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JP2013093461A - Deposition apparatus - Google Patents

Deposition apparatus Download PDF

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JP2013093461A
JP2013093461A JP2011235126A JP2011235126A JP2013093461A JP 2013093461 A JP2013093461 A JP 2013093461A JP 2011235126 A JP2011235126 A JP 2011235126A JP 2011235126 A JP2011235126 A JP 2011235126A JP 2013093461 A JP2013093461 A JP 2013093461A
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susceptor
plate portion
heat
substrate
forming apparatus
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Kenichiro Sakae
顕一郎 栄
Yasumasa Suzuki
康正 鈴木
Kenji Komuro
健司 小室
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Ulvac Inc
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Ulvac Inc
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Abstract

PROBLEM TO BE SOLVED: To provide a deposition apparatus which inhibits heat from escaping from a susceptor and prevents the damage by heat of a susceptor supporting member.SOLUTION: A deposition apparatus 10 heats a susceptor 21 with a heater 23 and introduces a material gas from a material gas introduction part 13 to a vacuum tank 11 to deposit a thin film on a substrate 51 disposed on a surface of the plate part 21a of the susceptor 21. A heat resistance member 22, which is made of a material different from the susceptor 21, is disposed between an end part of a cylinder part 21b of the susceptor 21 and the susceptor support member 31, and heat of the susceptor 21 is blocked by the heat resistance member 22 and thus is not easily transmitted to the susceptor support member 31.

Description

本発明は、基板を加熱しながら成膜する成膜装置に関する。   The present invention relates to a film forming apparatus for forming a film while heating a substrate.

現在、LEDは白熱電球に比べて消費電力が小さく、寿命が長いという特質を持ち、次世代照明として注目されている。LEDはサファイア基板上にn層と発光層とp層とからなる積層膜がエピタキシャル結晶成長により形成される。エピタキシャル成長にはMOVPE法(有機金属気相成長法)がよく用いられている。   Currently, LEDs have the characteristics of lower power consumption and longer life than incandescent bulbs, and are attracting attention as next-generation lighting. In an LED, a laminated film including an n layer, a light emitting layer, and a p layer is formed on a sapphire substrate by epitaxial crystal growth. MOVPE (metal organic vapor phase epitaxy) is often used for epitaxial growth.

図7はMOVPE法に用いられる従来の成膜装置100の内部構成図である。
従来の成膜装置100は、真空槽111と、真空槽111内を真空排気する真空排気部112と、真空槽111内に原料ガスを導入する原料ガス導入部113と、底部表面に基板151が載置される椀状のサセプタ121と、サセプタ121の内側に配置され、サセプタ121の底部裏面に対向されたヒーター123と、サセプタ121の底部側とは逆側の端部に設けられ、サセプタ121を支持するサセプタ支持部材131とを有している。
サセプタ121の材質はグラファイトであり、サセプタ支持部材131の材質は石英である。
FIG. 7 is an internal configuration diagram of a conventional film forming apparatus 100 used in the MOVPE method.
A conventional film forming apparatus 100 includes a vacuum chamber 111, a vacuum exhaust unit 112 that evacuates the vacuum chamber 111, a source gas introduction unit 113 that introduces a source gas into the vacuum chamber 111, and a substrate 151 on the bottom surface. A saddle-like susceptor 121 to be placed, a heater 123 disposed inside the susceptor 121 and opposed to the bottom rear surface of the susceptor 121, and provided at an end opposite to the bottom side of the susceptor 121, And a susceptor support member 131 that supports the susceptor.
The material of the susceptor 121 is graphite, and the material of the susceptor support member 131 is quartz.

この成膜装置100を用いて薄膜を形成するには、まず複数枚の基板151を真空槽111内に搬入し、サセプタ121の底部表面に配置する。
真空排気部112により真空槽111内を真空排気して真空雰囲気を形成する。以後真空排気を継続して真空槽111内の真空雰囲気を維持する。
In order to form a thin film using the film forming apparatus 100, first, a plurality of substrates 151 are carried into the vacuum chamber 111 and placed on the bottom surface of the susceptor 121.
The vacuum chamber 111 is evacuated by the evacuation unit 112 to form a vacuum atmosphere. Thereafter, evacuation is continued and the vacuum atmosphere in the vacuum chamber 111 is maintained.

ヒーター123には加熱用電源133が電気的に接続されている。加熱用電源133からヒーター123に電力を供給して、ヒーター123を発熱させる。
ヒーター123からの熱輻射によりサセプタ121が加熱され、サセプタ121からの熱伝導により基板151が加熱される。
原料ガス導入部113から真空槽111内に原料ガスを導入すると、導入された原料ガスは基板151上で熱により化学反応して結晶化し、薄膜が形成される。
A heating power source 133 is electrically connected to the heater 123. Electric power is supplied from the heating power supply 133 to the heater 123 to cause the heater 123 to generate heat.
The susceptor 121 is heated by heat radiation from the heater 123, and the substrate 151 is heated by heat conduction from the susceptor 121.
When the source gas is introduced into the vacuum chamber 111 from the source gas introduction unit 113, the introduced source gas is chemically reacted with heat on the substrate 151 to be crystallized to form a thin film.

基板151を加熱する工程では、サセプタ121の底部表面を900℃以上1300℃以下に加熱する必要があるのだが、サセプタ121の外周側面からの熱輻射やサセプタ支持部材131への熱伝導により熱が逃げるため、サセプタ121の底部表面では外周に近いほど温度が下がりやすく、基板151が配置される範囲内を温度差1℃以内の均一な温度に維持することは困難であった。また、サセプタ121のうち底部部分と側面部分の温度差が500℃以上になるとサセプタ121が破損するおそれがあった。   In the step of heating the substrate 151, it is necessary to heat the bottom surface of the susceptor 121 to 900 ° C. or more and 1300 ° C. or less. However, heat is generated by heat radiation from the outer peripheral side surface of the susceptor 121 or heat conduction to the susceptor support member 131. In order to escape, the temperature of the bottom surface of the susceptor 121 tends to decrease as it approaches the outer periphery, and it is difficult to maintain a uniform temperature within a temperature difference of 1 ° C. within the range where the substrate 151 is disposed. Further, when the temperature difference between the bottom portion and the side surface portion of the susceptor 121 is 500 ° C. or more, the susceptor 121 may be damaged.

