knuckle) that is a casting made of spheroidal graphite cast iron manufactured at a foundry A. Prediction equation is the formula of function form shown in equation (4) of the hardness H B used in step S72 to perform the hardness prediction equation of hardness calculating step S7, i.e. H B = ω + α 1 Cu eq + α 2 V 3 + α 3 N G + α 4 V 3 / V 2 (Formula 6)
age,
Similarly, the graphite particle number prediction formula used in the graphite particle number calculation step S71 of the hardness calculation step S7 is a functional equation of (Equation 5), that is, N G = ψ 1 + D CE1 V 1 −ψ 2 ) + β 2 V 1 + β 3 T max (Equation 7)
It was.

また、(式6)の定数α〜α4、ω及びCueqを求める式Cueq=Cu%+ξMn%の定数ξは表1に示す値を用いた。すなわち、α=100、α=250、α=−0.10、α=−50、ω=120、ξ=0.3とした。また、(式7)の定数β〜β、ψ、ψ並びにDCEを求める式DCE=C%+ξSi%−φの定数ξ及びφは、表2に示す値を用いた。すなわち、β=300、β=100、β=−1.0、ψ=1000、ψ=70、ξ=0.33、φ=4.5とした。 Moreover, the value shown in Table 1 was used for the constant ξ 2 of the formula Cu eq = Cu% + ξ 2 Mn% for obtaining the constants α 1 to α 4, ω and Cu eq of (Formula 6). That is, α 1 = 100, α 2 = 250, α 3 = −0.10, α 4 = −50, ω = 120, and ξ 2 = 0.3. Moreover, the constant β 1 3, ψ 1, formula D CE = constants C% + ξ 1 Si% -φ ξ 1 and φ for obtaining the [psi 2 and D CE, the values shown in Table 2 (Formula 7) Using. That is, β 1 = 300, β 2 = 100, β 3 = −1.0, ψ 1 = 1000, ψ 2 = 70, ξ 1 = 0.33, and φ = 4.5.

化学成分値設定工程S3では元素としてC、Si、Cu及びMnについて、表3に示す質量%の値を用いた。すなわち、C%=3.6、Si%=2.4、Cu=0.1、Mn%=0.2とした。なお、表3に示す実施例1の元素の質量%は、鋳物工場Aで製造される製品Aの製造において狙いとする化学成分値である。   In the chemical component value setting step S3, the mass% values shown in Table 3 were used for C, Si, Cu and Mn as elements. That is, C% = 3.6, Si% = 2.4, Cu = 0.1, and Mn% = 0.2. In addition, the mass% of the element of Example 1 shown in Table 3 is a chemical component value aimed at in the manufacture of the product A manufactured in the foundry A.

温度設定工程S4で与えた第1の温度T1〜第6の温度T6は、表4に示す値を用いた。すなわち、T1=1160、T2=1100、T3=1100、T4=1000、T5=740、T6=710とした。   The values shown in Table 4 were used for the first temperature T1 to the sixth temperature T6 given in the temperature setting step S4. That is, T1 = 1160, T2 = 1100, T3 = 1100, T4 = 1000, T5 = 740, T6 = 710.

また、冷却履歴解析工程S2において解析を終了する所定の温度TENDも、表4に示す値、すなわちTEND=600を用いた。 In addition, the value shown in Table 4, that is, T END = 600, was also used as the predetermined temperature T END for finishing the analysis in the cooling history analysis step S2.

以上の式と定数を用いて本発明の実施例により求めた硬度の予測値と、実際の鋳物すなわち実物の硬度の実測値と、の比較を図6に示す。図6(a)は製品Aにおいて硬度を予測及び実測した部位H1〜H4を示す図であり、図6(b)は図6(a)に示す部位H1〜H4における硬度Hの予測値と実測値とを比較した図である。図6(b)中の白抜きのマーカーによるプロットが実施例1の結果を示す。0.1質量%のCuを含有する実際の鋳物では、軟質のフェライト相が比較的多い組織となって硬度は低目となるが、Cu%=0.1に設定した実施例1により予測した硬度と実測の硬度とは良く一致しており、本発明によって球状黒鉛鋳鉄鋳物の硬度を精度よく予測できた。 FIG. 6 shows a comparison between the predicted value of hardness obtained by the example of the present invention using the above formulas and constants, and the actually measured value of the hardness of the actual casting, that is, the actual product. 6 (a) is a diagram showing a portion H1~H4 predicted and measured hardness in product A, Fig. 6 (b) and the predicted value of the hardness H B at the site H1~H4 shown in FIG. 6 (a) It is the figure which compared measured value. Plots with open markers in FIG. 6B show the results of Example 1. In an actual casting containing 0.1% by mass of Cu, the soft ferrite phase becomes a relatively large structure and the hardness is low, but this was predicted by Example 1 where Cu% = 0.1 was set. The hardness and the measured hardness were in good agreement, and the present invention was able to accurately predict the hardness of the spheroidal graphite cast iron casting.

