JP2010261061A - Method for producing Al alloy forged product - Google Patents
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Abstract
【課題】生産性向上、コスト削減を図りつつ、高品質のAl合金鍛造製品を得る。
【解決手段】本発明の製法は、Fe:0.2〜0.35%、Cu:0.05〜0.20%、Mn:0.3〜0.6%、Mg:1.3〜2.0%、Zn:4.6〜5.1%、Si:0.30%未満、Zr:0.1%以上かつTiとの合計量で0.2%未満含有し、「[Ti質量%]/[Zr質量%]≧0.2」の関係を満たし、残部がAl及び不可避不純物からなる合金組成を有するAl合金鍛造素材を得る工程と、Al合金鍛造素材に対し、350〜500℃の温度で熱間鍛造を行った後、400〜500℃の温度で溶体化処理を行うことにより、Al合金鍛造製品を得る工程と、Al合金鍛造製品に対し、自然時効処理を行わずに、人工時効処理を行う工程と、を含む。
【選択図】図1A high quality forged Al alloy product is obtained while improving productivity and reducing costs.
The production method of the present invention includes Fe: 0.2-0.35%, Cu: 0.05-0.20%, Mn: 0.3-0.6%, Mg: 1.3-2. 0.0%, Zn: 4.6-5.1%, Si: less than 0.30%, Zr: 0.1% or more, and less than 0.2% in total with Ti, “[Ti mass% ] / [Zr mass%] ≧ 0.2 ”, a step of obtaining an Al alloy forging material having an alloy composition with the balance consisting of Al and inevitable impurities, and an Al alloy forging material of 350 to 500 ° C. After performing hot forging at a temperature, a solution treatment is performed at a temperature of 400 to 500 ° C., thereby obtaining an Al alloy forged product, and without subjecting the Al alloy forged product to natural aging treatment. Performing an aging treatment.
[Selection] Figure 1
Description
本発明は、鍛造加工によってAl合金製品を製造するためのAl合金鍛造製品の製造方法及びその関連技術に関する。 The present invention relates to a method for producing an Al alloy forged product for producing an Al alloy product by forging and related techniques.
近年、高強度が必要なオートバイ部品を、アルミニウム(Al)合金の鍛造製品によって製造する技術が周知である。このような鍛造製品は、例えば下記特許文献1に示すようなAl−Zn−Mg系合金の鍛造素材を鍛造加工することによって製造されている。 2. Description of the Related Art In recent years, a technique for manufacturing a motorcycle part requiring high strength by a forged product of an aluminum (Al) alloy is well known. Such a forged product is manufactured by forging a forging material of an Al—Zn—Mg alloy as shown in Patent Document 1 below, for example.
一般のAl−Zn−Mg系合金素材の鍛造加工においては下記特許文献1に示すように、耐応力腐食割れ性や引張強度を向上させるために、型成形後のT6熱処理工程で、100時間程度室温に保持する自然時効処理を行った後、人工時効処理を行うようにしている。 In the forging of a general Al—Zn—Mg alloy material, as shown in the following Patent Document 1, in order to improve stress corrosion cracking resistance and tensile strength, in the T6 heat treatment step after mold forming, about 100 hours. Artificial aging treatment is performed after natural aging treatment is performed at room temperature.
しかしながら、上記従来の鍛造加工方法においては、型成形後に長時間の自然時効処理を行うようにしているため、生産に要するサイクルタイムが長くなり、生産効率の低下及びコストの増大を来してしまう。また場合によっては、自然時効処理によるワークの保管期間が長くなることにより、結露等による腐食が生じて、製品の品質を低下させるという問題が発生する。 However, in the conventional forging method described above, since natural aging treatment is performed for a long time after mold forming, the cycle time required for production becomes long, resulting in a decrease in production efficiency and an increase in cost. . In some cases, the storage period of the workpiece by natural aging treatment becomes longer, which causes corrosion due to condensation or the like, resulting in a problem that the quality of the product is deteriorated.
この発明は、上記の課題に鑑みてなされたもので、生産効率の向上及びコストの削減を図りつつ、高品質のAl合金鍛造製品を得ることができるAl合金鍛造製品の製造方法及びその関連技術を提供することを目的とする。 SUMMARY OF THE INVENTION The present invention has been made in view of the above problems, and a manufacturing method of an Al alloy forged product and related technology capable of obtaining a high quality Al alloy forged product while improving production efficiency and reducing costs. The purpose is to provide.
上記の目的を達成するため、本発明は、以下の構成を備えている。 In order to achieve the above object, the present invention comprises the following arrangement.
[1]Fe:0.2〜0.35質量%、Cu:0.05〜0.20質量%、Mn:0.3〜0.6質量%、Mg:1.3〜2.0質量%、Zn:4.6〜5.1質量%、Si:0.30質量%未満、Zr:0.1質量%以上かつTiとの合計量で0.2質量%未満含有し、「[Ti質量%]/[Zr質量%]≧0.2」の関係を満たし、残部がAl及び不可避不純物からなる合金組成を有するAl合金鍛造素材を得る工程と、
前記Al合金鍛造素材に対し、350〜500℃の温度で熱間鍛造を行った後、400〜500℃の温度で溶体化処理を行うことにより、Al合金鍛造製品を得る工程と、
前記Al合金鍛造製品に対し、自然時効処理を行わずに、人工時効処理を行う工程と、を含むことを特徴とするAl合金鍛造製品の製造方法。
[1] Fe: 0.2 to 0.35 mass%, Cu: 0.05 to 0.20 mass%, Mn: 0.3 to 0.6 mass%, Mg: 1.3 to 2.0 mass% Zn: 4.6-5.1% by mass, Si: less than 0.30% by mass, Zr: 0.1% by mass or more and less than 0.2% by mass in total with Ti, “[Ti mass %] / [Zr mass%] ≧ 0.2 ”, and obtaining an Al alloy forging material having an alloy composition with the balance consisting of Al and inevitable impurities,
A process of obtaining an Al alloy forged product by performing a solution treatment at a temperature of 400 to 500 ° C. after hot forging at a temperature of 350 to 500 ° C. with respect to the Al alloy forged material,
A step of performing artificial aging treatment on the Al alloy forged product without performing natural aging treatment on the Al alloy forged product.
[2]前記合金組成を有するAl合金溶湯を、連続鋳造して得られたAl合金鋳塊に対して均質化処理を施すことによって、Al合金鋳造部材を得る工程を更に含み、
前記Al合金鋳造部材を前記Al合金鍛造素材として用いるようにした前項1に記載のAl合金鍛造製品の製造方法。
[2] The method further includes a step of obtaining an Al alloy cast member by subjecting the Al alloy molten metal having the alloy composition to a homogenization treatment to an Al alloy ingot obtained by continuous casting,
The method for producing an Al alloy forged product according to item 1, wherein the Al alloy cast member is used as the Al alloy forged material.