そこで、ヒーター123のうち側面部分に近い位置のヒーターの負荷を大きくして、サセプタ121の側面部分の温度を上げる方法が考えられるが、サセプタ支持部材131の材質は石英であり、900℃以上のサセプタ121と接触するとサセプタ支持部材131が熱で破損するおそれがあった。   Therefore, a method of increasing the load of the heater near the side surface portion of the heater 123 and increasing the temperature of the side surface portion of the susceptor 121 can be considered. However, the material of the susceptor support member 131 is quartz, which is 900 ° C. or higher. When contacting with the susceptor 121, the susceptor support member 131 may be damaged by heat.

特開2011−18811号公報JP 2011-18811 A 再公表特許2008/016047号公報Republished Patent 2008/016047 再公表特許2007/066472号公報Republished Patent No. 2007/066642

本発明は上記従来技術の不都合を解決するために創作されたものであり、その目的は、サセプタからの熱逃げが抑制され、かつサセプタ支持部材の熱による破損を防止できる成膜装置を提供することにある。   The present invention was created to solve the above-described disadvantages of the prior art, and an object of the present invention is to provide a film forming apparatus in which heat escape from the susceptor is suppressed and damage to the susceptor support member can be prevented. There is.

上記課題を解決するために本発明は、真空槽と、前記真空槽内を真空排気する真空排気部と、前記真空槽内に原料ガスを導入する原料ガス導入部と、前記真空槽内に配置され、表面に基板が配置される板部と、前記板部の前記表面とは逆の裏面で一端の開口が蓋された筒部とからなるサセプタと、前記筒部の内側に配置され、前記板部の前記裏面と前記筒部の内周面とにそれぞれ対向されたヒーターと、前記筒部の前記一端とは逆の他端に設けられ、前記サセプタを支持するサセプタ支持部材と、を有し、前記ヒーターによって前記サセプタを加熱し、前記原料ガス導入部から前記真空槽内に原料ガスを導入し、前記板部の前記表面に配置された基板に薄膜を形成する成膜装置であって、前記筒部の前記他端と前記サセプタ支持部材との間には、前記サセプタとは別の材質である熱抵抗部材が配置された成膜装置である。
本発明は成膜装置であって、前記熱抵抗部材の線膨張率は前記サセプタの線膨張率より小さく、前記熱抵抗部材の熱伝導率は前記サセプタの熱伝導率より小さい成膜装置である。
本発明は成膜装置であって、前記サセプタの材質はグラファイトであり、前記熱抵抗部材の材質はSiCである成膜装置である。
本発明は成膜装置であって、前記板部のうち、前記基板が配置される範囲より外側には、前記基板が配置される範囲の厚みより厚みが薄い熱抵抗部分が環状に設けられた成膜装置である。
本発明は成膜装置であって、前記板部と前記筒部は分離可能に構成された成膜装置である。
本発明は成膜装置であって、前記板部は、900℃以上1300℃以下に加熱される成膜装置である。
In order to solve the above-described problems, the present invention provides a vacuum chamber, a vacuum exhaust unit that evacuates the vacuum chamber, a source gas introduction unit that introduces a source gas into the vacuum chamber, and a vacuum chamber disposed in the vacuum chamber. And a susceptor comprising a plate portion on which a substrate is disposed, and a cylinder portion having an opening at one end on the back surface opposite to the surface of the plate portion, and disposed inside the tube portion, A heater opposed to the back surface of the plate portion and the inner peripheral surface of the cylinder portion; and a susceptor support member provided at the other end opposite to the one end of the cylinder portion and supporting the susceptor. A film forming apparatus that heats the susceptor with the heater, introduces a source gas into the vacuum chamber from the source gas introduction unit, and forms a thin film on the substrate disposed on the surface of the plate unit; , Between the other end of the cylindrical portion and the susceptor support member A deposition apparatus the heat resistance member is disposed is another material from said susceptor.
The present invention is a film forming apparatus, wherein the thermal resistance member has a smaller linear expansion coefficient than the susceptor, and the thermal resistance member has a smaller thermal conductivity than the susceptor. .
The present invention is a film forming apparatus, wherein the material of the susceptor is graphite and the material of the heat resistance member is SiC.
This invention is a film-forming apparatus, Comprising: On the outer side of the range in which the said board | substrate is arrange | positioned among the said board parts, the heat resistance part thinner than the thickness of the range in which the said board | substrate is arrange | positioned was cyclically | annularly provided. A film forming apparatus.
This invention is a film-forming apparatus, Comprising: The said board part and the said cylinder part are film-forming apparatuses comprised so that separation | separation was possible.
This invention is a film-forming apparatus, Comprising: The said board part is a film-forming apparatus heated at 900 degreeC or more and 1300 degrees C or less.

サセプタからの熱逃げが抑制されるので、板部のうち基板が配置される範囲内を均一な温度に維持することができる。そのため、各基板に形成される薄膜の膜質差が小さくなり、歩留まりが向上する。   Since heat escape from the susceptor is suppressed, it is possible to maintain a uniform temperature within a range where the substrate is disposed in the plate portion. Therefore, the film quality difference between the thin films formed on each substrate is reduced, and the yield is improved.

サセプタ支持部材に熱が伝わりにくくなるため、サセプタ支持部材の熱による破損を防止できる。サセプタ支持部材の熱破損をおそれずに筒部を加熱することができ、筒部と板部との温度差を小さくして、板部からの熱逃げを防止できる。   Since it becomes difficult for heat to be transmitted to the susceptor support member, damage to the susceptor support member due to heat can be prevented. The cylindrical portion can be heated without fear of thermal damage to the susceptor support member, and the temperature difference between the cylindrical portion and the plate portion can be reduced to prevent heat escape from the plate portion.

本発明の成膜装置の内部構成図Internal configuration diagram of film forming apparatus of the present invention サセプタの板部の裏面の平面図Top view of the back side of the susceptor plate 熱抵抗部分の断面形状の別例を説明をするための図The figure for demonstrating another example of the cross-sectional shape of a thermal resistance part 熱抵抗部分と接触部との位置関係の別例を説明するための図The figure for demonstrating another example of the positional relationship of a thermal-resistance part and a contact part. サセプタの板部と筒部とが分離された状態を説明するための図The figure for demonstrating the state from which the board part and cylinder part of the susceptor were isolate | separated 本発明の成膜装置の別例の内部構成図Another internal configuration diagram of the film forming apparatus of the present invention 従来の成膜装置の内部構成図Internal configuration diagram of conventional film deposition system

<成膜装置の構造>
本発明の成膜装置の構造を説明する。
図1は成膜装置10の内部構成図である。
<Structure of deposition system>
The structure of the film forming apparatus of the present invention will be described.
FIG. 1 is an internal configuration diagram of the film forming apparatus 10.

