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JP2008106848A - Al-based composite screw and its manufacturing method - Google Patents

Al-based composite screw and its manufacturing method Download PDF

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JP2008106848A
JP2008106848A JP2006290155A JP2006290155A JP2008106848A JP 2008106848 A JP2008106848 A JP 2008106848A JP 2006290155 A JP2006290155 A JP 2006290155A JP 2006290155 A JP2006290155 A JP 2006290155A JP 2008106848 A JP2008106848 A JP 2008106848A
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screw
composite material
mold
melt
reinforcing material
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Inventor
Shoji Taniguchi
尚司 谷口
Atsuyuki Kobayashi
敬幸 小林
Yoji Kato
洋史 加藤
Kenji Ishimoto
健司 石本
Heishiro Takahashi
平四郎 高橋
Shinichi Sasaki
伸一 佐々木
Masahito Iguchi
真仁 井口
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Tohoku University NUC
Taiheiyo Cement Corp
NTK Ceratec Co Ltd
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Tohoku University NUC
Nihon Ceratec Co Ltd
Taiheiyo Cement Corp
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Priority to JP2006290155A priority Critical patent/JP2008106848A/en
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/25Process efficiency

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Abstract

【課題】室温での塑性変形加工により容易かつ高い生産性で安価に製造することができるAl基複合材製ネジおよびその製造方法を提供する。
【解決手段】Al基複合材製ネジ10は、Al基金属を主成分とした軸芯部12の外側に、軸芯部12と同種のAl基金属に強化材粒子が分散されてなる複合材料からなるネジ山部14が、この軸芯部12と連続して形成された構造を有している。このネジ10は、鋳型22内で強化材粒子44を分散させたAl基融体42を生成し、強化材粒子44がAl基融体42の周縁部に移動するようにAl基融体42を構成する溶融金属に電磁力を作用させ、Al基融体42を固化させて鋳型22から複合材からなる無垢棒を取り出し、これに転造法によりネジ山を形成することで製造される。
【選択図】図1
An Al-based composite material screw that can be easily and inexpensively manufactured by plastic deformation at room temperature and a manufacturing method thereof.
An Al-based composite material screw 10 is a composite material in which reinforcing material particles are dispersed in an Al-based metal of the same type as the shaft core portion 12 outside the shaft core portion 12 mainly composed of an Al-based metal. The screw thread part 14 which consists of has the structure formed continuously with this axial core part 12. As shown in FIG. The screw 10 generates an Al-based melt 42 in which reinforcing material particles 44 are dispersed in the mold 22, and the Al-based melt 42 is moved so that the reinforcing material particles 44 move to the peripheral portion of the Al-based melt 42. It is manufactured by applying an electromagnetic force to the molten metal constituting, solidifying the Al-based melt 42, taking out a solid rod made of a composite material from the mold 22, and forming a thread on this by a rolling method.
[Selection] Figure 1

Description

本発明は、金属AlまたはAl合金と、セラミックスとからなる複合材料を用いてなるAl基複合材製ネジとその製造方法に関する。   The present invention relates to an Al-based composite material screw made of a composite material made of metal Al or an Al alloy and ceramics, and a method for manufacturing the same.

近時、エンジンや自転車等の軽量化が望まれる分野では、その組み立てに使用されているネジを、従来の鉄製やステンレス製のものから、軽量なアルミ製のものに替える動きが広まっている。   Recently, in fields where weight reduction of engines, bicycles, and the like is desired, there has been a widespread movement of replacing screws used for assembly from those made of conventional iron or stainless steel to those made of lightweight aluminum.

しかしながら、アルミ製ネジは、強度が小さく、ネジ山が塑性変形し易いために、締め直しが困難であるという欠点がある。そのため、例えば、アルミサッシ窓の枠部材の組み立てにはステンレス製ネジが用いられている。このため、解体後のアルミリサイクルプロセスにおいては、全てのネジを取り外す必要があり、そのためのコストがかかる。   However, the aluminum screw has a drawback that it is difficult to retighten because the strength is small and the screw thread is easily plastically deformed. Therefore, for example, stainless steel screws are used for assembling the frame member of the aluminum sash window. For this reason, in the aluminum recycling process after dismantling, it is necessary to remove all the screws, which is costly.

そこで、例えば、金属をマトリックスとし、強化材としてセラミックス粒子を分散させた複合材料からなるネジが検討されている(例えば、特許文献1参照)。しかしながら、このような複合材料製のネジでは、ネジ山を温間鍛造や切削加工により形成する必要があるので、加工コストが高くなるという問題がある。
特開2000−343178号公報(段落[0009]、[0010]、[0016]等)
Therefore, for example, a screw made of a composite material in which a metal is used as a matrix and ceramic particles are dispersed as a reinforcing material has been studied (for example, see Patent Document 1). However, in such a composite screw, it is necessary to form a screw thread by warm forging or cutting, and there is a problem that the processing cost increases.
JP 2000-343178 A (paragraphs [0009], [0010], [0016], etc.)