(実施例2)鋳物工場B、製品A
実施例2は実施例1とは製造ラインが異なる鋳物工場Bにおいて製造される、実施例1と同一形状の球状黒鉛鋳鉄からなる鋳物である製品A(ステアリングナックル)に本発明の硬度を予測する方法を適用した例である。硬度予測式及び黒鉛粒数予測式は実施例1と同じ関数形の(式6)、(式7)を夫々用いたが、(式7)の定数β2、β、ψは表2に示すように実施例1とは異なる数値を用いた。すなわち、β=400、β=−0.1、ψ=500とした。表2に示す他の定数及び表1に示す定数は実施例1と同じ値を用いた。
(Example 2) Foundry B, product A
Example 2 predicts the hardness of the present invention for a product A (steering knuckle), which is a casting made of spheroidal graphite cast iron having the same shape as Example 1 manufactured in a foundry B having a different production line from Example 1. This is an example of applying the method. As the hardness prediction formula and the graphite grain number prediction formula, (Formula 6) and (Formula 7) having the same function form as in Example 1 were used, respectively, but constants β 2 , β 3 , and ψ 1 in (Formula 7) are shown in Table 2. As shown in FIG. 4, numerical values different from those in Example 1 were used. That is, β 2 = 400, β 3 = −0.1, and ψ 1 = 500. The other constants shown in Table 2 and the constants shown in Table 1 were the same as in Example 1.

化学成分値設定工程S3では元素としてC、Si、Cu及びMnについて、表3に示す質量%の値を用いた。すなわち、C%=3.7、Si%=2.3、Cu=0.4、Mn%=0.2とした。なお、表3に示す実施例2の元素の質量%は、鋳物工場Bで製造される製品Aの製造において狙いとする化学成分値である。   In the chemical component value setting step S3, the mass% values shown in Table 3 were used for C, Si, Cu and Mn as elements. That is, C% = 3.7, Si% = 2.3, Cu = 0.4, and Mn% = 0.2. In addition, the mass% of the element of Example 2 shown in Table 3 is a chemical component value aimed at in the manufacture of the product A manufactured in the foundry B.

温度設定工程S4で与えた第1の温度T1〜第6の温度T6は、表4に示すように実施例1と同じ値を用いた。   As shown in Table 4, the same values as in Example 1 were used for the first temperature T1 to the sixth temperature T6 given in the temperature setting step S4.

実施例2により硬度を計算した結果を、実施例1で示した図6(b)に合わせて同様に示す。実施例2で硬度を予測及び実測した部位H1〜H4は、実施例1と同一の図6(a)に示す部位とした。図6(b)は部位H1〜H4における硬度Hの予測値と実測値とを比較した図であり、図中の黒く塗りつぶしたマーカーによるプロットが実施例2の結果を示す。0.4質量%のCuを含有する実際の鋳物では、硬質のパーライト相が比較的多い組織となって硬度は高目となるが、Cu%=0.4に設定した実施例2により予測した硬度と実測の硬度とは良く一致しており、本発明によって球状黒鉛鋳鉄鋳物の硬度を精度よく予測できた。 The result of calculating the hardness according to Example 2 is also shown in accordance with FIG. 6B shown in Example 1. The parts H1 to H4 whose hardness was predicted and measured in Example 2 were the same as those shown in FIG. 6 (b) is a diagram of comparison between the predicted and measured values of the hardness H B at the site H1-H4, plotted by solid black marker in the figure shows the results of Example 2. In an actual casting containing 0.4% by mass of Cu, the hardness becomes high due to the structure having a relatively large amount of hard pearlite phase, but this was predicted by Example 2 where Cu% = 0.4 was set. The hardness and the measured hardness were in good agreement, and the present invention was able to accurately predict the hardness of the spheroidal graphite cast iron casting.