[3]前記人工時効処理として、90〜120℃の温度で2〜12時間保持した後、直ちに130〜170℃の温度で2〜12時間保持するようにした前項1または2に記載のAl合金鍛造製品の製造方法。
[3] The Al alloy according to the
[4]溶体化処理後のAl合金鍛造製品に対し、1時間以内に人工時効処理を行うようにした前項1〜3のいずれか1項に記載のAl合金鍛造製品の製造方法。 [4] The method for producing an Al alloy forged product according to any one of items 1 to 3, wherein the artificial aging treatment is performed within 1 hour for the Al alloy forged product after the solution treatment.
[5]前項1〜4のいずれか1項に記載の製造方法によって製造されたAl合金鍛造製品を、オートバイフレーム部品に仕上げるようにしたことを特徴とするオートバイフレーム部品の製造方法。 [5] A method for manufacturing a motorcycle frame part, wherein the Al alloy forged product manufactured by the manufacturing method according to any one of items 1 to 4 is finished into a motorcycle frame part.
発明[1]のAl合金鍛造製品の製造方法によれば、生産効率の向上及びコストの削減を図りつつ、高品質のAl−Zn−Mg系合金鍛造製品を得ることができる。 According to the method for producing an Al alloy forged product of the invention [1], a high quality Al—Zn—Mg based alloy forged product can be obtained while improving the production efficiency and reducing the cost.
発明[2][3]のAl合金鍛造製品の製造方法によれば、上記の効果に加えてさらに、より一層確実に高強度溶接構造用に適したAl合金鍛造製品を得ることができる。 According to the method for producing an Al alloy forged product of the inventions [2] and [3], in addition to the above effects, an Al alloy forged product suitable for a high-strength welded structure can be obtained more reliably.
なお、本発明において、「高強度溶接構造」とは、高強度が要求される溶接構造材に適した構造と言うことである。 In the present invention, “high-strength weld structure” means a structure suitable for a welded structure material that requires high strength.
発明[4]のAl合金鍛造製品の製造方法によれば、生産効率をより一層向上させることができる。 According to the method for producing an Al alloy forged product of the invention [4], the production efficiency can be further improved.
発明[5]のオートバイフレーム部品の製造方法によれば、生産効率の向上、コストの削減を図りつつ、高品質のオートバイフレーム部品を得ることができる。 According to the method for manufacturing a motorcycle frame part of the invention [5], a high-quality motorcycle frame part can be obtained while improving the production efficiency and reducing the cost.
本実施形態においては、Al合金鋳造部材を鍛造素材として、鍛造加工を行うようにしている。 In this embodiment, forging is performed using an Al alloy cast member as a forging material.
本実施形態における鍛造素材としてのAl合金鋳造部材は、特有の合金組成に規定される共に、金属組織において特有の晶出物の粒径及び分布状態に制御されている。 The Al alloy cast member as the forging material in the present embodiment is regulated by a specific alloy composition, and is controlled to have a specific crystal grain size and distribution state in the metal structure.
このAl合金鋳造部材は、所定の組成を有するAl合金溶湯を、所定の条件下で連続鋳造することによってAl合金鋳塊を得、そのAl合金鋳塊に対し、所定の均質化処理を施すことによって得られるものである。 This Al alloy cast member is obtained by continuously casting an Al alloy molten metal having a predetermined composition under predetermined conditions to obtain an Al alloy ingot, and subjecting the Al alloy ingot to a predetermined homogenization treatment. Is obtained.
まず始めにこのAl合金鋳造部材の構成について、その製造手順に従って詳細に説明する。 First, the configuration of the Al alloy cast member will be described in detail according to the manufacturing procedure.
本発明における鋳造素材としてのAl合金溶湯は、Feを0.2〜0.35質量%、Cuを0.05〜0.20質量%、Mnを0.3〜0.6質量%、Mgを1.3〜2.0質量%、Znを4.6〜5.1質量%、Siを0.30質量%未満、Zrを0.1質量%以上かつTiとの合計量で0.2質量%未満含有し、「[Ti質量%]/[Zr質量%]≧0.2」の関係を満たし、残部がAl及び不可避不純物からなる合金組成を有している。 The molten Al alloy as a casting material in the present invention is 0.2 to 0.35 mass% Fe, 0.05 to 0.20 mass% Cu, 0.3 to 0.6 mass% Mn, and Mg. 1.3 to 2.0 mass%, Zn is 4.6 to 5.1 mass%, Si is less than 0.30 mass%, Zr is 0.1 mass% or more, and 0.2 mass in total with Ti %, Satisfying the relationship of “[Ti mass%] / [Zr mass%] ≧ 0.2”, and the balance has an alloy composition consisting of Al and inevitable impurities.
上記の合金組成のうち、Feは、鋳造時の鋳塊割れや溶接時の溶接割れを抑制し、粗大再結晶を抑制する元素であり、本発明においては、Feの含有率(濃度)を0.2〜0.35質量%に調整する必要がある。 Among the above alloy compositions, Fe is an element that suppresses ingot cracking during casting and weld cracking during welding and suppresses coarse recrystallization. In the present invention, the Fe content (concentration) is 0. It is necessary to adjust to 2 to 0.35 mass%.
Feの含有率が0.2質量%未満では前記効果が小さく、0.35質量%を超えるとAl−Fe−Mn系の粗大晶出物が増加し、鍛造時の塑性加工性を阻害し、また、鍛造加工後の鍛造製品が最終的に車体等に組み付けられた際に、その鍛造製品(組付部品)における伸性(延性)、靭性、疲労強度及び衝撃特性が低下するので望ましくない。 When the Fe content is less than 0.2% by mass, the above effects are small, and when it exceeds 0.35% by mass, coarse Al-Fe-Mn based crystals are increased, and the plastic workability during forging is impaired. Further, when the forged product after forging is finally assembled to a vehicle body or the like, the ductility (ductility), toughness, fatigue strength, and impact characteristics of the forged product (assembled part) are deteriorated.
Cuは、アルミニウムマトリックスに固溶して、固溶体中の溶質の過飽和度を上げるなどして、強度を付与する元素であり、本発明においては、Cuの含有率(濃度)を0.05〜0.20質量%に調整する必要がある。 Cu is an element that imparts strength by being dissolved in an aluminum matrix and increasing the degree of supersaturation of the solute in the solid solution. In the present invention, the Cu content (concentration) is 0.05 to 0. It is necessary to adjust to 20% by mass.
Cuの含有量が0.05質量%未満では、十分な強度向上効果が得られず、0.20質量%を超えると、強度は向上するが耐応力腐食割れ性が著しく低下し、溶接割れを発生させる危険性も生じるので望ましくない。 When the Cu content is less than 0.05% by mass, a sufficient strength improvement effect cannot be obtained. When the Cu content exceeds 0.20% by mass, the strength is improved, but the stress corrosion cracking resistance is remarkably lowered, so This is not desirable because there is a risk of generation.
