JP2003034825A - Manufacturing method of high strength cold rolled steel sheet - Google Patents
Manufacturing method of high strength cold rolled steel sheetInfo
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- JP2003034825A JP2003034825A JP2001223740A JP2001223740A JP2003034825A JP 2003034825 A JP2003034825 A JP 2003034825A JP 2001223740 A JP2001223740 A JP 2001223740A JP 2001223740 A JP2001223740 A JP 2001223740A JP 2003034825 A JP2003034825 A JP 2003034825A
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Abstract
(57)【要約】
【課題】 加工性、溶接性に優れ、引張強度が340MPaを
超える高強度冷延鋼板の製造方法を提供する。
【解決手段】 低炭素鋼を、仕上温度Ar3〜Ar3+80℃で
熱間圧延し、最終圧延後1s以内に100℃/s以上の冷却速
度で80℃以上の温度範囲にわたって冷却し、650℃以下
で巻き取り、酸洗、冷間圧延を行った後、600℃から再
結晶終了までの温度域を100℃/sより大きい加熱速度で
焼鈍することを特徴とする高強度冷延鋼板の製造方法。
低炭素鋼は、mass%で、C: 0.2%以下、Si: 2.0%以
下、Mn: 2.5%以下、P: 0.1%以下、S: 0.03%以下、so
l.Al: 0.1%以下、N: 0.01%以下を含有し、残部が実質
的に鉄からなることを特徴とする高強度冷延鋼板の製造
方法。
(57) [Problem] To provide a method for producing a high-strength cold-rolled steel sheet having excellent workability and weldability and having a tensile strength exceeding 340 MPa. The A low carbon steel, finishing temperature Ar 3 hot rolled in to Ar 3 + 80 ° C., then cooled over 80 ° C. above the temperature range at 100 ° C. / s or more cooling rate within the final rolling after 1s, A high-strength cold-rolled steel sheet characterized by being rolled at 650 ° C or less, pickled and cold-rolled, and then annealed at a heating rate of more than 100 ° C / s from 600 ° C to the end of recrystallization. Manufacturing method.
For low carbon steel, mass%, C: 0.2% or less, Si: 2.0% or less, Mn: 2.5% or less, P: 0.1% or less, S: 0.03% or less, so
l. A method for producing a high-strength cold-rolled steel sheet, comprising: Al: 0.1% or less, N: 0.01% or less, and the balance substantially consisting of iron.
Description
【0001】[0001]
【発明の属する技術分野】本発明は、加工性、溶接性に
優れる高強度冷延鋼板の製造方法に関するものである。TECHNICAL FIELD The present invention relates to a method for producing a high-strength cold-rolled steel sheet having excellent workability and weldability.
【0002】[0002]
【従来の技術】近年、自動車用部品や家電製品などに使
用される鋼板において、引張強度の高い高強度冷延鋼板
が注目されている。従来より鋼の強化機構として、第74
・75回西山記念技術講座(昭和56年、日本鉄鋼協会)の
p.41に示されるように、固溶強化、析出強化、
変態強化、細粒化、加工硬化の5つの機構が知られ
ている。このうち、の加工硬化による高強度化は、鋼
の加工性を著しく劣化させるため、通常、高強度薄鋼板
の製造に関しては、〜の強化機構が用いられてい
る。2. Description of the Related Art In recent years, high-strength cold-rolled steel sheets having high tensile strength have been attracting attention as steel sheets used for automobile parts and home electric appliances. As a steel strengthening mechanism,
・ As shown on p.41 of 75th Nishiyama Memorial Technology Course (1981, Japan Iron and Steel Institute), solid solution strengthening, precipitation strengthening,
Five mechanisms are known: transformation strengthening, grain refinement, and work hardening. Among these, since strengthening by work hardening significantly deteriorates the workability of steel, the strengthening mechanisms of are usually used for the production of high strength thin steel sheets.