本発明はかかる事情に鑑みてなされたものであり、室温での塑性変形加工により容易かつ高い生産性で安価に製造することができるAl基複合材製ネジおよびその製造方法を提供することを目的とする。   The present invention has been made in view of such circumstances, and an object thereof is to provide an Al-based composite material screw that can be easily and inexpensively manufactured by plastic deformation at room temperature and a manufacturing method thereof. And

本発明に係るAl基複合材製ネジは、軸芯部はAl基金属を主成分としており、この軸芯部と同種のAl基金属に強化材粒子が分散されてなる複合材料からなるネジ山部が、この軸芯部の外側にこの軸芯部と連続して形成された構造を有していることを特徴としている。   In the Al-based composite material screw according to the present invention, the shaft core portion is mainly composed of an Al-based metal, and a thread made of a composite material in which reinforcing material particles are dispersed in the same Al-based metal as the shaft core portion. The portion has a structure formed on the outside of the shaft core portion so as to be continuous with the shaft core portion.

このようなAl基複合材製ネジは、鋳型内で強化材粒子を分散させたAl基融体を生成する工程と、強化材粒子がAl基融体の周縁部に移動するようにAl基融体を構成する溶融金属に電磁力を作用させる工程と、Al基融体を固化させて鋳型から複合材からなる無垢棒を取り出す工程と、無垢棒に転造法によりネジ山を形成する工程とを経ることによって製造される。   Such an Al-based composite screw includes a step of generating an Al-based melt in which reinforcing material particles are dispersed in a mold, and an Al-based melting so that the reinforcing material particles move to the peripheral portion of the Al-based melt. A step of applying electromagnetic force to the molten metal constituting the body, a step of solidifying the Al-based melt and taking out a solid bar made of a composite material from a mold, and a step of forming a thread on the solid bar by a rolling method Manufactured by going through.

本発明によれば、外周部がAl基金属と強化材との複合材料からなり、軸芯部(中心部)がAl基金属からなる棒状基材を用いることにより、金属製のネジの製造に広く用いられている転造法を用いてAl基複合材製ネジを製造することができる。これにより、高強度なネジを、容易かつ高い生産性で安価に製造することができる。   According to the present invention, the outer peripheral portion is made of a composite material of an Al-base metal and a reinforcing material, and the shaft core portion (center portion) is made of an Al-base metal. Al-based composite screws can be manufactured using widely used rolling methods. Thereby, a high-strength screw can be manufactured easily and inexpensively with high productivity.

以下に本発明の実施の形態について図面を参照して詳細に説明する。図1はAl基金属−セラミックス複合材料からなるネジ(以下「Al基複合材製ネジ」という)の組織構造を模式的に示す断面図である。   Embodiments of the present invention will be described below in detail with reference to the drawings. FIG. 1 is a cross-sectional view schematically showing the structure of a screw made of an Al-based metal-ceramic composite material (hereinafter referred to as “Al-based composite material screw”).

図1に示されるように、Al基複合材製ネジ10は、Al基金属を主成分とする軸芯部12と、軸芯部12の外側に軸芯部12と連続して形成され、軸芯部12と同種のAl基金属に強化材粒子が分散されてなる複合材料からなるネジ山部14を有している。このような構造により、Al基複合材製ネジ10は、純Al製ネジと比較して、高い強度を示す。   As shown in FIG. 1, an Al-based composite material screw 10 is formed continuously with an axial core portion 12 mainly composed of an Al-based metal and an axial core portion 12 outside the axial core portion 12. It has a threaded portion 14 made of a composite material in which reinforcing material particles are dispersed in the same Al-based metal as the core portion 12. With such a structure, the Al-based composite material screw 10 exhibits higher strength than a pure Al screw.

なお、Al基複合材製ネジ10の頭部16もまた、その中心部はAl基金属からなり、その外周部は複合材料からなる。これは、後述する通り、Al基複合材製ネジ10の製造方法に由来する。   The head portion 16 of the Al-based composite material screw 10 is also made of an Al-based metal at the center, and a composite material at the outer peripheral portion. This is derived from the manufacturing method of the Al-based composite screw 10 as described later.

Al基金属としては、純AlやAl−Mg系合金等が好適に用いられるが、これらに限定されるものではない。また、強化材粒子としては、SiC,Si,Al,AlN等のセラミックス粒子が好適に用いられ、これらは1種のみがAl基金属に添加されていてもよいし、2種以上がAl基金属に添加されていてもよい。さらに強化材粒子はこれらに限定されるものではなく、Al基金属よりも融点が高く、Al基金属と合金を形成しない金属材料、例えば、合金より析出する金属Si等であってもよい。 As the Al-based metal, pure Al, Al—Mg-based alloy, or the like is preferably used, but is not limited thereto. Further, as the reinforcing material particles, ceramic particles such as SiC, Si 3 N 4 , Al 2 O 3 , and AlN are preferably used, and only one kind of these may be added to the Al-based metal. More than seeds may be added to the Al-based metal. Further, the reinforcing material particles are not limited to these, and may be a metal material having a melting point higher than that of the Al-based metal and not forming an alloy with the Al-based metal, for example, metal Si precipitated from the alloy.