Mnは、粗大再結晶を抑制する元素であり、本発明においては、Mnの含有率(濃度)を0.3〜0.6質量%に調整する必要がある。 Mn is an element that suppresses coarse recrystallization. In the present invention, it is necessary to adjust the content (concentration) of Mn to 0.3 to 0.6% by mass.
Mnの含有率が0.3質量%未満では前記効果が小さく、0.6質量%を超えるとAl−Fe−Mn系の粗大晶出物が増加し、鍛造時の塑性加工性を阻害し、また、鍛造加工後の鍛造製品が、最終的に車体等に組み付けられた際に、その鍛造製品(組付部品)における伸性、靭性、疲労強度が低下するので望ましくない。 When the content of Mn is less than 0.3% by mass, the above effect is small, and when it exceeds 0.6% by mass, the Al-Fe-Mn series coarse crystallized matter increases, and the plastic workability during forging is impaired. Further, when the forged product after forging is finally assembled to a vehicle body or the like, the ductility, toughness, and fatigue strength of the forged product (assembled part) are lowered, which is not desirable.
Mgは、Znと共存することにより、MgZn2金属間化合物(η相)を析出させて機械的強度を向上させる元素である。本発明においては、Mgの含有率(濃度)を1.3〜2.0質量%に調整する必要がある。 Mg is an element that precipitates MgZn 2 intermetallic compound (η phase) and improves mechanical strength by coexisting with Zn. In the present invention, it is necessary to adjust the Mg content (concentration) to 1.3 to 2.0 mass%.
Mgの含有率が1.3質量%未満の場合には前記効果が小さく、2.0質量%を超える場合には応力腐食割れ性や焼入れ感受性が低下するので望ましくない。 When the Mg content is less than 1.3% by mass, the above effect is small, and when it exceeds 2.0% by mass, the stress corrosion cracking property and quenching sensitivity are lowered, which is not desirable.
Znは、上記したように、Mgと共存することによりMgZn2金属間化合物(η相)を析出させて機械的強度を向上させる元素である。本発明においては、Znの含有率(濃度)を4.6〜5.1質量%に調整する必要がある。 As described above, Zn is an element that improves mechanical strength by precipitating MgZn 2 intermetallic compound (η phase) by coexisting with Mg. In the present invention, it is necessary to adjust the Zn content (concentration) to 4.6 to 5.1 mass%.
Znの濃度が4.6質量%未満の場合には前記効果が小さく、5.1質量%を超える場合には応力腐食割れ性や焼入れ感受性が低下するので望ましくない。 When the Zn concentration is less than 4.6% by mass, the above effect is small, and when it exceeds 5.1% by mass, the stress corrosion cracking property and quenching sensitivity are lowered, which is not desirable.
Siの含有率は、0.30質量%を超えない量に調整する必要がある。すなわちSi含有量が多すぎると、製品における延性、靱性、疲労強度及びw衝撃性が低下するので望ましくない。その上さらに、Siの含有率が多くなると、Mgと反応し、時効析出挙動が変化し、熱処理時の自然時効が必要となるので好ましくない。 It is necessary to adjust the Si content to an amount not exceeding 0.30 mass%. That is, if the Si content is too large, the ductility, toughness, fatigue strength and w impact property of the product are lowered, which is not desirable. Furthermore, if the Si content increases, it reacts with Mg, the aging precipitation behavior changes, and natural aging during heat treatment is required, which is not preferable.
Zrは、粗大再結晶を抑制し、溶接部の結晶粒微細化を促進する元素であり、本発明においては、Zrの含有率(濃度)を0.1質量%以上に調整し、かつ「TiとZrとの添加量(含有率)合計が0.2質量%を超えないように調整する必要がある。 Zr is an element that suppresses coarse recrystallization and promotes refinement of the crystal grain of the weld. In the present invention, the content (concentration) of Zr is adjusted to 0.1% by mass or more, and “Ti It is necessary to adjust so that the total amount (content) of Zr and Zr does not exceed 0.2% by mass.
Zrの濃度が0.1質量%未満では前記効果が小さい。またZrを大量に添加すると、鋳造時の結晶粒微細化のために添加されるTiB2のBと反応して、ZrB2を生成し、結晶粒微細化を阻害する。このため、TiB2を大量に添加する必要が生じる。しかし、TiB2及びZrB2は硬質粒子であるため、鍛造加工後の鍛造製品に対し切削加工を行う際に、その切削加工時のバイト寿命を短くするため、あまり大量の添加は望ましくない。そこで、Zrの添加量(濃度)としては、上記したように、0.1質量%以上に調整し、かつTiとZrとの添加量合計を0.2質量%未満に調整する必要がある。 The effect is small when the concentration of Zr is less than 0.1% by mass. When a large amount of Zr is added, it reacts with B of TiB 2 added for crystal grain refinement during casting to produce ZrB 2 and inhibit crystal grain refinement. For this reason, it becomes necessary to add a TiB 2 in large quantities. However, since TiB 2 and ZrB 2 are hard particles, when cutting a forged product after forging, in order to shorten the tool life at the time of cutting, it is not desirable to add too much. Therefore, it is necessary to adjust the addition amount (concentration) of Zr to 0.1% by mass or more as described above, and to adjust the total addition amount of Ti and Zr to less than 0.2% by mass.
なお本発明において、より好ましくは、Tiの添加量を0.03〜0.05質量%、Zrの添加量を0.10〜0.15質量%に設定するのが良い。 In the present invention, it is more preferable to set the addition amount of Ti to 0.03 to 0.05 mass% and the addition amount of Zr to 0.10 to 0.15 mass%.
更に本発明のAl合金組成では、TiとZrとの間において、「[Ti質量%]/[Zr質量%]≧0.2」の関係を満足させる必要がある。 Furthermore, in the Al alloy composition of the present invention, it is necessary to satisfy the relationship “[Ti mass%] / [Zr mass%] ≧ 0.2” between Ti and Zr.
すなわち、Zrは前述したように、鋳造時の結晶粒微細化のために添加されるTiB2のBと反応して、ZrB2を生成し、結晶粒微細化を阻害する。そのため、Zr添加量に対するTiB2添加量が少ないと、鋳造時の結晶粒が粗くなり、機械的強度及び伸び(延び)の低下を生じ、更には、鋳造時に鋳塊の割れを生じるため、Ti及びZrの質量比(Ti質量%/Zr質量%)が0.2以上となるように、TiB2及びZrの添加量を制御する必要がある。 That is, as described above, Zr reacts with B of TiB 2 added for crystal grain refinement at the time of casting to produce ZrB 2 and inhibits crystal grain refinement. Therefore, if the TiB 2 addition amount relative to the Zr addition amount is small, the crystal grains at the time of casting become coarse, resulting in a decrease in mechanical strength and elongation (elongation). and the mass ratio of Zr (Ti wt% / Zr mass%) is such that 0.2 or more, it is necessary to control the amount of TiB 2 and Zr.