【0003】強化機構〜のうち特に細粒化は、加
工性や溶接性を大きく損なうことなく高強度化する方法
として、最も有効な手段である。この細粒化をベースの
強化機構として、さらに高強度化が必要となる場合に
は、固溶強化、析出強化、あるいは変態強化を組
み合わせることもできる。Among the strengthening mechanisms (1) to (3), especially fine graining is the most effective means as a method for increasing the strength without significantly impairing the workability and weldability. When further strengthening is required with this grain refining mechanism as a base strengthening mechanism, solid solution strengthening, precipitation strengthening, or transformation strengthening can be combined.
【0004】組織の細粒化については、熱延鋼板の場合
には、熱間で強加工を行い、急冷することで実現されて
いる。しかしながら、薄物で表面粗度や板厚精度にも優
れた冷延鋼板の場合は、冷間圧延後に再結晶焼鈍を行う
必要があり、細粒化を達成することは一般には困難であ
った。そこで、高強度冷延鋼板において組織の細粒化を
図ることを目的として、いくつかの技術が提案されてい
る。In the case of a hot-rolled steel sheet, the fine graining of the structure is realized by carrying out hot strong working and quenching. However, in the case of a cold-rolled steel sheet that is thin and has excellent surface roughness and plate thickness accuracy, it is necessary to perform recrystallization annealing after cold rolling, and it has been generally difficult to achieve grain refinement. Therefore, some techniques have been proposed for the purpose of making the structure finer in the high-strength cold-rolled steel sheet.
【0005】例えば、特許3046128号公報には、加工性
に優れた硬質表面処理原板の製造方法が提案されてい
る。ここでは、Mnを0.5〜1.5%含有する鋼を、通常の熱
間圧延条件により熱延鋼帯とし、冷間圧延後、連続焼鈍
を行うに際し、500℃以上の温度域を300〜2000℃/sで加
熱し、730〜830℃に2秒以下滞在させ、100〜500℃/sの
冷却速度で冷却する。このように、超急速加熱により、
Cの拡散が抑制されることで2相分離が進まず、フェライ
トの粒成長が抑制されることで超微細粒が得られるとい
うものである。For example, Japanese Patent No. 3046128 proposes a method of manufacturing a hard surface-treated original plate having excellent workability. Here, steel containing 0.5 to 1.5% of Mn is a hot-rolled steel strip under normal hot rolling conditions, and after cold rolling, when performing continuous annealing, a temperature range of 500 ° C. or higher is 300 to 2000 ° C. / Heat at s, stay at 730 ~ 830 ℃ for 2 seconds or less, and cool at a cooling rate of 100 ~ 500 ℃ / s. In this way, by ultra-rapid heating,
By suppressing the diffusion of C, the two-phase separation does not proceed, and by suppressing the grain growth of ferrite, ultrafine grains can be obtained.
【0006】特許2688384号公報には、伸びフランジ性
に優れた高張力冷延鋼板の製造方法が提案されている。
これは、Nbを0.005〜0.045wt%添加した鋼を熱間圧延お
よび冷間圧延をおこなった後、5℃/s以上の加熱速度で
加熱、焼鈍を行う方法であり、特にNb添加により細粒化
を実現することを意図するものである。さらに、加熱速
度も大きいほうが微細化には有利とされ、そのため5℃/
s以上、好ましくは10℃/s以上、実施例では最大20℃/s
までの例が示されている。このとき、フェライト粒径と
しては、平均11μmまでの細粒化が実現されている。Japanese Patent No. 2688384 proposes a method for producing a high-strength cold-rolled steel sheet having excellent stretch flangeability.
This is a method of hot rolling and cold rolling steel with Nb added at 0.005 to 0.045 wt%, followed by heating and annealing at a heating rate of 5 ° C / s or more. Is intended to be realized. In addition, a higher heating rate is advantageous for miniaturization, so 5 ° C /
s or more, preferably 10 ℃ / s or more, in the example maximum 20 ℃ / s
Examples are shown up to. At this time, the ferrite grain size has been reduced to an average of 11 μm.