次に、このような構造を有するAl基複合材製ネジ10の製造方法について説明する。図2にAl基複合材製ネジ10の製造に用いる無垢棒の製造装置の概略構成例を示す。この製造装置20は、Al基金属を溶融させるための有底円筒形状の鋳型(坩堝)22と、この鋳型22を鉛直姿勢で支持する台座部24と、鋳型22を囲繞するように設けられた誘導コイル26と、誘導コイル26に高周波電流を供給するための高周波電源28を有している。鋳型22には、鋳型22に充填された金属原料の高周波誘導加熱時および鋳型22内のAl基融体の電磁分離(交流磁場印加)時にその影響を受け難い材料、具体的には、SiO(石英ガラス、合成石英)製のものが好適である。台座部24は耐熱レンガ等を用いることができる。誘導コイル26の線径やターン数(巻き数)は鋳型22の大きさや鋳型22に投入される金属の溶解能力を考慮して、適宜、設定される。高周波電源28は、鋳型22に充填された金属原料の高周波誘導加熱と鋳型22内のAl基融体の電磁分離を行うことができるように、周波数と出力を調節する機能を有する。 Next, a method for manufacturing the Al-based composite screw 10 having such a structure will be described. FIG. 2 shows a schematic configuration example of a solid bar manufacturing apparatus used for manufacturing the Al-based composite material screw 10. The manufacturing apparatus 20 is provided so as to surround the casting mold 22 with a bottomed cylindrical mold (crucible) 22 for melting the Al-based metal, a pedestal portion 24 that supports the casting mold 22 in a vertical posture, and the casting mold 22. An induction coil 26 and a high frequency power supply 28 for supplying a high frequency current to the induction coil 26 are provided. The mold 22 is made of a material that is not easily affected by high-frequency induction heating of the metal raw material filled in the mold 22 and electromagnetic separation (AC magnetic field application) of the Al-based melt in the mold 22, specifically, SiO 2. Those made of (quartz glass, synthetic quartz) are preferred. The pedestal portion 24 can use heat-resistant bricks or the like. The wire diameter and the number of turns (the number of turns) of the induction coil 26 are appropriately set in consideration of the size of the mold 22 and the melting ability of the metal put into the mold 22. The high frequency power supply 28 has a function of adjusting the frequency and output so that high frequency induction heating of the metal raw material filled in the mold 22 and electromagnetic separation of the Al-based melt in the mold 22 can be performed.

なお、製造装置20に、鋳型22を冷却するための冷却水を鋳型22の外周に吹き付けるための冷却水スプレー装置、鋳型22内の溶融物を撹拌するための撹拌棒、鋳型22とこのような冷却水スプレー管をその内部に収容し、誘導コイル26がその外部に配置されるように設置される保護管を設けることも好ましい。   In addition, a cooling water spray device for spraying cooling water for cooling the mold 22 on the outer periphery of the mold 22, a stirring rod for stirring the melt in the mold 22, the mold 22, and the like It is also preferable to provide a protective pipe that is installed so that the cooling water spray pipe is accommodated therein and the induction coil 26 is disposed outside thereof.

また、製造装置20は、1本の誘導コイルが高周波誘導加熱と電磁分離の両方を行う構成となっているが、高周波誘導加熱用コイルと電磁分離用コイルを別々に備えており、各コイルにそれぞれの駆動電源が接続された構成としてもよい。   In addition, the manufacturing apparatus 20 has a configuration in which one induction coil performs both high-frequency induction heating and electromagnetic separation, but the high-frequency induction heating coil and the electromagnetic separation coil are separately provided, It is good also as a structure where each drive power supply was connected.

Al基複合材製ネジ10の製造に用いる無垢棒の製造は、まず、鋳型22に原料たるAl基金属の粉末(または塊状物)と強化材粉末を所定比で充填し、これを高周波誘導加熱することで、強化材粒子が分散したAl基融体を生成させる。このAl基融体を撹拌して強化材粒子の分布の均一化を図ることも好ましい。   The solid rod used in the manufacture of the Al-based composite screw 10 is manufactured by first filling the mold 22 with the Al-based metal powder (or lump) and the reinforcing material powder in a predetermined ratio, and subjecting this to high-frequency induction heating. By doing so, an Al-based melt in which reinforcing material particles are dispersed is generated. It is also preferable to stir the Al-based melt to make the distribution of reinforcing material particles uniform.

なお、強化材粒子が分散したAl基融体を生成させることができる限りにおいて、原料に制限はない。例えば、最初に純Alを鋳型22に投入してAl融体を生成させ、これに強化材粒子を添加して混合したり、或いは強化材粒子を含有するAl基金属を添加して溶解混合する等の方法も好適に用いられる。   The raw material is not limited as long as an Al-based melt in which reinforcing material particles are dispersed can be generated. For example, first, pure Al is put into the mold 22 to produce an Al melt, and reinforcing material particles are added to and mixed with this, or an Al-based metal containing reinforcing material particles is added and dissolved and mixed. Such a method is also preferably used.