ここで、実施例1及び実施例2で予測した硬度と実物の鋳物の硬度を比較すると、実物の鋳物の硬度は、鋳物工場Aの製品Aの硬度は低目となり、鋳物工場Bの製品Aの硬度は高目となっている。また同一の製品Aであっても、その部位によって硬度が相違している。図6(b)から分かるように、本発明の球状黒鉛鋳鉄鋳物の硬度の予測方法によれば、鋳物工場や部位によって相違する鋳物の硬度の高低差も含めて、これを精度よく予測できている。   Here, comparing the hardness predicted in Example 1 and Example 2 with the hardness of the actual casting, the hardness of the actual casting is lower than that of the product A of the foundry A, and the product A of the foundry B The hardness is high. Moreover, even if it is the same product A, hardness differs with the site | parts. As can be seen from FIG. 6 (b), according to the method for predicting the hardness of the spheroidal graphite cast iron casting of the present invention, it is possible to accurately predict this, including the difference in the hardness of the casting, which differs depending on the foundry and location. Yes.

(比較例1)鋳物工場A、製品A
比較例1は、実施例1と同一の鋳物工場Aで製造される同一の製品A(ステアリングナックル)に本発明の硬度を予測する方法を適用するにあたり、共析変態の冷却速度(第3の冷却速度)のみを考慮して硬度を予測した例である。比較例1では、化学成分値設定工程S3及び最高温度計算工程S5は実行せず、また、温度設定工程S4では第5の温度T5及び第6の温度T6のみを設定し、冷却速度計算工程S6では第3の冷却速度計算工程S63のみを実行した。
(Comparative example 1) Foundry A, product A
In Comparative Example 1, in applying the method of predicting the hardness of the present invention to the same product A (steering knuckle) manufactured in the same foundry A as in Example 1, the cooling rate of the eutectoid transformation (third This is an example in which the hardness is predicted considering only the cooling rate. In Comparative Example 1, the chemical component value setting step S3 and the maximum temperature calculation step S5 are not executed. In the temperature setting step S4, only the fifth temperature T5 and the sixth temperature T6 are set, and the cooling rate calculation step S6. Then, only the third cooling rate calculation step S63 was executed.

また、硬度計算工程S7では黒鉛粒数計算工程S71を実行せず、すなわち黒鉛粒数予測式(式5)の関数形の式(式7)を用いることなく、かつ硬度予測式を実行する工程S72での硬度Hの予測式(式4)の関数形の式(式6)のうち、定数ω及びαと第3の冷却速度Vのみを用いた関数形の式、すなわち
=ω+α (式8)
を使用して硬度計算工程S7を実行した。
Further, in the hardness calculation step S7, the graphite particle number calculation step S71 is not executed, that is, the hardness prediction equation is executed without using the functional equation (Equation 7) of the graphite particle number prediction equation (Equation 5). Of the functional formula (formula 6) of the prediction formula (formula 4) of the hardness H B in S72, the functional formula using only the constants ω and α 2 and the third cooling rate V 3 , that is, H B = Ω + α 2 V 3 (Formula 8)
Was used to execute the hardness calculation step S7.

比較例1では、表1及び表2に示すように(式8)の定数ω及びαを実施例1と同一に設定した以外は、(式6)及び(式7)の全ての定数を設定しなかった。また、表3に示すように化学成分値設定工程S3は実行しないので元素と各元素の質量%は設定しなかった。また、温度設定工程S4では第3の冷却速度計算工程S63で使用する第5の温度T5及び第6の温度T6のみを与え、表4に示すように実施例1と同じ値を用いた。また、冷却履歴解析工程S2において解析を終了する所定の温度TENDは、表4に示すように実施例1と同じ値を用いた。 In Comparative Example 1, except that Table 1 and Table 2 the constants ω and alpha 2 (Formula 8) was set in the same manner as in Example 1, all the constants of the equation (6) and (7) Not set. In addition, as shown in Table 3, the chemical component value setting step S3 was not executed, so the elements and the mass% of each element were not set. In the temperature setting step S4, only the fifth temperature T5 and the sixth temperature T6 used in the third cooling rate calculation step S63 were given, and the same values as in Example 1 were used as shown in Table 4. In addition, as the predetermined temperature T END that ends the analysis in the cooling history analysis step S2, the same value as in Example 1 was used as shown in Table 4.