また本発明のAl合金組成では、SiとMgとの間において、「[Si質量%]≦0.2×[Mg質量%]−0.1」の関係を満足させるのが好ましい。 In the Al alloy composition of the present invention, it is preferable to satisfy the relationship of “[Si mass%] ≦ 0.2 × [Mg mass%] − 0.1” between Si and Mg.
すなわちSiは不純物として含有される元素であり、Siの含有量が多過ぎる場合、鍛造加工後の鍛造製品における伸性、靭性、疲労強度が低下するおそれがある。そればかりか、Si含有量が多過ぎる場合、Mgと反応し、時効析出挙動が変化し、熱処理時の自然時効が必要となるので望ましくない。これらの挙動は、Siの単独の働きだけではなく、Mg量とも関連があるため、上記したように[Si質量%]≦0.2×[Mg質量%]−0.1となるようにSi含有量を制御するのが好ましい。 That is, Si is an element contained as an impurity, and when the Si content is too large, the ductility, toughness, and fatigue strength of the forged product after forging may be reduced. In addition, when the Si content is too high, it reacts with Mg, changes the aging precipitation behavior, and requires natural aging during heat treatment, which is not desirable. Since these behaviors are related not only to the single function of Si but also to the amount of Mg, as described above, [Si mass%] ≦ 0.2 × [Mg mass%] − 0.1. It is preferable to control the content.
本実施形態においては、以上の合金組成を有するAl合金溶湯を、連続鋳造することによってAl合金鋳塊を得るものである。 In this embodiment, an Al alloy ingot is obtained by continuously casting a molten Al alloy having the above alloy composition.
さらに本実施形態においては、上記のAl合金鋳塊に対して均質化処理を行って、Al合金鋳造部材を得るものである。 Furthermore, in this embodiment, homogenization process is performed with respect to said Al alloy ingot, and an Al alloy cast member is obtained.
こうして得られたAl合金鋳造部材は、鍛造素材として用いられる。すなわち上記Al合金鋳造部材としての鍛造素材を、350〜500℃の温度条件で、熱間鍛造することによって、Al合金鍛造製品を製造するものである。 The Al alloy cast member thus obtained is used as a forging material. That is, an Al alloy forged product is manufactured by hot forging the forging material as the Al alloy cast member at a temperature of 350 to 500 ° C.
ここで、熱間鍛造時の温度が350℃より低い場合には、鍛造時の塑性加工性が悪化し、所望する形状の鍛造製品が得られないばかりか、金型の破損、鍛造製品の割れを生じる原因となる。また熱間鍛造時の温度が500℃よりも高い場合には、共晶融解により、鍛造製品の表面付近に穴欠陥が生じたり、融点が低い金属の凝集が生じるおそれがある。従って本発明においては、熱間鍛造時の温度条件を、350〜500℃に調整するのが望ましい。 Here, when the temperature during hot forging is lower than 350 ° C., the plastic workability during forging deteriorates, and not only a forged product having a desired shape is obtained, but also die breakage, cracking of the forged product. Cause. When the temperature during hot forging is higher than 500 ° C., hole defects may occur near the surface of the forged product or aggregation of metals having a low melting point may occur due to eutectic melting. Therefore, in this invention, it is desirable to adjust the temperature conditions at the time of hot forging to 350-500 degreeC.
また本発明においては、上記ように得られたAl合金鍛造製品に対し、400〜500℃で溶体化処理を行うことによって、鍛造製品の機械的強度をより一層向上させることができる。 In the present invention, the mechanical strength of the forged product can be further improved by performing a solution treatment at 400 to 500 ° C. on the Al alloy forged product obtained as described above.
この溶体化処理において、処理温度が400℃よりも低い場合、析出強化元素の固溶量が少なくなるため、その後の人工時効処理での析出量が少なくなり、十分な機械的強度が得られなくなるおそれがある。また処理温度が500℃よりも高い場合には、共晶融解により、鍛造製品の表面付近に穴欠陥及び融点が低い金属の凝集が生じるおそれがある。 In this solution treatment, when the treatment temperature is lower than 400 ° C., the solid solution amount of the precipitation strengthening element is reduced, so that the precipitation amount in the subsequent artificial aging treatment is reduced and sufficient mechanical strength cannot be obtained. There is a fear. Further, when the processing temperature is higher than 500 ° C., hole defects and aggregation of a metal having a low melting point may occur near the surface of the forged product due to eutectic melting.
本発明において、溶体化処理を行ったAl合金鍛造製品は、自然時効処理を行わずに、人工時効処理を行うものである。 In the present invention, the Al alloy forged product subjected to solution treatment is subjected to artificial aging treatment without performing natural aging treatment.
ここで本発明における時効処理は、自然時効処理と、人工時効処理とに大別される。 Here, the aging treatment in the present invention is roughly divided into a natural aging treatment and an artificial aging treatment.
自然時効処理は、溶体化処理後、製品を室温で放置し、低温で時効を進行させるというような処理であり、具体的には、室温(0〜50℃程度)で24〜72時間保持するような処理である。 The natural aging treatment is a treatment in which, after solution treatment, the product is left at room temperature and aging proceeds at a low temperature. Specifically, it is kept at room temperature (about 0 to 50 ° C.) for 24 to 72 hours. It is a process like this.
これに対し、人工時効処理は、人工時効処理は、溶体化処理後、製品を熱処理炉に投入し、高温で時効を進行させる処理である。具体的には、鍛造製品に対し、温度を室温から1時間かけて100℃まで上昇させて6時間保持する。その後、温度を100℃から1時間かけて150℃まで上昇させて、8時間保持した後、空冷によって室温まで温度を低下させるように処理するものである。 On the other hand, the artificial aging treatment is a treatment in which, after solution treatment, the product is put into a heat treatment furnace and aging is advanced at a high temperature. Specifically, the temperature of the forged product is increased from room temperature to 100 ° C. over 1 hour and held for 6 hours. Thereafter, the temperature is raised from 100 ° C. to 150 ° C. over 1 hour, held for 8 hours, and then treated so that the temperature is lowered to room temperature by air cooling.