Al基融体の温度を一定とした後に高周波誘導加熱電源を切り、続いて電磁分離用コイルに所定周波数の交流電流を流す。これにより鋳型22内のAl基融体に電磁力を作用させて、強化材粒子をAl基融体の周縁部に移動、集積させる。   After making the temperature of the Al-based melt constant, the high-frequency induction heating power supply is turned off, and then an alternating current of a predetermined frequency is passed through the electromagnetic separation coil. Thus, electromagnetic force is applied to the Al-based melt in the mold 22 to move and accumulate the reinforcing material particles on the peripheral portion of the Al-based melt.

図3に強化材粒子の移動メカニズムを模式的に示す。誘導コイル26に交流電流を通電することで発生する交流磁場32とAl基融体42中に誘導される誘導電流34との相互作用によって電磁力36が生じ、この電磁力36が発生しない強化材粒子44には電磁力36とは反対の方向に力がかかる。この反対の方向がAl基融体42の外周へと向かう方向となるので、この作用を利用して強化材粒子44をAl基融体42の周縁部に集積させることができる。   FIG. 3 schematically shows the movement mechanism of the reinforcing material particles. An electromagnetic force 36 is generated by the interaction between the AC magnetic field 32 generated by applying an AC current to the induction coil 26 and the induction current 34 induced in the Al-based melt 42, and the reinforcing material does not generate this electromagnetic force 36. A force is applied to the particle 44 in a direction opposite to the electromagnetic force 36. Since the opposite direction is the direction toward the outer periphery of the Al-based melt 42, the reinforcing material particles 44 can be accumulated on the peripheral portion of the Al-based melt 42 using this action.

このような電磁分離のメカニズムから、Al基金属と強化材粒子との組み合わせは、両者に導電性の差があるものであればよく、強化材粒子の濃度にも制限がないことがわかる。   From such an electromagnetic separation mechanism, it can be seen that the combination of the Al-based metal and the reinforcing material particles only needs to have a difference in conductivity, and the concentration of the reinforcing material particles is not limited.

この電磁分離用コイルへの給電方法には、一定時間連続して電流を流す方法が好適に用いられる。   As a method for supplying power to the electromagnetic separation coil, a method of flowing a current continuously for a predetermined time is preferably used.

強化材粒子の集積幅(以下、「表皮厚さ」という)の制御は電磁分離の際にコイルに流す電流の周波数により調節することができる。この表皮厚さδは、δ=(πμσf)−1/2(透磁率μ=4π×10−7H・m−1、導電率σ=3.80×10Ω−1−1、f:周波数)により求められる。 Control of the reinforcing particle accumulation width (hereinafter referred to as “skin thickness”) can be adjusted by the frequency of the current flowing through the coil during electromagnetic separation. This skin thickness δ is δ = (πμ e σf) −1/2 (permeability μ e = 4π × 10 −7 H · m −1 , conductivity σ = 3.80 × 10 6 Ω −1 m − 1 , f: frequency).

したがって、先に示した図1ではネジ山部14全体が複合材料から形成されている形態としたが、表面のみが複合材料からなりその内側はAl基金属からなるネジ山部を有するAl基複合材製ネジもまた、このような強化材粒子の濃度や電磁分離の条件を制御することにより、製造することができることがわかる。   Accordingly, in FIG. 1 shown above, the entire thread portion 14 is formed of a composite material. However, only the surface is made of a composite material, and the inside thereof is an Al-based composite having a thread portion made of an Al-based metal. It can be seen that the material screw can also be manufactured by controlling the concentration of the reinforcing material particles and the electromagnetic separation conditions.

続いて、この電磁分離処理が終了したら、鋳型22を冷却してAl基融体を固化させる。これにより鋳型22内に、その中心部は金属成分が主成分となっており、外周部に強化材粒子が集積・分散した複合材からなる無垢棒が形成される。   Subsequently, when this electromagnetic separation process is completed, the mold 22 is cooled to solidify the Al-based melt. As a result, a solid rod made of a composite material in which a metal component is a main component in the mold 22 and the reinforcing material particles are accumulated and dispersed in the outer periphery is formed in the mold 22.

この無垢棒を鋳型22から取り出し、転造法によりこの無垢棒にネジ山を形成する。転造法は、冷間塑性変形加工の一種であって、ネジの一般的な製造方法として周知であり、丸棒材(無垢棒)をネジの形をした複数の円筒状の金型(ロール)で挟み込み、回転させながら押し付けることによって丸棒材を塑性変形させ、ネジ山の形を造る方法である。   The solid bar is taken out from the mold 22 and a thread is formed on the solid bar by a rolling method. The rolling method is a kind of cold plastic deformation process, and is well known as a general method for manufacturing screws. A round bar (solid bar) is a plurality of cylindrical molds (rolls) in the form of screws. ), And a round bar material is plastically deformed by pressing it while rotating and making a screw thread shape.