共析変態の冷却速度(第3の冷却速度)のみを考慮した比較例による硬度の予測値と実物の硬度の実測値との比較を図12に示す。比較例1で硬度を予測及び実測した部位H1〜H4は、実施例1と同一の図6(a)に示す部位とした。図12は部位H1〜H4における硬度Hの予測値と実測値とを比較した図であり、図中の白抜きのマーカーによるプロットが比較例1の結果を示す。比較例1で予測した硬度は実測の硬度から大きく逸脱しており両者は一致しなかった。 FIG. 12 shows a comparison between the predicted hardness value and the actual hardness measurement value in the comparative example in consideration of only the eutectoid transformation cooling rate (third cooling rate). The parts H1 to H4 whose hardness was predicted and measured in Comparative Example 1 were the same as those shown in FIG. Figure 12 is a view of comparing the predicted and measured values of the hardness H B at the site H1-H4, are plotted by marker white in the figure shows the results of Comparative Example 1. The hardness predicted in Comparative Example 1 greatly deviated from the actually measured hardness, and the two did not match.

(比較例2)鋳物工場B、製品A
比較例2は、実施例2と同一の鋳物工場Bで製造される同一の製品A(ステアリングナックル)に本発明の硬度を予測する方法を適用するにあたり、共析変態の冷却速度(第3の冷却速度)のみを考慮して硬度を予測した例である。比較例2では、比較例1と同様に、化学成分値設定工程S3及び最高温度計算工程S5は実行せず、また、温度設定工程S4では第5の温度T5及び第6の温度T6のみを設定し、冷却速度計算工程S6では第3の冷却速度計算工程S63のみを実行した。
(Comparative example 2) Foundry B, product A
In Comparative Example 2, in applying the method of predicting the hardness of the present invention to the same product A (steering knuckle) manufactured in the same foundry B as in Example 2, the cooling rate of the eutectoid transformation (third This is an example in which the hardness is predicted considering only the cooling rate. In Comparative Example 2, as in Comparative Example 1, the chemical component value setting step S3 and the maximum temperature calculation step S5 are not executed, and only the fifth temperature T5 and the sixth temperature T6 are set in the temperature setting step S4. In the cooling rate calculation step S6, only the third cooling rate calculation step S63 was executed.

また、硬度計算工程S7では黒鉛粒数計算工程S71を実行せず、すなわち黒鉛粒数予測式(式5)の関数形の式(式7)を用いることなく、かつ硬度予測式を実行する工程S72での硬度Hの予測式の関数形の式は、比較例1と同一の(式8)を使用して硬度計算工程S7を実行した。 Further, in the hardness calculation step S7, the graphite particle number calculation step S71 is not executed, that is, the hardness prediction equation is executed without using the functional equation (Equation 7) of the graphite particle number prediction equation (Equation 5). hardness H equation functional form of the prediction equation of B in the S72, and executes the hardness calculating step S7 using Comparative example 1 the same and the (equation 8).

比較例2は、比較例1と同様に表1及び表2に示すように、(式8)の定数ω及びαを実施例1と同一に設定した以外は、(式6)及び(式7)の全ての定数を設定しなかった。また、表3に示すように元素と各元素の質量%は設定せず、表4に示すように第5の温度T5及び第6の温度T6並びに解析を終了する所定の温度TENDはいずれも実施例1と同じ値を用いた。 As in Comparative Example 1, Comparative Example 2 is similar to Comparative Example 1 except that constants ω and α 2 of (Equation 8) are set to be the same as those in Example 1, as shown in Table 1 and Table 2. All constants of 7) were not set. The mass% of the elements and each element as shown in Table 3 is not set, any given temperature T END to end the fifth temperature T5 and temperature T6 and analysis of the sixth, as shown in Table 4 The same values as in Example 1 were used.