また本発明において、Al合金鍛造製品は、生産性の向上、コストの削減及び品質の向上を図るために、溶体化処理後、長時間放置せずに、直ちに次の処理(人工時効処理)を行うのが好ましい。具体的には、Al合金鍛造製品に対し、溶体化処理後、1時間以内、望ましくは、溶体化処理直後に、人工時効処理を行うのが好ましい。 In the present invention, for the Al alloy forged product, the following treatment (artificial aging treatment) is performed immediately after the solution treatment without leaving it for a long time in order to improve productivity, reduce costs and improve quality. It is preferred to do so. Specifically, the artificial aging treatment is preferably performed on the Al alloy forged product within 1 hour after the solution treatment, preferably immediately after the solution treatment.
本発明においては、この人工時効処理を行うことによって、伸性、靭性、疲労強度及び衝撃特性を十分に向上させることができ、所望の機械的強度を備えた高品質の鍛造製品を確実に得ることができる。 In the present invention, by performing this artificial aging treatment, the ductility, toughness, fatigue strength, and impact characteristics can be sufficiently improved, and a high-quality forged product having a desired mechanical strength can be reliably obtained. be able to.
以上説明したように、本発明のAl合金鍛造製品の製造方法によれば、鍛造加工の型成形後に溶体化処理を行った後、自然時効処理を行わずに、直ちに人工時効処理を行うものであるため、生産効率の向上及びコストの削減を図ることができる。 As described above, according to the method for producing an Al alloy forged product of the present invention, after the solution treatment is performed after the forging die forming, the artificial aging treatment is performed immediately without performing the natural aging treatment. Therefore, it is possible to improve production efficiency and reduce costs.
また、本発明の製法により得られたAl合金鍛造製品は、後述の実施例からも明らかなように、割れや穴欠陥、粗大な再結晶等の不具合が発生するのを防止できるとともに、十分な引張強度及び破断伸び性を有し、優れた性質を備えるものである。更に自然時効により鍛造製品が長時間放置されることもないため、その長時間の放置に起因して、結露等による腐食が生じるのを確実に防止でき、高い製品品質を維持することができる。 Moreover, the Al alloy forged product obtained by the production method of the present invention can prevent the occurrence of defects such as cracks, hole defects, and coarse recrystallization, as is clear from the examples described later, and is sufficient. It has tensile strength and elongation at break and has excellent properties. Furthermore, since the forged product is not left for a long time due to natural aging, it is possible to reliably prevent the occurrence of corrosion due to dew condensation or the like due to the long time leaving, and to maintain high product quality.
また本発明の製法により得られたAl合金鍛造製品は、上記したような優れた機械的特性を備えるものであるため、車両用フレーム部品等の高強度溶接構造用の部品として好適に使用することができる。例えば本発明による鍛造製品は図3に示すように、端部にシャフト(2)が挿入固定されるオートバイフレーム(1)として利用することができる。 In addition, since the Al alloy forged product obtained by the production method of the present invention has excellent mechanical properties as described above, it should be suitably used as a component for a high-strength welded structure such as a vehicle frame component. Can do. For example, as shown in FIG. 3, the forged product according to the present invention can be used as a motorcycle frame (1) in which a shaft (2) is inserted and fixed at an end portion.
次に表1及び図1を参照しつつ、本発明の実施例及び比較例について詳細に説明する。 Next, examples and comparative examples of the present invention will be described in detail with reference to Table 1 and FIG.
なお図1は実施例及び比較例の各サンプルの合金組成におけるZr含有量とTi含有量との関係を示すグラフである。同グラフにおいて、「実」は実施例、「比」は比較例、丸数字は実施例及び比較例の各番号を示し、実施例は「○」印、比較例は「×」印で示している。更に同グラフにおいて、線分(A1)は「Zr質量%=0.1質量%」、線分(A2)は「[Ti質量%]+[Zr質量%]=0.2質量%」、線分(A3)は「[Ti質量%]/[Zr質量%]=0.2」で特定される線分をそれぞれ示す。従ってこれらの線分(A1)〜(A3)で囲まれる領域が、ZrとTiの関係の基で本発明の要旨に相当する部分である。更に図1において破線で囲まれる領域は、本発明の好適範囲である。 FIG. 1 is a graph showing the relationship between the Zr content and the Ti content in the alloy compositions of the samples of Examples and Comparative Examples. In the graph, “actual” indicates an example, “ratio” indicates a comparative example, a circle number indicates each number of the example and comparative example, the example indicates “◯”, and the comparative example indicates “×”. Yes. Further, in the graph, the line segment (A1) is “Zr mass% = 0.1 mass%”, and the line segment (A2) is “[Ti mass%] + [Zr mass%] = 0.2 mass%”. The minute (A3) indicates a line segment specified by “[Ti mass%] / [Zr mass%] = 0.2”. Therefore, the region surrounded by these line segments (A1) to (A3) is a portion corresponding to the gist of the present invention based on the relationship between Zr and Ti. Further, a region surrounded by a broken line in FIG. 1 is a preferable range of the present invention.
<実施例1〜6>
表1及び図1に示すように、実施例1〜6の各サンプルを作製するために、各サンプルに対応する組成のAl合金を溶解し、各サンプルに対応するAl合金溶湯を準備した。
<Examples 1-6>
As shown in Table 1 and FIG. 1, in order to produce each sample of Examples 1 to 6, an Al alloy having a composition corresponding to each sample was melted, and a molten Al alloy corresponding to each sample was prepared.
こうして得られた各Al合金溶湯を金型に鋳込んで、図4に示すような形状のディスクサンプル(3)を採取し、JIS H 1305に記載の発光分光分析により分析した。 Each of the Al alloy melts thus obtained was cast into a mold, and a disk sample (3) having a shape as shown in FIG. 4 was collected and analyzed by emission spectroscopic analysis described in JIS H 1305.
なおディスクサンプル(3)の各種サイズ(s1)〜(s6)は次の通りである。すなわちs1が18mm、s2が30mm、s3が50mm、s4が35mm、s5が5mm、s6が5mmである。 Various sizes (s1) to (s6) of the disk sample (3) are as follows. That is, s1 is 18 mm, s2 is 30 mm, s3 is 50 mm, s4 is 35 mm, s5 is 5 mm, and s6 is 5 mm.
分析の結果、表1に示す目標成分値の各サンプルが得られたことを確認した後、各サンプルに対応するAl合金溶湯に対し、気体加圧式ホットトップ鋳造機を用いて、連続鋳造を行い、各サンプルに対応する直径55mmの丸棒状のAl合金鋳造部材(鋳塊)を作製した。その後、連続鋳造部材を定尺に切断し、460℃で7時間の均質化処理を施した。 As a result of analysis, after confirming that each sample of the target component values shown in Table 1 was obtained, continuous casting was performed on the Al alloy molten metal corresponding to each sample using a gas pressurization type hot top casting machine. A round bar-shaped Al alloy cast member (ingot) having a diameter of 55 mm corresponding to each sample was produced. Thereafter, the continuously cast member was cut into a standard length and subjected to a homogenization treatment at 460 ° C. for 7 hours.