成膜装置10は、真空槽11と、真空槽11内を真空排気する真空排気部12と、真空槽11内に原料ガスを導入する原料ガス導入部13と、真空槽11内に配置され、表面に基板51が配置される板部21aと、板部21aの表面とは逆の裏面で一端の開口が蓋された筒部21bとからなるサセプタ21と、筒部21bの内側に配置され、板部21aの裏面と筒部21bの内周面とにそれぞれ対向されたヒーター23と、筒部21bの前記一端とは逆の他端に設けられ、サセプタ21を支持するサセプタ支持部材31とを有している。   The film forming apparatus 10 is disposed in the vacuum chamber 11, a vacuum exhaust unit 12 that evacuates the vacuum chamber 11, a source gas introduction unit 13 that introduces a source gas into the vacuum chamber 11, and the vacuum chamber 11. A susceptor 21 including a plate portion 21a on which the substrate 51 is arranged, a cylinder portion 21b whose end is covered with a back surface opposite to the surface of the plate portion 21a, and an inner side of the cylinder portion 21b. A heater 23 opposed to the back surface of the plate portion 21a and the inner peripheral surface of the cylinder portion 21b, and a susceptor support member 31 that is provided at the other end opposite to the one end of the cylinder portion 21b and supports the susceptor 21. Have.

原料ガス導入部13はここでは、一面に複数の放出孔13cが設けられた放出容器13aと、放出容器13aに接続され、放出容器13a内に原料ガスを供給する原料ガス源13bとを有している。
放出容器13aのうち、放出孔13cが設けられた面は真空槽11内に露出されており、原料ガス源13bから放出容器13a内に原料ガスを供給すると、供給された原料ガスは各放出孔13cから真空槽11内に放出されるようになっている。
Here, the raw material gas introduction unit 13 includes a discharge container 13a having a plurality of discharge holes 13c provided on one surface, and a raw material gas source 13b connected to the discharge container 13a and supplying the raw material gas into the discharge container 13a. ing.
Of the discharge container 13a, the surface provided with the discharge hole 13c is exposed in the vacuum chamber 11, and when the source gas is supplied into the discharge container 13a from the source gas source 13b, the supplied source gas is supplied to each discharge hole. 13c is discharged into the vacuum chamber 11.

サセプタ21の材質はここでは表面がSiCで覆われたグラファイトであり、900℃以上1300℃以下の温度に加熱されても損傷しないようになっている。なお、グラファイトの350℃以上400℃以下の温度範囲での線膨張率は5.0×10-6/Kであり、熱伝導率は130W/(m・K)である。 Here, the material of the susceptor 21 is graphite whose surface is covered with SiC, and is not damaged even when heated to a temperature of 900 ° C. or higher and 1300 ° C. or lower. Note that the linear expansion coefficient of graphite in the temperature range of 350 ° C. to 400 ° C. is 5.0 × 10 −6 / K, and the thermal conductivity is 130 W / (m · K).

図2は板部21aの裏面の平面図である。
板部21aはここでは円板形状であり、表面に複数枚の基板51が配置される範囲が設けられた基板配置部45を有している。
FIG. 2 is a plan view of the back surface of the plate portion 21a.
Here, the plate portion 21a has a disk shape, and has a substrate placement portion 45 provided with a range in which a plurality of substrates 51 are placed on the surface.

また、板部21aの裏面のうち基板配置部45より外側の外周部分には後述する筒部21bの長手方向の一端と環状に接触できる環状の接触部46が設けられている。図1を参照し、接触部46の厚みは基板配置部45の厚みと同じか基板配置部45の厚みより薄くされている。   In addition, an annular contact portion 46 that can be annularly contacted with one end in the longitudinal direction of a cylindrical portion 21b described later is provided on the outer peripheral portion of the back surface of the plate portion 21a outside the substrate placement portion 45. Referring to FIG. 1, the thickness of contact portion 46 is the same as the thickness of substrate placement portion 45 or thinner than the thickness of substrate placement portion 45.

板部21aは放出容器13aの放出孔13cが設けられた面と対面する位置に配置され、板部21aの表面は放出孔13cが設けられた面と対向されている。
筒部21bはここでは内周直径が板部21aの直径より小さい円筒形状であり、中心軸線が板部21aの中心を通り板部21aの表面に対して直角な中心軸線と一致された状態で、長手方向の一端が板部21aの裏面の接触部46に環状に接触されて取り付けられ、筒部21bの一端の開口は板部21aの裏面で蓋されている。
The plate portion 21a is disposed at a position facing the surface provided with the discharge hole 13c of the discharge container 13a, and the surface of the plate portion 21a is opposed to the surface provided with the discharge hole 13c.
Here, the cylindrical portion 21b has a cylindrical shape whose inner peripheral diameter is smaller than the diameter of the plate portion 21a, and the central axis passes through the center of the plate portion 21a and is aligned with the central axis perpendicular to the surface of the plate portion 21a. One end in the longitudinal direction is attached in an annular contact with the contact portion 46 on the back surface of the plate portion 21a, and the opening at one end of the tube portion 21b is covered with the back surface of the plate portion 21a.

サセプタ支持部材31の材質はここでは石英であり、筒形状に形成されている。
筒部21bのうち板部21aとは逆側の端部には後述する熱抵抗部材22が固定され、サセプタ支持部材31は、中心軸線が筒部21bの中心軸線と一致された状態で、長手方向の一端が熱抵抗部材22に固定されている。
The material of the susceptor support member 31 is quartz here, and is formed in a cylindrical shape.
A thermal resistance member 22 to be described later is fixed to an end portion of the cylindrical portion 21b opposite to the plate portion 21a, and the susceptor support member 31 has a longitudinal axis in a state where the central axis coincides with the central axial line of the cylindrical portion 21b. One end of the direction is fixed to the heat resistance member 22.

サセプタ支持部材31のうち熱抵抗部材22とは逆側の端部は、真空槽11の壁面に設けられた開口を通って真空槽11の外側まで延ばされており、サセプタ支持部材31の当該端部には、サセプタ支持部材31を回転させる回転部32が接続されている。   The end of the susceptor support member 31 opposite to the heat resistance member 22 is extended to the outside of the vacuum chamber 11 through an opening provided in the wall surface of the vacuum chamber 11, and the susceptor support member 31 A rotating portion 32 that rotates the susceptor support member 31 is connected to the end portion.