【0007】特公平2-1210号公報には、延性の良好な高
張力冷延鋼板の製造方法が提案されている。この技術で
は、熱間圧延、酸洗、冷間圧延後の連続焼鈍に際し、少
なくとも600℃からAc1変態点までの温度域を5℃/s以上
の加熱速度で加熱し、10s〜10min均熱保持した後、冷却
を制御しながら行う。これは、フェライト粒の再結晶開
始温度である600℃からAc1変態点に至る加熱時間を短縮
することで、フェライト組織を微細な再結晶粒あるいは
未再結晶状態とし、その状態でAc1変態点以上の温度に
加熱することで、逆変態するオーステナイト粒を微細化
させることを意図している。加熱速度の上限は特に定め
ていないが、実施例では最大30℃/sまでの例が示されて
いる。Japanese Patent Publication No. 2-1210 proposes a method for producing a high-strength cold-rolled steel sheet having good ductility. In this technology, at the time of continuous annealing after hot rolling, pickling, and cold rolling, the temperature range from at least 600 ° C to the Ac 1 transformation point is heated at a heating rate of 5 ° C / s or more, and the soaking is performed for 10s to 10min. After holding, cooling is performed while controlling. This is because by shortening the heating time from the recrystallization start temperature of ferrite grains from 600 ℃ to the Ac 1 transformation point, the ferrite structure becomes fine recrystallized grains or unrecrystallized state, and the Ac 1 transformation occurs in that state. It is intended to make the austenite grains that undergo reverse transformation finer by heating to a temperature above the point. Although the upper limit of the heating rate is not particularly defined, the example shows a maximum of 30 ° C./s.
【0008】特開平10-237549号公報には、ノンイヤリ
ング性に優れ、コイルの長手方向、幅方向における特性
が均一な缶用鋼板の製造方法が提案されている。この技
術では、仕上げ圧延温度800〜1000℃で熱間圧延した
後、1次冷間圧延し、次いで、加熱速度を10℃/sec 以
上、均熱温度をAc1変態点〜800℃、かつ均熱時間を60 s
ec以下とする連続焼鈍を行い、さらに、圧下率20%以下
で2次冷間圧延している。Japanese Unexamined Patent Publication (Kokai) No. 10-237549 proposes a method of manufacturing a steel sheet for a can, which has excellent non-earing properties and has uniform properties in the longitudinal and width directions of the coil. In this technology, after hot rolling at a finish rolling temperature of 800 to 1000 ° C, primary cold rolling is performed, then a heating rate of 10 ° C / sec or more, a soaking temperature of Ac 1 transformation point to 800 ° C, and a soaking temperature. 60 s heat time
Continuous annealing at ec or less is performed, and secondary cold rolling is performed at a reduction rate of 20% or less.
【0009】特公平1-25381号公報には、Tiを0.002〜0.
020%含有する鋼を、熱間圧延後急冷し、270℃以下の温
度で巻取り、冷間圧延後、加熱速度1〜100℃/s、均熱温
度650〜850℃で連続焼鈍を行う方法が提案されている。
この方法は、熱間圧延での低温巻取により鋼中に固溶C
を残留させ、冷間圧延後の焼鈍過程でセメンタイトを微
細に析出させることで、高r値化が実現できるというも
のである。なお、熱間圧延後巻取りまでの時間として
は、10〜20s要した例が示されている。Japanese Patent Publication No. 1-25381 discloses a Ti content of 0.002 to 0.
A method of quenching steel containing 020% after hot rolling, winding at a temperature of 270 ° C or lower, and performing continuous annealing at a heating rate of 1 to 100 ° C / s and a soaking temperature of 650 to 850 ° C after cold rolling. Is proposed.
This method consists of solid solution C in steel by low temperature winding in hot rolling.