更に均質化処理後の連続鋳造丸棒を直径50mmに外周切削して、60mmの長さに切断して鍛造素材とした。そしてその鍛造素材を、450℃で予備加熱した後、丸棒側面方向から厚さ10mmに据え込んだ。その後、その据込品(Al合金鍛造製品)に460℃で溶体化処理を施した。溶体化処理の後、各据込品に対し、自然時効を行わずに直ちに人工時効処理を行った。人工時効処理としては、110℃で6時間保持後、連続して昇温し、150℃で8時間保持した。 Further, the continuously cast round bar after the homogenization treatment was subjected to outer peripheral cutting to a diameter of 50 mm and cut to a length of 60 mm to obtain a forging material. The forged material was preheated at 450 ° C., and then placed at a thickness of 10 mm from the side of the round bar. Thereafter, the upsetting product (Al alloy forged product) was subjected to a solution treatment at 460 ° C. After solution treatment, artificial aging treatment was performed immediately on each upset product without natural aging. As an artificial aging treatment, after holding at 110 ° C. for 6 hours, the temperature was continuously raised and held at 150 ° C. for 8 hours.
<実施例1〜7の対比例(自然時効有)>
Al合金鍛造製品(据込品)に対し、溶体化処理を行った後、人工時効処理を行う前に、室温(25℃)で100Hr保持する自然時効を行った以外は、上記実施例と同様にして、対比例1〜6の鍛造製品サンプルを得た。
<Comparison of Examples 1-7 (with natural aging)>
After performing solution treatment on Al alloy forged product (fixed product) and before performing artificial aging treatment, it was the same as the above example except that natural aging was carried out at room temperature (25 ° C) for 100 hours. Thus, forged product samples of proportionality 1 to 6 were obtained.
<比較例1〜16>
上記実施例と同様にして、表1に示すように、各比較例に対応する合金組成のAl合金鋳造部材としての鍛造素材をを作製した。
<Comparative Examples 1-16>
In the same manner as in the above examples, as shown in Table 1, forging materials were produced as Al alloy cast members having an alloy composition corresponding to each comparative example.
さらにその鍛造素材を、表1に示す条件で予備加熱した後、丸棒側面方向から厚さ10mmに据え込んだ。続けて、その据込品(鍛造製品)に表1に示す条件で溶体化処理を施した。 Further, the forging material was preheated under the conditions shown in Table 1, and then placed to a thickness of 10 mm from the side surface of the round bar. Subsequently, the upsetting product (forged product) was subjected to a solution treatment under the conditions shown in Table 1.
その後、その据込品に対し、上記と同様の自然時効を行った後、もしくは自然時効を行わずに直ちに、上記と同様の人工時効処理を行った。 Thereafter, the artificial aging treatment similar to that described above was performed on the installed product after performing natural aging similar to the above or immediately without performing natural aging.
<評価> <Evaluation>
表2に示すように、得られた試料(サンプル)を、溶剤除去性浸透探傷試験(カラーチェック)により試料表面の割れ及び穴欠陥の有無を確認した後、試料を切断し、断面を研磨した。その後、研磨した試料をエッチングし、光路に偏光ガラスを挿入した金属顕微鏡にて観察し、表面及び内部における粗大再結晶の有無を確認した。 As shown in Table 2, the obtained sample (sample) was checked for the presence of cracks and hole defects on the sample surface by a solvent-removable penetrant flaw detection test (color check), and then the sample was cut and the cross section was polished. . Thereafter, the polished sample was etched and observed with a metal microscope having a polarizing glass inserted in the optical path to confirm the presence or absence of coarse recrystallization on the surface and inside.
なお、結晶粒径の測定は、光学顕微鏡写真上で切片法によって求め、500μm以上の結晶粒がある場合について、粗大再結晶粒「有り」と判断し、それ以外の場合を粗大再結晶粒「無し」と判断した。 The crystal grain size is measured by a section method on an optical microscope photograph. When there are crystal grains of 500 μm or more, it is determined that there is a coarse recrystallized grain “exist”, and otherwise, the coarse recrystallized grain “ It was judged as “None”.
また、顕微鏡観察の際には、切削性を悪化させるTi系の金属間化合物がないかどうかについても確認した。 In addition, it was also confirmed whether there was any Ti-based intermetallic compound that deteriorated the machinability during microscopic observation.
更に、元々の素材長手方向に平行な方向からJIS14A比例試験片を採取し、引張強度、0.2%耐力、破断伸びを測定した。 Furthermore, a JIS 14A proportional test piece was taken from a direction parallel to the original material longitudinal direction, and tensile strength, 0.2% proof stress, and elongation at break were measured.
また据込品から、2mm×4.3mm×42.4mmの試験片を切り出し、4.3mm×42.4mmの面の中央部に、3点曲げ治具を用いて耐力の70%に相当する応力を負荷した。負荷の際には、試験片と治具との間は電気的に絶縁した。腐食液として、純水1リットル当り、酸化クロム(IV)36g、二クロム酸カリウム30g、塩化ナトリウム3
gを溶解させ、95〜100℃に保持した溶液を用意した。応力を負荷した試験片をこの腐食液中に16時間浸漬した後に、試験片を外観観察し、割れが発生しているかどうかについて確認した。
In addition, a test piece of 2 mm × 4.3 mm × 42.4 mm is cut out from the installed product, and it corresponds to 70% of the proof stress using a three-point bending jig in the center of the 4.3 mm × 42.4 mm surface. Stress was applied. During the load, the test piece and the jig were electrically insulated. As a corrosive liquid, 36 g of chromium (IV) oxide, 30 g of potassium dichromate, 3 sodium chloride per liter of pure water
The solution which melt | dissolved g and was hold | maintained at 95-100 degreeC was prepared. After the test piece loaded with stress was immersed in the corrosive liquid for 16 hours, the appearance of the test piece was observed to confirm whether cracks were generated.
なお、表2においては、データの比較を容易に行えるように、実施例1〜7のサンプルと、対比例1〜7のサンプル(自然時効を行った以外は実施例1〜7と同様のもの)とを同行に記載している。すなわち「実施例/対比例」の各行において、「自然時効無[B]」の列には、実施例サンプルの物性値(引張強度、0.2%耐力、破断伸び)が記載され、「自然時効有[A]」の列には、対比例サンプルの物性値(引張強度、0.2%耐力、破断伸び)がそれぞれ記載されている。さらに「割れ、穴欠陥の有無」「粗大再結晶の有無」「応力腐食割れの有無」の各評価については、実施例のものも、対比例のものも同じ評価結果となるため、列を分けずに同列に記載している。 In Table 2, the samples of Examples 1 to 7 and the samples of Comparative Examples 1 to 7 (same as those of Examples 1 to 7 except that natural aging was performed so that the data can be easily compared) ) In the same bank. That is, in each column of “Example / Comparison”, the column of “Natural aging [B]” describes the physical property values (tensile strength, 0.2% proof stress, elongation at break) of the Example sample. In the column “Aging [A]”, the physical property values (tensile strength, 0.2% proof stress, elongation at break) of the comparative sample are described. Furthermore, for each evaluation of “presence / absence of cracks and hole defects”, “presence / absence of coarse recrystallization”, and “presence / absence of stress corrosion cracking”, the evaluation results are the same for both the example and the comparative example. It is listed in the same column.