回転部32はここではモーターであり、動力をサセプタ支持部材31に伝達して、サセプタ支持部材31をサセプタ支持部材31の中心軸線を中心に回転できるように構成されている。
回転部32によりサセプタ支持部材31を回転させると、サセプタ21と熱抵抗部材22もサセプタ支持部材31と一緒にサセプタ支持部材31の中心軸線を中心に回転するようになっている。
Here, the rotating unit 32 is a motor, and is configured to transmit power to the susceptor support member 31 so that the susceptor support member 31 can rotate about the central axis of the susceptor support member 31.
When the susceptor support member 31 is rotated by the rotating portion 32, the susceptor 21 and the heat resistance member 22 are also rotated around the central axis of the susceptor support member 31 together with the susceptor support member 31.

真空槽11の壁面の開口とサセプタ支持部材31の外周側面との間の隙間には磁気シール34が配置されて隙間は塞がれており、サセプタ支持部材31を回転させても真空槽11の気密性が維持されるようになっている。   A magnetic seal 34 is disposed in the gap between the opening of the wall surface of the vacuum chamber 11 and the outer peripheral side surface of the susceptor support member 31 so that the gap is closed. Even if the susceptor support member 31 is rotated, Airtightness is maintained.

ヒーター23はここでは、円板形状の第一のヒーター23aと、内周直径が第一のヒーター23aの直径より大きいリング状の第二のヒーター23bと、内周直径が第二のヒーター23bの外周直径より大きい筒状の第三のヒーター23cとを有している。第三のヒーター23cの長手方向の長さは、筒部21bの長手方向の長さより短くされている。   Here, the heater 23 includes a disk-shaped first heater 23a, a ring-shaped second heater 23b having an inner peripheral diameter larger than the diameter of the first heater 23a, and an inner peripheral diameter of the second heater 23b. It has a cylindrical third heater 23c larger than the outer diameter. The length of the third heater 23c in the longitudinal direction is shorter than the length of the cylindrical portion 21b in the longitudinal direction.

第一〜第三のヒーター23a〜23cは、それぞれの中心軸線が一致された状態で、筒部21bの内側に配置され、第一、第二のヒーター23a、23bの表面は板部21aの裏面とそれぞれ対面され、第三のヒーター23cの外周側面は筒部21bの内周面と対面されている。   The first to third heaters 23a to 23c are arranged on the inner side of the cylindrical portion 21b in a state where the respective central axes are aligned, and the surfaces of the first and second heaters 23a and 23b are the back surfaces of the plate portion 21a. The outer peripheral side surface of the third heater 23c faces the inner peripheral surface of the cylindrical portion 21b.

第一〜第三のヒーター23a〜23cは板部21aと筒部21bとからそれぞれ離間されており、回転部32によりサセプタ21を回転させても、第一〜第三のヒーター23a〜23cは真空槽11に対して静止するようになっている。   The first to third heaters 23a to 23c are separated from the plate portion 21a and the cylinder portion 21b, respectively. Even if the susceptor 21 is rotated by the rotating portion 32, the first to third heaters 23a to 23c are vacuumed. It is designed to be stationary with respect to the tank 11.

第一〜第三のヒーター23a〜23cには加熱用電源33が電気的に接続されている。加熱用電源33から第一〜第三のヒーター23a〜23cに電力を供給すると、第一〜第三のヒーター23a〜23cは発熱して輻射熱を放出するようになっている。板部21aの裏面と筒部21bの内周面は放出された輻射熱を受けるとそれぞれ加熱される。   A heating power source 33 is electrically connected to the first to third heaters 23a to 23c. When power is supplied from the heating power source 33 to the first to third heaters 23a to 23c, the first to third heaters 23a to 23c generate heat and emit radiant heat. The back surface of the plate portion 21a and the inner peripheral surface of the tube portion 21b are heated when they receive the emitted radiant heat.

第一、第二のヒーター23a、23bと板部21aの裏面との間の間隔と、第三のヒーター23cと筒部21bの内周面との間の間隔はそれぞれ狭いほど、輻射熱による加熱効率が大きいため好ましい。   The heating efficiency by radiant heat is so small that the space | interval between the 1st, 2nd heater 23a, 23b and the back surface of the board part 21a and the space | interval between the 3rd heater 23c and the internal peripheral surface of the cylinder part 21b are respectively narrow. Is preferable because of a large value.

板部21aは中心からの距離に応じて異なる複数のヒーターで加熱されることにより、板部21aのうち基板配置部45より外側の外周部分から熱が失われやすい場合でも、外周側のヒーター(ここでは第二のヒーター23b)の出力を増加させれば、基板配置部45内を均一な温度に加熱できるようになっている。   The plate portion 21a is heated by a plurality of different heaters depending on the distance from the center, so that even if heat is easily lost from the outer peripheral portion outside the substrate placement portion 45 of the plate portion 21a, the outer peripheral heater ( Here, if the output of the second heater 23b) is increased, the inside of the substrate placement portion 45 can be heated to a uniform temperature.

板部21aが第一、第二のヒーター23a、23bにより加熱されるだけでなく、筒部21bも第三のヒーター23cにより加熱されることにより、板部21aと筒部21bの温度差を小さくすることができ、板部21aから筒部21bに移動する熱量を少なくできる。   Not only is the plate portion 21a heated by the first and second heaters 23a and 23b, but the cylindrical portion 21b is also heated by the third heater 23c, thereby reducing the temperature difference between the plate portion 21a and the cylindrical portion 21b. It is possible to reduce the amount of heat transferred from the plate portion 21a to the tube portion 21b.

筒部21bのうち板部21a側とは逆側の端部とサセプタ支持部材31との間には、サセプタ21とは別の材質である熱抵抗部材22が配置されている。
熱抵抗部材22の材質はここではSiC(炭化ケイ素)であり、1300℃以上の高温に加熱されても損傷しないようになっている。なお、SiCの25℃(室温)以上400℃以下の温度範囲での線膨張率は4.0×10-6/Kであり、熱伝導率は84W/(m・K)である。
A thermal resistance member 22, which is a material different from the susceptor 21, is disposed between the end of the cylinder portion 21 b opposite to the plate portion 21 a side and the susceptor support member 31.
Here, the material of the heat resistance member 22 is SiC (silicon carbide), and is not damaged even when heated to a high temperature of 1300 ° C. or higher. The linear expansion coefficient of SiC in the temperature range of 25 ° C. (room temperature) to 400 ° C. is 4.0 × 10 −6 / K, and the thermal conductivity is 84 W / (m · K).