このようにAl基複合材製ネジ10の製造プロセスにおいては、強化材粒子を所望の部位に分散させてなる複合材無垢棒を、鋳型22内での原料溶融、強化材粒子の集積、固化という簡単な操作によって行うことができる。また、ネジ山の形成に汎用されているネジの成形技術を用いることができるので、生産性が高く、安価に製造することができる。   Thus, in the manufacturing process of the Al-based composite material screw 10, the solid composite rod in which the reinforcing material particles are dispersed in a desired portion is referred to as melting of raw materials in the mold 22, accumulation of reinforcing material particles, and solidification. This can be done with a simple operation. In addition, since a screw forming technique that is widely used for forming threads can be used, the productivity is high and the screw can be manufactured at low cost.

本例では単純化した鋳型構成を示したが、パイプ状鋳型の片端からAl基金属を連続的に供給し、電磁分離を行った後の他方端部に冷却機構を設けて、固化した丸棒を引き抜くことで、連続鋳造も可能である。   In this example, a simplified mold configuration was shown. However, a solid bar was prepared by continuously supplying Al-based metal from one end of a pipe-shaped mold and providing a cooling mechanism at the other end after electromagnetic separation. Continuous casting is also possible by pulling out.

(実施例1)
図2に示した構造を有し、かつ、表1に記載した規格で構成された製造装置を用いて、最初に所定量の純Alを鋳型中で高周波誘導加熱(周波数:30kHz)して溶解し、750℃に保持した。続いて、高周波誘導加熱を継続しながら、この溶融AlにSiC分散Al合金(Hydro Aluminium社製、Siが9%,Mgが6%で残部がAl、SiC:23重量%、SiC平均粒径:13μm(この合金からアルカリ抽出したSiC粒子のHELOS粒径分布装置による体積基準粒度分布からの算出による))を、Al基融体におけるSiC濃度が最終的に4.5重量%となるように所定量添加し、SiC分散Al基融体を生成させ、これを750℃に保持した。なお、SiC分散Al合金の溶解は、SiC粒子の電磁分離を防止するために、Al基融体を撹拌しながら行った。
(Example 1)
Using a manufacturing apparatus having the structure shown in FIG. 2 and configured according to the standards described in Table 1, first, a predetermined amount of pure Al is melted by high-frequency induction heating (frequency: 30 kHz) in a mold. And kept at 750 ° C. Subsequently, while continuing high-frequency induction heating, this molten Al was mixed with an SiC-dispersed Al alloy (manufactured by Hydro Aluminum, Si 9%, Mg 6%, the balance Al, SiC: 23% by weight, SiC average particle diameter: 13 μm (calculated from the volume-based particle size distribution of SiC particles alkali-extracted from this alloy by means of a HELOS particle size distribution device) so that the SiC concentration in the Al-based melt finally becomes 4.5% by weight. A fixed amount was added to produce a SiC-dispersed Al-based melt, which was maintained at 750 ° C. The SiC-dispersed Al alloy was dissolved while stirring the Al-based melt in order to prevent electromagnetic separation of the SiC particles.

SiC分散Al合金が完全に溶解して、その温度が750℃に安定した後に高周波誘導加熱を停止した。その後さらに20秒間、Al基融体を撹拌してSiC粒子を分散させた。その後速やかに誘導コイルに220アンペアの電流(周波数:30kHz)を30秒間連続して流すことで、Al基融体の電磁分離を行った。高周波電源を切って電磁分離を終了させ、試料を自然冷却、固化させた。鋳型から取り出した無垢棒の形状は、大凡、φ11mm×100mmであった。   High frequency induction heating was stopped after the SiC-dispersed Al alloy was completely dissolved and its temperature was stabilized at 750 ° C. Thereafter, the Al-based melt was further stirred for 20 seconds to disperse the SiC particles. Immediately after that, a 220 ampere current (frequency: 30 kHz) was continuously passed through the induction coil for 30 seconds to perform electromagnetic separation of the Al-based melt. The high frequency power supply was turned off to finish electromagnetic separation, and the sample was naturally cooled and solidified. The shape of the solid bar taken out from the mold was approximately φ11 mm × 100 mm.

この無垢棒をその長さ方向と垂直に切断し、その断面組織を光学顕微鏡により観察した。また、この無垢棒に転造法によりネジ山を形成し、得られたネジをその長さ方向と平行に切断して、その断面組織を光学顕微鏡で観察した。   The solid bar was cut perpendicular to the length direction, and the cross-sectional structure was observed with an optical microscope. Further, a thread was formed on this solid rod by a rolling method, and the obtained screw was cut in parallel with the length direction, and the cross-sectional structure was observed with an optical microscope.

図4に作製した無垢棒の断面の光学顕微鏡写真を示す。この写真に示されるように、無垢棒の周縁部に、SiC粒子の集積層が均一に形成されており、周波数30kHzの表皮厚さδ(=1.49mm)に対応していることが確認された。また、無垢棒の中心部分は金属Alが主成分となっていることが確認された。   FIG. 4 shows an optical micrograph of a cross section of the solid bar produced. As shown in this photograph, it was confirmed that the SiC particle accumulation layer was uniformly formed on the periphery of the solid bar, corresponding to the skin thickness δ (= 1.49 mm) at a frequency of 30 kHz. It was. In addition, it was confirmed that the central part of the solid bar is mainly composed of metal Al.