比較例2により硬度を計算した結果を、比較例1で示した図12に合わせて同様に示す。比較例2で硬度を予測及び実測した部位H1〜H4は、実施例1と同一の図6(a)に示す部位とした。図12は部位H1〜H4における硬度Hの予測値と実測値とを比較した図であり、図中の黒く塗りつぶしたマーカーによるプロットが比較例2の結果を示す。比較例2で予測した硬度は実測の硬度から大きく逸脱しており両者は一致しなかった。 The result of calculating the hardness according to Comparative Example 2 is similarly shown in accordance with FIG. 12 shown in Comparative Example 1. The parts H1 to H4 whose hardness was predicted and measured in Comparative Example 2 were the same as those shown in FIG. Figure 12 is a view of comparing the predicted and measured values of the hardness H B at the site H1-H4, are plotted by solid black marker in the figure shows the results of Comparative Example 2. The hardness predicted in Comparative Example 2 greatly deviated from the actually measured hardness, and the two did not match.

ここで比較例1及び比較例2で予測した硬度と実物の鋳物の硬度を比較すると、実物の鋳物の硬度は、前述したように鋳物工場Aの製品Aと鋳物工場Bの製品Aでは硬度の高低差があるのに対して、比較例1及び比較例2で予測した硬度は、いずれも約150〜210Hの硬度範囲に入っており、実物の鋳物の硬度の高低差を予測できていない。しかも予測値は、実測値からの乖離が大きい。このように、共析変態の冷却速度のみを考慮した比較例では、実際の鋳物の硬度の予測精度が低い。 Here, comparing the hardness predicted in Comparative Example 1 and Comparative Example 2 with the hardness of the actual casting, the hardness of the actual casting is the hardness of the product A of the foundry A and the product A of the foundry B as described above. whereas there is a height difference, hardness predicted in Comparative example 1 and Comparative example 2 are both are contained in the hardness range of about 150~210H B, not been able to predict the height difference between the hardness of the real casting . Moreover, the predicted value has a large deviation from the actually measured value. Thus, in the comparative example which considered only the cooling rate of the eutectoid transformation, the prediction accuracy of the actual casting hardness is low.

Figure 2018062006
Figure 2018062006

Figure 2018062006
Figure 2018062006

Figure 2018062006
Figure 2018062006

Figure 2018062006
Figure 2018062006

1 凝固冷却曲線
2 過冷却
1 Solidification cooling curve 2 Supercooling

Claims (5)