熱抵抗部材22の形状はここではリング状の板であり、表面はサセプタ21の筒部21bの一端に環状に接触して固定され、裏面はサセプタ支持部材31の一端に環状に接触して固定されている。   Here, the shape of the heat resistance member 22 is a ring-shaped plate, the front surface is annularly contacted and fixed to one end of the cylindrical portion 21 b of the susceptor 21, and the rear surface is annularly contacted and fixed to one end of the susceptor support member 31. Has been.

熱抵抗部材22と筒部21bとの接触面積は、サセプタ支持部材31と筒部21bとの接触面積より大きく、ここではサセプタ支持部材31と筒部21bとは非接触にされている。   The contact area between the thermal resistance member 22 and the cylinder part 21b is larger than the contact area between the susceptor support member 31 and the cylinder part 21b. Here, the susceptor support member 31 and the cylinder part 21b are not in contact with each other.

900℃以上1300℃以下の温度範囲での熱抵抗部材22の線膨張率はサセプタ21の線膨張率より小さくされており、熱抵抗部材22が第三のヒーター23cからの熱輻射や筒部21bからの熱伝導により加熱されても、熱抵抗部材22と筒部21bとの間の固定部分や熱抵抗部材22とサセプタ支持部材31との間の固定部分が緩まないようになっている。   The linear expansion coefficient of the thermal resistance member 22 in the temperature range of 900 ° C. or higher and 1300 ° C. or lower is made smaller than the linear expansion coefficient of the susceptor 21, and the thermal resistance member 22 generates heat radiation from the third heater 23c or the cylinder portion 21b. Even if it is heated by heat conduction from, the fixed portion between the heat resistance member 22 and the cylindrical portion 21b and the fixed portion between the heat resistance member 22 and the susceptor support member 31 are not loosened.

また、900℃以上1300℃以下の温度範囲での熱抵抗部材22の熱伝導率はサセプタ21の熱伝導率より小さくされており、筒部21bの熱は熱抵抗部材22に遮られてサセプタ支持部材31に伝わりにくくなっている。そのため、第三のヒーター23cにより筒部21bが加熱されても、サセプタ支持部材31が熱により損傷することが防止される。   In addition, the thermal conductivity of the thermal resistance member 22 in the temperature range of 900 ° C. or higher and 1300 ° C. or lower is smaller than the thermal conductivity of the susceptor 21, and the heat of the cylindrical portion 21 b is blocked by the thermal resistance member 22 to support the susceptor. It is difficult to be transmitted to the member 31. Therefore, even if the cylinder part 21b is heated by the third heater 23c, the susceptor support member 31 is prevented from being damaged by heat.

また、サセプタ支持部材31と第三のヒーター23cとの間の距離は熱抵抗部材22の厚みだけ余分に離間されており、第三のヒーター23cの熱輻射がサセプタ支持部材31に伝わりにくくなっている。   Further, the distance between the susceptor support member 31 and the third heater 23c is excessively separated by the thickness of the heat resistance member 22, and the heat radiation of the third heater 23c is not easily transmitted to the susceptor support member 31. Yes.

本実施例ではサセプタ21の材質はグラファイトであり、熱抵抗部材22の材質はSiCであるが、900℃以上1300℃以下の温度範囲での線膨張率がサセプタ21の線膨張率より小さく、900℃以上1300℃以下の温度範囲での熱伝導率がサセプタ21の熱伝導率より小さければ、熱抵抗部材22の材質はSiCに限定されず、例えばPBN(熱分解窒化ホウ素)でもよい。できるだけ900℃以上1300℃以下の温度範囲での線膨張率の小さい材料が好ましい。   In this embodiment, the material of the susceptor 21 is graphite and the material of the heat resistance member 22 is SiC. However, the linear expansion coefficient in the temperature range of 900 ° C. or higher and 1300 ° C. or lower is smaller than the linear expansion coefficient of the susceptor 21. If the thermal conductivity in the temperature range of not lower than 1 ° C. and lower than 1300 ° C. is smaller than the thermal conductivity of the susceptor 21, the material of the thermal resistance member 22 is not limited to SiC, and may be, for example, PBN (pyrolytic boron nitride). A material with a low coefficient of linear expansion in the temperature range of 900 ° C. or higher and 1300 ° C. or lower is preferable.

なお、熱抵抗部材22の形状はリング状に限定されるものではない。各ヒーター23a〜23cとサセプタ支持部材31との間を遮蔽する形状であれば、各ヒーター23a〜23cからの熱輻射によりサセプタ支持部材31が加熱されることを防止できて好ましい。   The shape of the heat resistance member 22 is not limited to a ring shape. If it is the shape which shields between each heater 23a-23c and the susceptor support member 31, it can prevent that the susceptor support member 31 is heated by the thermal radiation from each heater 23a-23c, and is preferable.

本実施例では、サセプタ21の板部21aのうち、基板配置部45より外側には、基板配置部45の厚みより厚みが薄い熱抵抗部分41が環状に設けられている。
ここでは熱抵抗部分41は、板部21aのうち、裏面側が窪む形状で設けられているが、表面側が窪む形状で設けられていてもよいし、表面側と裏面側の両方から窪む形状で設けられていてもよい。窪みの断面形状は、ここでは図1に示すように「コ」字形状(一辺が欠けた四角形状)であるが、図3に示すように「U」字形状(円弧形状)でもよい。
In the present embodiment, a thermal resistance portion 41 having a thickness smaller than the thickness of the substrate placement portion 45 is annularly provided outside the substrate placement portion 45 in the plate portion 21 a of the susceptor 21.
Here, the thermal resistance portion 41 is provided in a shape in which the back surface side is recessed in the plate portion 21a, but may be provided in a shape in which the front surface side is recessed, or is recessed from both the front surface side and the back surface side. It may be provided in a shape. Here, the cross-sectional shape of the depression is a “U” shape (a square shape with one side missing) as shown in FIG. 1, but may be a “U” shape (an arc shape) as shown in FIG. 3.

また、ここでは熱抵抗部分41は接触部46の内周より内側に設けられているが、図4に示すように熱抵抗部分41の一部が接触部46にされていてもよい。
基板配置部45内から基板配置部45より外側の外周部分に向かって径方向に移動する熱に対して、熱抵抗部分41では基板配置部45よりも厚みが薄いために熱のコンダクタンスが小さくなっており、熱の移動速度が低下するようになっている。
Here, although the thermal resistance portion 41 is provided on the inner side of the inner periphery of the contact portion 46, a part of the thermal resistance portion 41 may be made into the contact portion 46 as shown in FIG. 4.
With respect to the heat that moves in the radial direction from the inside of the substrate placement portion 45 toward the outer peripheral portion outside the substrate placement portion 45, the thermal resistance portion 41 is thinner than the substrate placement portion 45, so that the thermal conductance is reduced. Therefore, the speed of heat transfer is reduced.