図5A〜5Dに作製したネジの断面の光学顕微鏡写真を示す。図5B,5C,5Dはそれぞれ図5A中の領域(a)部,(b)部,(c)部の拡大写真である。従来のSiCを金属Alに均一分散させた材料ではネジの作製に転造法を用いることはできなかったが、周縁部にSiCの集積層を形成し、中心部を金属Alで構成した円柱状複合材を用いれば、転造法によるネジ製造が可能であることが確認された。   The optical micrograph of the cross section of the produced screw is shown in FIGS. 5B, 5C, and 5D are enlarged photographs of regions (a), (b), and (c) in FIG. 5A, respectively. In the conventional material in which SiC is uniformly dispersed in metal Al, the rolling method could not be used for the production of the screw, but a cylindrical shape in which a SiC integrated layer was formed at the periphery and the center was composed of metal Al. It was confirmed that if a composite material is used, screws can be manufactured by a rolling method.

ネジ山部分の拡大写真に見られるように、加工前の無垢棒の状態と比較して、ネジ山部分ではSiC粒子の集積層が密になっている。これは、ネジ山が圧縮変形によって形作られるために、ネジの谷の部分のSiC粒子がネジ山へと押し寄せられたことによる結果であると考えられる。   As can be seen in the enlarged photograph of the thread portion, the SiC particle accumulation layer is denser in the thread portion than in the state of the solid rod before processing. This is thought to be a result of the SiC particles in the valley of the screw being pushed toward the thread because the thread is formed by compressive deformation.

(実施例2)
鋳型に最初に投入する金属として、実施例1の純Alに代えてAl合金(Al−7075)を用いたことと、SiC分散Al合金としてSiCの平均粒径が21μmのものをもちいたことの2点を除いて、実施例1と同じ手順に従い、ネジを作製した。ネジの断面の光学顕微鏡写真を図6に示す。図6B,6Cはそれぞれ図6A中の領域(a)部,(b)部の拡大写真である。
(Example 2)
As the metal initially put into the mold, Al alloy (Al-7075) was used in place of the pure Al of Example 1, and the SiC-dispersed Al alloy had an average SiC particle size of 21 μm. A screw was produced according to the same procedure as in Example 1 except for two points. An optical micrograph of the cross section of the screw is shown in FIG. 6B and 6C are enlarged photographs of regions (a) and (b) in FIG. 6A, respectively.

図6A〜6Cに示されるように、ネジ山の形状も崩れておらず、クラックの発生も見られないことから、主成分にAl基合金を用いた場合にも、転造法により容易にネジ形状に塑性変形加工することができるということが確認できた。また、ネジ山部分にSiC粒子が均一に分散していることが確認できた。
As shown in FIGS. 6A to 6C, the shape of the screw thread is not collapsed and cracks are not observed. Therefore, even when an Al-based alloy is used as the main component, the screw can be easily formed by the rolling method. It was confirmed that it can be plastically deformed into a shape. It was also confirmed that SiC particles were uniformly dispersed in the thread portion.

(トルク試験)
実施例2のネジを再び製造し、そのトルク試験を以下の方法で行った。すなわち、ネジの軸部の万力で挟んで固定し、ネジ部にステンレス製のナットを嵌め込む。その上からさらにステンレス製の長ナットを嵌め込み、下部のナットをスパナで固定しながら、上部の長ナットを10N・m刻みのトルクで締め込み、ネジ部が破断する締め付けトルクの値を求めた。比較のために、実施例2のネジの基材であるAl−7075合金のみからなるネジを2本作製して、同様に締め付けトルクを測定した。
(Torque test)
The screw of Example 2 was manufactured again, and the torque test was performed by the following method. That is, it fixes by pinching with the vise of the axial part of a screw, and a stainless steel nut is inserted in a screw part. A stainless steel long nut was further fitted from above, and the lower nut was fixed with a wrench, and the upper long nut was tightened with a torque in increments of 10 N · m, and a tightening torque value at which the threaded portion was broken was obtained. For comparison, two screws made only of an Al-7075 alloy, which is the base material of the screw of Example 2, were produced, and the tightening torque was measured in the same manner.

測定結果を表2に示す。実施例2のネジの規格はM12である。実施例2のネジは30〜40N・mの締め付けトルクではネジ山の変形が認められなかった。これに対して、Al−7075合金のみからなるネジは、表2に示す通り、20N・mの締め付けトルクを超えると、ネジ山に変形が生じることが確認された。これらのことから、実施例2のネジは、SiC粒子をネジ山部分に集積させたことで、ネジ山が変形し難くなっていると考えられる。したがって、従来のアルミネジでは小さいトルクでネジ山が変形してしまい、繰り返しの使用が困難であったが、SiC粒子をネジ山部へ集積させることにより、繰り返し使用にも耐えうるネジが作製できる。   The measurement results are shown in Table 2. The screw standard of Example 2 is M12. As for the screw of Example 2, no deformation of the thread was observed at a tightening torque of 30 to 40 N · m. On the other hand, as shown in Table 2, it was confirmed that when the screw made of only the Al-7075 alloy exceeds the tightening torque of 20 N · m, the thread is deformed. From these facts, it can be considered that the screw of Example 2 is difficult to deform because the SiC particles are accumulated in the thread portion. Therefore, in the conventional aluminum screw, the screw thread is deformed with a small torque and it is difficult to use it repeatedly. However, by integrating SiC particles in the screw thread part, a screw that can withstand repeated use can be manufactured.