また各比較例1〜16において、物性値(引張強度、0.2%耐力、破断伸び)については、自然時効を行ったもの(「自然時効有[A]」)と、自然時効を行わなかったもの(「自然時効無[B]」)との各2種類のサンプルに対する評価結果がそれぞれ記載されている。さらに「割れ、穴欠陥の有無」「粗大再結晶の有無」「応力腐食割れの有無」の各評価については、自然時効の有無にかかわらず、同じ評価結果となるため、列を分けずに同列に記載している。 In each of Comparative Examples 1 to 16, the physical property values (tensile strength, 0.2% proof stress, elongation at break) were those subjected to natural aging (“natural aging present [A]”) and natural aging was not performed. The evaluation results for each of the two types of samples are described. In addition, the evaluation results for “existence of cracks and hole defects”, “existence of coarse recrystallization”, and “existence of stress corrosion cracking” are the same regardless of whether there is natural aging. It is described in.
<結果>
本発明の要件を全て満たしている実施例1〜6については、試料に割れ及び穴欠陥は発生せず、表面及び内部に粗大な再結晶は認められなかった。更に実施例1〜7は、引張強度、0.2%耐力、破断伸びがそれぞれ優れており、優れた物性(特性)を備えるものであった。なおこれらの物性の良否を判断するに際しては、引張強度が400MPa以上、0.2%耐力が350MPa以上、伸びが10%以上のものを「優れている」と評価した。
<Result>
About Examples 1-6 which satisfy | fill all the requirements of this invention, a crack and a hole defect did not generate | occur | produce in the sample, but the coarse recrystallization was not recognized by the surface and the inside. Further, Examples 1 to 7 were excellent in tensile strength, 0.2% proof stress, and elongation at break, and had excellent physical properties (characteristics). In judging the quality of these physical properties, those having a tensile strength of 400 MPa or more, a 0.2% proof stress of 350 MPa or more, and an elongation of 10% or more were evaluated as “excellent”.
自然時効を行わない場合(実施例[B])に対し、自然時効を行った場合(対比例[A])における各特性値の低下率([A]/[B])に関しても、実施例1〜7のものは、対比例に対しても遜色がなく、優れた評価が得られた。 In the case where natural aging is not performed (example [B]), the reduction rate ([A] / [B]) of each characteristic value when natural aging is performed (comparative [A]) is also described in the example. Those of Nos. 1 to 7 were not inferior to the proportionality, and excellent evaluation was obtained.
なお本実施例においては、自然時効有無による物性値低下率の良否を判断するに際しては、低下率が1.05以下のものを「優れている」と評価した。 In this example, when determining whether the rate of decrease in the physical property value due to the presence or absence of natural aging was good or bad, those having a rate of decrease of 1.05 or less were evaluated as “excellent”.
比較例1のものは、Mg含有量が少ないため、自然時効の有無にかかわらず、引張強度、0.2%耐力が不十分であった。また自然時効を省略したものでは、引張強度及び0.2%耐力等の特性が低下していた。 In Comparative Example 1, since the Mg content was small, the tensile strength and 0.2% proof stress were insufficient regardless of the presence or absence of natural aging. In addition, when natural aging was omitted, properties such as tensile strength and 0.2% proof stress were lowered.
比較例2のものは、Mg及びZnの含有量が少ないため、自然時効を省略したものでは、引張強度及び0.2%耐力等の特定が低下していた。 In Comparative Example 2, since the contents of Mg and Zn were small, the specifications such as tensile strength and 0.2% proof stress were lowered in cases where natural aging was omitted.
比較例3のものは、Fe、Mn及びZrの含有量が少ないため、自然時効の有無にかかわらず、加工ひずみが溶体化により開放される際に、表面及び内部に粗大再結晶を生じた。また、この粗大再結晶により引張特性、特に伸びが大幅に低下していた。 In Comparative Example 3, the content of Fe, Mn, and Zr was small, and therefore, regardless of the presence or absence of natural aging, coarse recrystallization occurred on the surface and inside when the processing strain was released by solution treatment. Further, this coarse recrystallization significantly reduced the tensile properties, particularly the elongation.
比較例4のものは、Ti−B添加量が少なく、結果的にTi含有量が少ないため、鋳造時に結晶粒が微細化できず、鋳塊割れを生じた。 In Comparative Example 4, the Ti-B addition amount was small, and as a result, the Ti content was small, so that the crystal grains could not be refined during casting, and ingot cracking occurred.
比較例5のものは、Cu、Mg及びZn添加量が少ないため、自然時効の有無にかかわらず、引張強度及び0.2%耐力等の物性が低下していた。 In Comparative Example 5, since the addition amount of Cu, Mg and Zn was small, physical properties such as tensile strength and 0.2% proof stress were lowered regardless of the presence or absence of natural aging.
比較例6のものは、Mg含有量及びSi含有量がいずれも多すぎるため、引張強度及び0.2%耐力は優れているものの、自然時効を省略したものでは特性が低下していた。 In Comparative Example 6, since both the Mg content and the Si content are too large, the tensile strength and the 0.2% proof stress are excellent, but the characteristics were deteriorated when natural aging was omitted.
比較例7のものは、Mg含有量が多すぎるため、伸びが大きく低下していた。 In Comparative Example 7, the elongation was greatly reduced because the Mg content was too high.
比較例8のものは、Zn含有量が少ないため、主要強化成分の析出強化が十分に行われず、引張強度及び0.2%耐力が低下していた。 In Comparative Example 8, since the Zn content was small, the precipitation strengthening of the main strengthening component was not sufficiently performed, and the tensile strength and the 0.2% yield strength were reduced.
比較例9のもは、Zn含有量が多すぎたため、アルミニウムよりも卑な金属間化合物が粒界に多量に連続析出し、この粒界に沿って応力腐食割れが生じた。 In Comparative Example 9, since the Zn content was too large, a large amount of base intermetallic compounds than aluminum precipitated continuously at the grain boundaries, and stress corrosion cracking occurred along these grain boundaries.
比較例10のものは、Mg含有量が多すぎたため、アルミニウムよりも卑な金属間化合物が粒界に多量に連続析出し、この粒界に沿って応力腐食割れが生じた。 In Comparative Example 10, since the Mg content was too large, a larger amount of intermetallic compounds than aluminum were continuously precipitated at the grain boundaries, and stress corrosion cracking occurred along these grain boundaries.