そのため、基板配置部45内から熱が逃げにくく、基板配置部45内はヒーター23で加熱されることにより均一な温度に維持できるようになっている。
本実施例では、サセプタ21の板部21aと筒部21bは分離可能に構成されている。図5は板部21aと筒部21bとが分離された状態の概略図である。板部21aの接触部46は板部21aと筒部21bとの間の切れ目になっている。
Therefore, it is difficult for heat to escape from the inside of the substrate placement portion 45, and the inside of the substrate placement portion 45 can be maintained at a uniform temperature by being heated by the heater 23.
In the present embodiment, the plate portion 21a and the cylindrical portion 21b of the susceptor 21 are configured to be separable. FIG. 5 is a schematic view showing a state where the plate portion 21a and the cylindrical portion 21b are separated. The contact portion 46 of the plate portion 21a is a cut between the plate portion 21a and the cylindrical portion 21b.

そのため、板部21aと筒部21bとが一体に形成されて切れ目が存在しない場合に比べて、板部21aと筒部21bとの接触面積が小さく、板部21aから筒部21bに向かって移動する熱に対して熱のコンダクタンスが小さくなっており、板部21aのうち基板配置部45より外側の外周部分から熱が逃げにくくなっている。   Therefore, compared to the case where the plate portion 21a and the cylinder portion 21b are integrally formed and there is no cut, the contact area between the plate portion 21a and the cylinder portion 21b is small and moves from the plate portion 21a toward the cylinder portion 21b. The heat conductance is small with respect to the heat to be generated, and it is difficult for heat to escape from the outer peripheral portion of the plate portion 21a outside the substrate placement portion 45.

接触部46が板部21aの裏面の外周まで延ばされている場合には、接触部46の厚みが薄いほど板部21aの外周側面の面積が小さくなるため、板部21aの外周側面からの熱輻射が少なくなり、板部21aのうち基板配置部45より外側の外周部分からはさらに熱が逃げにくくなって好ましい。   When the contact part 46 is extended to the outer periphery of the back surface of the plate part 21a, the area of the outer peripheral side surface of the plate part 21a becomes smaller as the thickness of the contact part 46 becomes thinner. Thermal radiation is reduced, and heat is more difficult to escape from the outer peripheral portion of the plate portion 21a outside the substrate placement portion 45, which is preferable.

また後述する成膜工程により板部21a表面に付着物が付着して汚れても、板部21aと筒部21bは分離可能であり、成膜工程後に板部21aだけを真空槽11の外側に搬出して洗浄したり、別の板部21aに交換することができるため、メンテナンスが容易である。   In addition, even if deposits adhere to the surface of the plate part 21a by the film forming process described later, the plate part 21a and the cylinder part 21b can be separated, and only the plate part 21a is placed outside the vacuum chamber 11 after the film forming process. Since it can be carried out and washed, or replaced with another plate portion 21a, maintenance is easy.

<成膜装置を用いた成膜方法>
上述の成膜装置10を用いて基板51に薄膜を形成する成膜方法を説明する。
真空槽11内に基板51を搬入し、サセプタ21の板部21aのうち基板配置部45表面に接触して、基板51を配置する。本実施例では基板51にサファイア基板を使用するが、本発明は基板51の材質がサファイアの場合に限定されない。
<Film Forming Method Using Film Forming Apparatus>
A film forming method for forming a thin film on the substrate 51 using the film forming apparatus 10 will be described.
The substrate 51 is carried into the vacuum chamber 11, and the substrate 51 is placed in contact with the surface of the substrate placement portion 45 in the plate portion 21 a of the susceptor 21. In this embodiment, a sapphire substrate is used as the substrate 51, but the present invention is not limited to the case where the material of the substrate 51 is sapphire.

真空排気部12により真空槽11内を真空排気して、真空雰囲気を形成する。以後、真空排気部12による真空排気を継続して、真空槽11内の真空雰囲気を維持する。
回転部32によりサセプタ21をサセプタ支持部材31と熱抵抗部材22と一緒に、サセプタ支持部材31の中心軸線を中心に回転させる。すると、基板51もサセプタ21と一緒にサセプタ支持部材31の中心軸線を中心に回転する。以後、回転部32によるサセプタ21の回転を継続する。
The vacuum chamber 11 is evacuated by the evacuation unit 12 to form a vacuum atmosphere. Thereafter, evacuation by the evacuation unit 12 is continued, and the vacuum atmosphere in the vacuum chamber 11 is maintained.
The susceptor 21 is rotated about the central axis of the susceptor support member 31 together with the susceptor support member 31 and the heat resistance member 22 by the rotating unit 32. Then, the substrate 51 also rotates around the central axis of the susceptor support member 31 together with the susceptor 21. Thereafter, the rotation of the susceptor 21 by the rotating unit 32 is continued.

加熱用電源33から第一〜第三のヒーター23a〜23cに電力を供給して、第一〜第三のヒーター23a〜23cを発熱させる。
サセプタ21の板部21aの裏面と筒部21bの内周面のうち第一〜第三のヒーター23a〜23cと対面する部分は、第一〜第三のヒーター23a〜23cからの輻射熱を受けて加熱される。サセプタ21は回転部32により回転されており、第一〜第三のヒーター23a〜23cの配置に関わらずサセプタ21のうちサセプタ支持部材31の中心軸線から同一距離の部分は均一な熱量で加熱される。
Electric power is supplied from the heating power source 33 to the first to third heaters 23a to 23c to cause the first to third heaters 23a to 23c to generate heat.
The portion of the inner surface of the susceptor 21 that faces the first to third heaters 23a to 23c receives the radiant heat from the first to third heaters 23a to 23c. Heated. The susceptor 21 is rotated by a rotating unit 32, and a portion of the susceptor 21 that is the same distance from the central axis of the susceptor support member 31 is heated with a uniform amount of heat regardless of the arrangement of the first to third heaters 23a to 23c. The

板部21aの内部では熱伝導により裏面から表面に向かって熱が伝わる。ここでは板部21a表面が900℃以上1300℃以下になるように加熱する。基板51は板部21a表面に接触して配置されており、板部21a表面からの熱伝導により基板51が加熱される。
筒部21b内部でも熱伝導により内周面から外周面に向かって熱が伝わる。
Inside the plate portion 21a, heat is transferred from the back surface to the front surface by heat conduction. Here, heating is performed so that the surface of the plate portion 21a is 900 ° C. or higher and 1300 ° C. or lower. The substrate 51 is disposed in contact with the surface of the plate portion 21a, and the substrate 51 is heated by heat conduction from the surface of the plate portion 21a.
Even inside the cylinder portion 21b, heat is transmitted from the inner peripheral surface to the outer peripheral surface by heat conduction.