また、実施例2のネジは、締め付けトルクが40N・mを超えたところで、ネジ部が破断した。M12型のアルミネジの締め付け規定トルクは21N・mであり、一般的な鉄系M12型ネジの締め付け規定トルクは42N・mであることから、鉄系ネジと同等の締め付けトルクを有していることが確認された。
Further, the screw portion of Example 2 was broken when the tightening torque exceeded 40 N · m. The specified tightening torque for M12 type aluminum screws is 21 N · m, and the specified tightening torque for general iron-based M12 type screws is 42 N · m. Was confirmed.

本発明に係るAl基複合材製ネジの組織構造を模式的に示す断面図。Sectional drawing which shows typically the structure | tissue structure of the screw made from Al group composite material which concerns on this invention. Al基複合材製ネジの製造に用いる無垢棒の製造装置の概略構成を示す図。The figure which shows schematic structure of the manufacturing apparatus of the solid rod used for manufacture of screws made from Al group composite material. Al基融体における強化材粒子の移動メカニズムを模式的に示す図。The figure which shows typically the movement mechanism of the reinforcing material particle in Al-based melt. 実施例1に係る無垢棒の断面の光学顕微鏡写真。2 is an optical micrograph of a cross section of a solid bar according to Example 1. FIG. 実施例1のネジの断面の光学顕微鏡写真。3 is an optical micrograph of a cross section of a screw of Example 1. FIG. 図5A中の領域(a)部の拡大写真。The enlarged photograph of the area | region (a) part in FIG. 5A. 図5A中の領域(b)部の拡大写真。The enlarged photograph of the area | region (b) part in FIG. 5A. 図5A中の領域(c)部の拡大写真Enlarged photo of area (c) in FIG. 5A 実施例2のネジの断面の光学顕微鏡写真。4 is an optical micrograph of a cross section of a screw of Example 2. FIG. 図6A中の領域(a)部の拡大写真。The enlarged photograph of the area | region (a) part in FIG. 6A. 図6A中の領域(b)部の拡大写真。The enlarged photograph of the area | region (b) part in FIG. 6A.

符号の説明Explanation of symbols

10…Al基複合材製ネジ、12…軸芯部、14…ネジ山部、16…頭部、20…製造装置、22…鋳型、24…台座部、26…誘導コイル、28…高周波電源、32…交流磁場、34…誘導電流、36…電磁力、42…Al基融体、44…強化材粒子。   DESCRIPTION OF SYMBOLS 10 ... Al group composite material screw, 12 ... Shaft core part, 14 ... Screw thread part, 16 ... Head, 20 ... Manufacturing apparatus, 22 ... Mold, 24 ... Base part, 26 ... Induction coil, 28 ... High frequency power supply, 32 ... alternating magnetic field, 34 ... induced current, 36 ... electromagnetic force, 42 ... Al-based melt, 44 ... reinforcing material particles.

Claims (5)

Al基金属を主成分とする軸芯部と、
前記軸芯部の外側にこの軸芯部と連続して形成され、前記軸芯部と同種のAl基金属に強化材粒子が分散されてなる複合材料からなるネジ山部と、
を有することを特徴とするAl基複合材製ネジ。
An axial core mainly composed of an Al-based metal;
A threaded portion made of a composite material formed continuously with the shaft core portion on the outside of the shaft core portion, and reinforcing material particles dispersed in the same kind of Al-based metal as the shaft core portion;
A screw made of an Al-based composite material, characterized by comprising:
前記強化材粒子はSiCであることを特徴とする請求項1に記載のAl基複合材製ネジ。   The Al-based composite material screw according to claim 1, wherein the reinforcing material particles are SiC. 鋳型内で強化材粒子を分散させたAl基融体を生成する工程と、
前記強化材粒子が前記Al基融体の周縁部に移動するように、前記Al基融体を構成する溶融金属に電磁力を作用させる工程と、
前記Al基融体を固化させて、前記鋳型から複合材からなる無垢棒を取り出す工程と、
前記無垢棒に転造法によりネジ山を形成する工程と、を有することを特徴とするAl基複合材製ネジの製造方法。
Producing an Al-based melt in which reinforcing material particles are dispersed in a mold;
Applying electromagnetic force to the molten metal constituting the Al-based melt so that the reinforcing material particles move to the peripheral edge of the Al-based melt;
Solidifying the Al-based melt and taking out a solid bar made of a composite material from the mold; and
Forming a screw thread on the solid bar by a rolling method, and a method for producing an Al-based composite screw.
前記強化材粒子はSiCであり、前記Al基融体は純Al融体またはAl合金融体であることを特徴とする請求項3に記載のAl基複合材製ネジの製造方法。   The method for producing an Al-based composite material screw according to claim 3, wherein the reinforcing material particles are SiC, and the Al-based melt is a pure Al melt or an Al alloy. 前記Al基融体に電磁力を作用させる工程は、前記鋳型を囲繞するように誘導コイルを配置し、前記鋳型の長さ方向に交流磁場を発生させることにより行うことを特徴とする請求項3または請求項4に記載のAl基複合材製ネジの製造方法。   The step of applying an electromagnetic force to the Al-based melt is performed by arranging an induction coil so as to surround the mold and generating an alternating magnetic field in the length direction of the mold. Or the manufacturing method of the screw made from Al group composite material of Claim 4.
JP2006290155A 2006-10-25 2006-10-25 Al-based composite screw and its manufacturing method Pending JP2008106848A (en)