球状黒鉛鋳鉄鋳物の硬度を予測する方法であって、
鋳物要素を含む解析モデルを作成する要素作成工程(S1)と、
球状黒鉛鋳鉄からなる溶湯が前記鋳物要素を流動し充填されて前記球状黒鉛鋳鉄の共析変態温度よりも低い温度に冷却されるまでの期間の前記鋳物要素の伝熱を経時的に解析して、前記鋳物要素の時刻と温度との組データを取得する冷却履歴解析工程(S2)と、
前記球状黒鉛鋳鉄の化学成分値を与える化学成分値設定工程(S3)と、
前記鋳物要素の冷却速度を計算するための設定温度を与える温度設定工程(S4)と、
前記鋳物要素の組データに基づいて前記鋳物要素の最高温度を求める最高温度計算工程(S5)と、
前記設定温度と前記組データとに基づいて、共晶凝固の冷却速度を計算する第1の冷却速度計算工程(S61)、共晶凝固後の冷却速度を計算する第2の冷却速度計算工程(S62)及び共析変態の冷却速度を計算する第3の冷却速度計算工程(S63)を含む冷却速度計算工程(S6)と、
前記最高温度、前記共晶凝固の冷却速度、前記共晶凝固後の冷却速度、前記共析変態の冷却速度及び前記化学成分値に基づいて、硬度予測式により前記鋳物要素の硬度を計算する硬度計算工程(S7)と
を有することを特徴とする球状黒鉛鋳鉄鋳物の硬度を予測する方法。
A method for predicting the hardness of a spheroidal graphite cast iron casting,
An element creation step (S1) for creating an analysis model including a casting element;
Analyzing the heat transfer of the casting element over time during the period from when the molten metal composed of spheroidal graphite cast iron flows and fills the casting element and is cooled to a temperature lower than the eutectoid transformation temperature of the spheroidal graphite cast iron. , A cooling history analysis step (S2) for acquiring set data of time and temperature of the casting element;
A chemical component value setting step (S3) for giving a chemical component value of the spheroidal graphite cast iron;
A temperature setting step (S4) for providing a set temperature for calculating the cooling rate of the casting element;
A maximum temperature calculation step (S5) for obtaining a maximum temperature of the casting element based on the set data of the casting element;
Based on the set temperature and the set data, a first cooling rate calculation step (S61) for calculating a cooling rate for eutectic solidification, and a second cooling rate calculation step for calculating a cooling rate after eutectic solidification ( A cooling rate calculation step (S6) including S62) and a third cooling rate calculation step (S63) for calculating the cooling rate of the eutectoid transformation;
Based on the maximum temperature, the cooling rate of the eutectic solidification, the cooling rate after the eutectic solidification, the cooling rate of the eutectoid transformation, and the chemical component value A method of predicting the hardness of the spheroidal graphite cast iron casting, comprising a calculation step (S7).
前記化学成分値設定工程(S3)で与える化学成分値は元素として少なくともC、Si、Cu及びMnを含む請求項1に記載の球状黒鉛鋳鉄鋳物の硬度を予測する方法。   The method for predicting the hardness of a spheroidal graphite cast iron casting according to claim 1, wherein the chemical component value given in the chemical component value setting step (S3) includes at least C, Si, Cu and Mn as elements. 前記硬度計算工程(S7)は、前記最高温度、前記共晶凝固の冷却速度及び少なくとも元素としてCとSiを含む化学成分値に基づいて前記鋳物要素の黒鉛粒数を計算する黒鉛粒数計算工程(S71)を含む請求項1又は請求項2に記載の球状黒鉛鋳鉄鋳物の硬度を予測する方法。   The hardness calculation step (S7) is a graphite particle number calculation step of calculating the number of graphite particles of the casting element based on the maximum temperature, the eutectic solidification cooling rate, and the chemical component value including at least C and Si as elements. The method for predicting the hardness of the spheroidal graphite cast iron casting according to claim 1 or 2, comprising (S71). 前記硬度計算工程(S7)は、前記共析変態の冷却速度と前記共晶凝固後の冷却速度との相対値の計算を含む請求項1乃至請求項3のいずれかに記載の球状黒鉛鋳鉄鋳物の硬度を予測する方法。   The spheroidal graphite cast iron casting according to any one of claims 1 to 3, wherein the hardness calculation step (S7) includes calculation of a relative value between a cooling rate of the eutectoid transformation and a cooling rate after the eutectic solidification. Of predicting hardness. 前記硬度計算工程(S7)で計算される鋳物要素の硬度を画像として出力する硬度出力工程(S8)を有する請求項1乃至請求項4のいずれかに記載の球状黒鉛鋳鉄鋳物の硬度を予測する方法。   The hardness of the spheroidal graphite cast iron casting according to any one of claims 1 to 4, further comprising a hardness output step (S8) for outputting the hardness of the cast element calculated in the hardness calculation step (S7) as an image. Method.
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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114528670A (en) * 2022-04-21 2022-05-24 潍柴动力股份有限公司 Method for detecting tensile strength of casting
CN117920967A (en) * 2024-01-25 2024-04-26 东莞市德辉玻璃有限公司 Die casting production process of intelligent lock

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002192328A (en) * 2000-12-22 2002-07-10 Suzuki Motor Corp Method of manufacturing spheroidal graphite cast iron casting
JP2008155230A (en) * 2006-12-21 2008-07-10 Nissan Motor Co Ltd Casting plan design method
JP2010052019A (en) * 2008-08-28 2010-03-11 Hitachi Metals Ltd Simulation method for sand mold casting

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2002192328A (en) * 2000-12-22 2002-07-10 Suzuki Motor Corp Method of manufacturing spheroidal graphite cast iron casting
JP2008155230A (en) * 2006-12-21 2008-07-10 Nissan Motor Co Ltd Casting plan design method
JP2010052019A (en) * 2008-08-28 2010-03-11 Hitachi Metals Ltd Simulation method for sand mold casting

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114528670A (en) * 2022-04-21 2022-05-24 潍柴动力股份有限公司 Method for detecting tensile strength of casting
CN114528670B (en) * 2022-04-21 2022-07-19 潍柴动力股份有限公司 Method for detecting tensile strength of casting
CN117920967A (en) * 2024-01-25 2024-04-26 东莞市德辉玻璃有限公司 Die casting production process of intelligent lock

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