比較例11のものは、[Zr量]+[Ti量]が0.2質量%以上であるため、光学顕微鏡観察にて、機械加工の際に刃具の摩耗やバリの発生の原因となるTi系の金属間化合物が多数観察された。 In Comparative Example 11, since [Zr amount] + [Ti amount] is 0.2% by mass or more, it is a cause of wear of blades and generation of burrs during machining by observation with an optical microscope. Many intermetallic compounds of the system were observed.
比較例12のものは、鍛造温度が低すぎため、伸び不足による限界割れを生じた。 Since the forging temperature of the comparative example 12 was too low, a critical crack was generated due to insufficient elongation.
比較例13のものは、鍛造温度が高すぎたため、熱間脆化による粒界割れを生じた。 Since the forging temperature of the comparative example 13 was too high, intergranular cracking due to hot embrittlement occurred.
比較例14のものは、溶体化温度が低すぎたため、析出強化元素の固溶が十分に行われず、析出量が不足したため、引張強度、0.2%耐力が低下していた。 In Comparative Example 14, since the solution temperature was too low, the precipitation strengthening element was not sufficiently dissolved, and the amount of precipitation was insufficient, so that the tensile strength and 0.2% proof stress were lowered.
比較例15のものは、溶体化温度温度が高すぎたため、共晶融解を生じ、試料の表面に穴欠陥を生じた。 In Comparative Example 15, since the solution temperature was too high, eutectic melting occurred, resulting in hole defects on the surface of the sample.
以上の実施例から明らかように、本発明によれば、自然時効を行わずとも、引張強度、0.2%耐力、破断伸び等の各種物性に優れたAl−Zn−Mg系鍛造製品を得ることができ、高品質のAl合金鍛造製品を効率良く安価に製造することができる。 As is clear from the above examples, according to the present invention, an Al—Zn—Mg based forged product excellent in various physical properties such as tensile strength, 0.2% proof stress and elongation at break can be obtained without performing natural aging. It is possible to produce a high-quality Al alloy forged product efficiently and inexpensively.
本発明のAl合金鍛造製品の製造方法は、高品質のAl鍛造製品を製造するための鍛造加工技術に適用可能である。 The method for producing an Al alloy forged product according to the present invention can be applied to a forging technique for producing a high-quality Al forged product.
1:オートバイフレーム(鍛造製品) 1: Motorcycle frame (forged products)
Claims (5)
前記Al合金鍛造素材に対し、350〜500℃の温度で熱間鍛造を行った後、400〜500℃の温度で溶体化処理を行うことにより、Al合金鍛造製品を得る工程と、
前記Al合金鍛造製品に対し、自然時効処理を行わずに、人工時効処理を行う工程と、を含むことを特徴とするAl合金鍛造製品の製造方法。 Fe: 0.2-0.35 mass%, Cu: 0.05-0.20 mass%, Mn: 0.3-0.6 mass%, Mg: 1.3-2.0 mass%, Zn: 4.6 to 5.1% by mass, Si: less than 0.30% by mass, Zr: 0.1% by mass or more and less than 0.2% by mass in total with Ti, “[Ti mass%] / Satisfying the relationship of [Zr mass%] ≧ 0.2 ”, and obtaining an Al alloy forging material having an alloy composition with the balance consisting of Al and inevitable impurities;
A process of obtaining an Al alloy forged product by performing a solution treatment at a temperature of 400 to 500 ° C. after hot forging at a temperature of 350 to 500 ° C. with respect to the Al alloy forged material,
A step of performing artificial aging treatment on the Al alloy forged product without performing natural aging treatment on the Al alloy forged product.
前記Al合金鋳造部材を前記Al合金鍛造素材として用いるようにした請求項1に記載のAl合金鍛造製品の製造方法。 The method further includes a step of obtaining an Al alloy cast member by subjecting the Al alloy molten metal having the alloy composition to a homogenization treatment for an Al alloy ingot obtained by continuous casting,
The method for producing an Al alloy forged product according to claim 1, wherein the Al alloy cast member is used as the Al alloy forged material.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2011155609A1 (en) * | 2010-06-11 | 2011-12-15 | 昭和電工株式会社 | Method for producing al alloy joined body |
| JP2015007273A (en) * | 2013-06-25 | 2015-01-15 | 株式会社神戸製鋼所 | Aluminum alloy cast material for weld structural member and manufacturing method thereof |
| JP2015007274A (en) * | 2013-06-25 | 2015-01-15 | 株式会社神戸製鋼所 | Aluminum alloy cast material for weld structural member and manufacturing method thereof |
| CN111500909A (en) * | 2020-05-12 | 2020-08-07 | 吉林市江机机械设备制造有限公司 | Cast aluminum alloy material and preparation method thereof |
| CN112191795A (en) * | 2020-09-30 | 2021-01-08 | 贵州安大航空锻造有限责任公司 | Forging and pressing forming method for large-scale forge piece |
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| JPH10280081A (en) * | 1997-04-08 | 1998-10-20 | Sky Alum Co Ltd | Frame-shaped member with high strength and high precision, made of al-zn-mg alloy, and its production |
| WO2008044642A1 (en) * | 2006-10-05 | 2008-04-17 | Showa Denko K.K. | Aluminum alloy forged product and method of producing the same |
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| JPH10280081A (en) * | 1997-04-08 | 1998-10-20 | Sky Alum Co Ltd | Frame-shaped member with high strength and high precision, made of al-zn-mg alloy, and its production |
| WO2008044642A1 (en) * | 2006-10-05 | 2008-04-17 | Showa Denko K.K. | Aluminum alloy forged product and method of producing the same |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
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| WO2011155609A1 (en) * | 2010-06-11 | 2011-12-15 | 昭和電工株式会社 | Method for producing al alloy joined body |
| EP2592170A4 (en) * | 2010-06-11 | 2017-06-28 | Showa Denko K.K. | Method for producing al alloy joined body |
| JP2015007273A (en) * | 2013-06-25 | 2015-01-15 | 株式会社神戸製鋼所 | Aluminum alloy cast material for weld structural member and manufacturing method thereof |
| JP2015007274A (en) * | 2013-06-25 | 2015-01-15 | 株式会社神戸製鋼所 | Aluminum alloy cast material for weld structural member and manufacturing method thereof |
| CN111500909A (en) * | 2020-05-12 | 2020-08-07 | 吉林市江机机械设备制造有限公司 | Cast aluminum alloy material and preparation method thereof |
| CN112191795A (en) * | 2020-09-30 | 2021-01-08 | 贵州安大航空锻造有限责任公司 | Forging and pressing forming method for large-scale forge piece |
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