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Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103415712A (en) * 2011-03-10 2013-11-27 西门子公司 A screw or pin made of two different materials
CN106164504A (en) * 2014-03-20 2016-11-23 日本发条株式会社 Fastening parts and rod-shaped parts for fastening parts
KR101729293B1 (en) 2017-02-20 2017-04-21 김종갑 Manufacturing method of electric magnetic brake and thereby electric magnetic brake
KR101779198B1 (en) 2017-03-13 2017-09-19 정운겸 Manufacturing method of electric connecting terminal
CN107923429A (en) * 2015-08-28 2018-04-17 日本发条株式会社 Secure component and secure component bar-like member
WO2023240096A3 (en) * 2022-06-07 2024-01-11 Yazaki Corporation Aluminum-carbon metal matrix composites for fasteners
CN118048543A (en) * 2024-01-12 2024-05-17 南京理工大学 Titanium phosphide particle reinforced Al-Si based composite material and preparation method thereof
CN119974580A (en) * 2025-03-31 2025-05-13 东华大学 A method for manufacturing a thermoplastic composite material and metal hybrid structure rivet and self-heating riveting method

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61213330A (en) * 1985-03-18 1986-09-22 Toshiba Corp Bar-shaped body having high-temperature resistant strength and its production
JPS6376834A (en) * 1986-09-19 1988-04-07 Toshiba Corp Manufacture of lightweight bolt
JPH0367708A (en) * 1989-06-03 1991-03-22 Sumitomo Rubber Ind Ltd Method for measuring tire abrasion
JP2004034084A (en) * 2002-07-03 2004-02-05 J-Tec Inc Method for manufacturing partially reinforced metal matrix composite material

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS61213330A (en) * 1985-03-18 1986-09-22 Toshiba Corp Bar-shaped body having high-temperature resistant strength and its production
JPS6376834A (en) * 1986-09-19 1988-04-07 Toshiba Corp Manufacture of lightweight bolt
JPH0367708A (en) * 1989-06-03 1991-03-22 Sumitomo Rubber Ind Ltd Method for measuring tire abrasion
JP2004034084A (en) * 2002-07-03 2004-02-05 J-Tec Inc Method for manufacturing partially reinforced metal matrix composite material

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103415712A (en) * 2011-03-10 2013-11-27 西门子公司 A screw or pin made of two different materials
US10294977B2 (en) 2014-03-20 2019-05-21 Nhk Spring Co., Ltd. Fastening member and rod-like member for fastening member
CN106164504A (en) * 2014-03-20 2016-11-23 日本发条株式会社 Fastening parts and rod-shaped parts for fastening parts
CN106164504B (en) * 2014-03-20 2019-05-28 日本发条株式会社 Fastening parts and rod-shaped parts for fastening parts
EP3121464A4 (en) * 2014-03-20 2017-10-25 NHK Spring Co., Ltd. Fastening member, and rod-shaped member for fastening member
CN107923429B (en) * 2015-08-28 2020-07-28 日本发条株式会社 Fastening parts and rod-shaped parts for fastening parts
EP3343049A4 (en) * 2015-08-28 2019-03-20 NHK Spring Co., Ltd. FASTENING ELEMENT AND ROD-TYPE ELEMENT FOR FIXING ELEMENTS
CN107923429A (en) * 2015-08-28 2018-04-17 日本发条株式会社 Secure component and secure component bar-like member
US10767678B2 (en) 2015-08-28 2020-09-08 Nhk Spring Co., Ltd. Fastening member and rod-shaped member for fastening member
KR101729293B1 (en) 2017-02-20 2017-04-21 김종갑 Manufacturing method of electric magnetic brake and thereby electric magnetic brake
KR101779198B1 (en) 2017-03-13 2017-09-19 정운겸 Manufacturing method of electric connecting terminal
WO2023240096A3 (en) * 2022-06-07 2024-01-11 Yazaki Corporation Aluminum-carbon metal matrix composites for fasteners
CN118048543A (en) * 2024-01-12 2024-05-17 南京理工大学 Titanium phosphide particle reinforced Al-Si based composite material and preparation method thereof
CN119974580A (en) * 2025-03-31 2025-05-13 东华大学 A method for manufacturing a thermoplastic composite material and metal hybrid structure rivet and self-heating riveting method

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