板部21aの外周側面と筒部21bの外周面は真空槽11内に露出されており、板部21aの外周側面と筒部21bの外周側面から熱輻射により熱が失われるものの、筒部21bとサセプタ支持部材31との間には熱抵抗部材22が配置され、筒部21bの熱は熱抵抗部材22に遮られてサセプタ支持部材31に逃げにくくなっている。そのため、筒部21bの温度低下が熱抵抗部材22を持たない従来の構成より抑制され、板部21aと筒部21bとの温度差を従来の構成より小さくでき、板部21aから筒部21bへの熱伝導による熱逃げを防止できる。
また、筒部21bからの熱伝導によるサセプタ支持部材31の加熱が抑制され、サセプタ支持部材31が熱により損傷することを防止できる。
Although the outer peripheral side surface of the plate portion 21a and the outer peripheral surface of the cylindrical portion 21b are exposed in the vacuum chamber 11, heat is lost by heat radiation from the outer peripheral side surface of the plate portion 21a and the outer peripheral side surface of the cylindrical portion 21b. The heat resistance member 22 is disposed between the susceptor support member 31 and the heat of the cylindrical portion 21b is blocked by the heat resistance member 22 so that it is difficult for the susceptor support member 31 to escape. Therefore, the temperature drop of the cylinder part 21b is suppressed from the conventional structure which does not have the heat resistance member 22, and the temperature difference between the plate part 21a and the cylinder part 21b can be made smaller than that of the conventional structure, and from the plate part 21a to the cylinder part 21b. Heat escape due to heat conduction can be prevented.
Moreover, the heating of the susceptor support member 31 due to heat conduction from the cylindrical portion 21b is suppressed, and the susceptor support member 31 can be prevented from being damaged by heat.

板部21aのうち基板配置部45は熱抵抗部分41で取り囲まれている。熱抵抗部分41の厚みは基板配置部45の厚みより薄く、板部21aのうち基板配置部45より外側の外周部分の温度が熱輻射により下がっても、基板配置部45内から外周部分には熱が逃げにくくなっている。そのため、基板配置部45内は温度差1℃以内の均一な温度に維持され、各基板51は均一な温度に加熱される。   Of the plate portion 21 a, the substrate placement portion 45 is surrounded by the thermal resistance portion 41. The thickness of the thermal resistance portion 41 is thinner than the thickness of the substrate placement portion 45, and even if the temperature of the outer peripheral portion outside the substrate placement portion 45 of the plate portion 21 a is lowered by thermal radiation, The heat is difficult to escape. Therefore, the inside of the substrate placement unit 45 is maintained at a uniform temperature within a temperature difference of 1 ° C., and each substrate 51 is heated to a uniform temperature.

原料ガス源13bから放出容器13a内に原料ガスを供給する。原料ガスには加熱された基板51上で化学反応できるガスを使用し、ここではTMG(トリメチルガリウム)ガスとNH3ガスを使用するが、本発明は原料ガスがTMGガスとNH3ガスの場合に限定されない。 A source gas is supplied from the source gas source 13b into the discharge vessel 13a. As the source gas, a gas capable of chemically reacting on the heated substrate 51 is used. Here, TMG (trimethylgallium) gas and NH 3 gas are used. However, in the present invention, the source gas is TMG gas and NH 3 gas. It is not limited to.

供給された原料ガスは放出孔13cから真空槽11内に放出され、加熱された基板51の表面に到達し、基板51の熱により化学反応して結晶化し、基板51の表面に薄膜が形成される。ここではGaNの薄膜が形成される。   The supplied source gas is discharged into the vacuum chamber 11 from the discharge hole 13c, reaches the surface of the heated substrate 51, is crystallized by a chemical reaction with the heat of the substrate 51, and a thin film is formed on the surface of the substrate 51. The Here, a GaN thin film is formed.

回転部32によりサセプタ21を回転させており、板部21a表面の中心から同一距離に配置された複数の基板51には均一な量の原料ガスが到達して均一な膜厚の薄膜が形成される。
板部21aのうち基板配置部45内は均一な温度に維持されており、各基板51は均一な温度に加熱され、各基板51に形成される薄膜の膜質差は小さくなる。
The susceptor 21 is rotated by the rotating part 32, and a uniform amount of source gas reaches the plurality of substrates 51 arranged at the same distance from the center of the surface of the plate part 21a to form a thin film having a uniform film thickness. The
The substrate placement portion 45 in the plate portion 21a is maintained at a uniform temperature, and each substrate 51 is heated to a uniform temperature, so that the difference in film quality between thin films formed on each substrate 51 is reduced.

各基板51の表面に所定の膜厚の薄膜を形成したのち、原料ガス源13bからの原料ガスの放出を停止させる。加熱用電源33から第一〜第三のヒーター23a〜23cへの電力の供給を停止する。回転部32によるサセプタ21の回転を停止する。   After a thin film having a predetermined thickness is formed on the surface of each substrate 51, the release of the source gas from the source gas source 13b is stopped. The supply of power from the heating power source 33 to the first to third heaters 23a to 23c is stopped. The rotation of the susceptor 21 by the rotating unit 32 is stopped.

真空排気部12による真空排気を停止し、真空槽11内を大気に曝す。成膜済みの基板51を真空槽11の外側に搬出し、後工程に回す。
未成膜の基板51を真空槽11内に搬入し、上述の成膜工程を繰り返す。
The evacuation by the evacuation unit 12 is stopped, and the inside of the vacuum chamber 11 is exposed to the atmosphere. The film-formed substrate 51 is carried out to the outside of the vacuum chamber 11 and is sent to a subsequent process.
The undeposited substrate 51 is carried into the vacuum chamber 11 and the above-described deposition process is repeated.

なお、本発明は図6を参照し、サセプタ21の板部21aに熱抵抗部分41が設けられていない構成も含まれるが、板部21aに熱抵抗部分41が設けられている構成の方が基板配置部45内を均一な温度に維持し易いため好ましい。   The present invention includes a configuration in which the thermal resistance portion 41 is not provided in the plate portion 21a of the susceptor 21 with reference to FIG. 6, but the configuration in which the thermal resistance portion 41 is provided in the plate portion 21a is included. This is preferable because the inside of the substrate placement portion 45 can be easily maintained at a uniform temperature.

また、サセプタ21の板部21aと筒部21bとが密着して固定され、又は一体成形されて分離できない構成も本発明に含まれるが、板部21aと筒部21bとが互いに分離できる構成の方が、板部21aから筒部21bへの熱逃げをより効果的に抑制でき、またメンテナンスが容易であるため好ましい。   In addition, a configuration in which the plate portion 21a and the cylindrical portion 21b of the susceptor 21 are closely fixed and fixed or integrally molded and cannot be separated is also included in the present invention, but the plate portion 21a and the cylindrical portion 21b can be separated from each other. This is preferable because heat escape from the plate portion 21a to the tube portion 21b can be more effectively suppressed and maintenance is easy.

10……成膜装置
11……真空槽
12……真空排気部
13……原料ガス導入部
21……サセプタ
21a……板部
21b……筒部
22……熱抵抗部材
23……ヒーター
31……サセプタ支持部材
41……熱抵抗部分
51……基板
DESCRIPTION OF SYMBOLS 10 ... Film-forming apparatus 11 ... Vacuum chamber 12 ... Vacuum exhaust part 13 ... Raw material gas introduction part 21 ... Susceptor 21a ... Plate part 21b ... Cylindrical part 22 ... Heat resistance member 23 ... Heater 31 ... ... Susceptor support member 41 ... Thermal resistance part 51 ... Substrate

Claims (6)

真空槽と、
前記真空槽内を真空排気する真空排気部と、
前記真空槽内に原料ガスを導入する原料ガス導入部と、
前記真空槽内に配置され、表面に基板が配置される板部と、前記板部の前記表面とは逆の裏面で一端の開口が蓋された筒部とからなるサセプタと、
前記筒部の内側に配置され、前記板部の前記裏面と前記筒部の内周面とにそれぞれ対向されたヒーターと、
前記筒部の前記一端とは逆の他端に設けられ、前記サセプタを支持するサセプタ支持部材と、
を有し、
前記ヒーターによって前記サセプタを加熱し、前記原料ガス導入部から前記真空槽内に原料ガスを導入し、前記板部の前記表面に配置された基板に薄膜を形成する成膜装置であって、
前記筒部の前記他端と前記サセプタ支持部材との間には、前記サセプタとは別の材質である熱抵抗部材が配置された成膜装置。
A vacuum chamber;
An evacuation unit for evacuating the vacuum chamber;
A source gas introduction part for introducing a source gas into the vacuum chamber;
A susceptor comprising a plate portion disposed in the vacuum chamber and having a substrate disposed on a surface thereof, and a cylindrical portion whose one end is covered with a back surface opposite to the surface of the plate portion;
A heater disposed inside the cylindrical portion and opposed to the back surface of the plate portion and the inner peripheral surface of the cylindrical portion;
A susceptor support member that is provided at the other end opposite to the one end of the cylindrical portion and supports the susceptor;
Have
A film forming apparatus that heats the susceptor by the heater, introduces a source gas into the vacuum chamber from the source gas introduction unit, and forms a thin film on a substrate disposed on the surface of the plate unit;
A film forming apparatus in which a thermal resistance member made of a material different from that of the susceptor is disposed between the other end of the cylindrical portion and the susceptor support member.
前記熱抵抗部材の線膨張率は前記サセプタの線膨張率より小さく、
前記熱抵抗部材の熱伝導率は前記サセプタの熱伝導率より小さい請求項1記載の成膜装置。
The linear expansion coefficient of the thermal resistance member is smaller than the linear expansion coefficient of the susceptor,
The film forming apparatus according to claim 1, wherein a thermal conductivity of the thermal resistance member is smaller than a thermal conductivity of the susceptor.
前記サセプタの材質はグラファイトであり、前記熱抵抗部材の材質はSiCである請求項1又は請求項2のいずれか1項記載の成膜装置。   The film forming apparatus according to claim 1, wherein a material of the susceptor is graphite, and a material of the heat resistance member is SiC. 前記板部のうち、前記基板が配置される範囲より外側には、前記基板が配置される範囲の厚みより厚みが薄い熱抵抗部分が環状に設けられた請求項1乃至請求項3のいずれか1項記載の成膜装置。   The thermal resistance part whose thickness is thinner than the thickness of the range in which the said board | substrate is arrange | positioned outside the range in which the said board | substrate is arrange | positioned among the said board parts is given in any one of Claim 1 thru | or 3. 2. The film forming apparatus according to 1. 前記板部と前記筒部は分離可能に構成された請求項1乃至請求項4のいずれか1項記載の成膜装置。   The film forming apparatus according to claim 1, wherein the plate portion and the cylindrical portion are configured to be separable. 前記板部は、900℃以上1300℃以下に加熱される請求項1乃至請求項5のいずれか1項記載の成膜装置。   The film forming apparatus according to claim 1, wherein the plate portion is heated to 900 ° C. or higher and 1300 ° C. or lower.
JP2011235126A 2011-10-26 2011-10-26 Deposition apparatus Pending JP2013093461A (en)

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JP2017228596A (en) * 2016-06-20 2017-12-28 三星電子株式会社Samsung Electronics Co.,Ltd. Wafer mounting mechanism with heater and film forming apparatus
JP2019169636A (en) * 2018-03-23 2019-10-03 東京エレクトロン株式会社 Substrate heating apparatus and substrate processing apparatus using the same
JP7358576B1 (en) 2022-07-21 2023-10-10 積水化学工業株式会社 Film deposition equipment and method for manufacturing film-coated wafers

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JPH04280418A (en) * 1991-03-08 1992-10-06 Fujitsu Ltd Vapor growth device
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JPH0465819A (en) * 1990-07-06 1992-03-02 Nissin Electric Co Ltd Vapor growth device
JPH04186823A (en) * 1990-11-21 1992-07-03 Toshiba Corp Vapor growth device
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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2017228596A (en) * 2016-06-20 2017-12-28 三星電子株式会社Samsung Electronics Co.,Ltd. Wafer mounting mechanism with heater and film forming apparatus
JP2019169636A (en) * 2018-03-23 2019-10-03 東京エレクトロン株式会社 Substrate heating apparatus and substrate processing apparatus using the same
JP7358576B1 (en) 2022-07-21 2023-10-10 積水化学工業株式会社 Film deposition equipment and method for manufacturing film-coated wafers
JP2024013909A (en) * 2022-07-21 2024-02-01 積水化学工業株式会社 Film deposition equipment and method for manufacturing film-coated wafers

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