It is possible to achieve a high r-value by allowing the cementite to remain and finely depositing cementite in the annealing process after cold rolling. An example is shown in which the time from hot rolling to winding is 10 to 20 seconds.
【0010】[0010]
【発明が解決しようとする課題】しかし、前述の従来技
術については、次のような問題点があった。すなわち、
特許3046128号公報記載の技術のように、超急速加熱を
行うことによりCの拡散を抑えることで、オーステナイ
ト粒の生成および成長は抑制されるものの、フェライト
粒の核生成サイトの増加、および粒成長の抑制に関して
は不十分である。従って、フェライト粒の十分な細粒化
はなされていないと考えられ、加工性に関しても不十分
なものとなっている。However, the above-mentioned prior art has the following problems. That is,
As in the technique described in Japanese Patent No. 3046128, by suppressing the diffusion of C by performing ultra-rapid heating, although the generation and growth of austenite grains are suppressed, the nucleation site of ferrite grains increases, and grain growth. Is insufficient for the suppression of Therefore, it is considered that the ferrite grains are not sufficiently refined, and the workability is insufficient.
【0011】特許2688384号公報記載の技術について
は、Nb添加に伴う炭窒化物の形成により、細粒化できる
ことになっているが、同時に再結晶温度の上昇を招く。
そのため、焼鈍温度を高めに設定する必要があり、かえ
って十分な細粒化を達成することは困難である。さら
に、加熱速度の増加により細粒化できるとしているもの
の、実質的には最大20℃/s程度を想定しているに過ぎ
ず、粒成長を抑える程度の効果しかない。従って、結果
的に十分な細粒化は達成できておらず、強度と延性のバ
ランスに劣っている。In the technique described in Japanese Patent No. 2688384, it is supposed that the carbonitrides can be formed by the addition of Nb, but the grain size can be reduced, but at the same time, the recrystallization temperature is increased.
Therefore, it is necessary to set the annealing temperature higher, and it is rather difficult to achieve sufficient grain refinement. Further, although it is said that the particles can be made finer by increasing the heating rate, the actual maximum is about 20 ° C./s, which is only an effect of suppressing the grain growth. Therefore, as a result, sufficient grain refinement has not been achieved, and the balance between strength and ductility is poor.
【0012】特公平2-1210号公報記載の技術について
も、加熱速度の増加により細粒化できるとしているもの
の、実質的には最大でも50℃/s程度を想定しているに過
ぎず、粒成長を抑える程度の効果しかない。従って、十
分な細粒化は達成できないと考えられる。なお、この公
報によると、高強度化と高延性化が達成できるとしてい
るが、これは焼鈍後の冷却制御により生成した低温変態
相の効果が大きく、溶接時の耐HAZ軟化性に問題を残し
ている。The technology described in Japanese Examined Patent Publication No. 2110-2 is also said to be able to make fine particles by increasing the heating rate, but practically only a maximum of about 50 ° C./s is assumed, and It has only the effect of suppressing growth. Therefore, it is considered that sufficient grain refinement cannot be achieved. According to this publication, higher strength and higher ductility can be achieved, but this has a large effect of the low temperature transformation phase generated by cooling control after annealing, leaving a problem in HAZ softening resistance during welding. ing.
【0013】特開平10-237549号公報記載の技術につい
ても、加熱速度の増加により細粒化できるとしているも
のの、実質的には最大でも30℃/s程度を想定しているに
過ぎず、粒成長を抑える程度の効果しかない。従って、
この場合も十分な細粒化は達成できないと考えられ、結
果的に加工性に関しては不十分と言える。In the technique described in Japanese Patent Laid-Open No. 10-237549, it is said that fine particles can be formed by increasing the heating rate, but in reality, only a maximum of about 30 ° C./s is assumed, and It has only the effect of suppressing growth. Therefore,
Even in this case, it is considered that sufficient grain refinement cannot be achieved, and as a result, it can be said that workability is insufficient.
【0014】特公平1-25381号公報記載の技術について
は、熱間圧延終了後例えば1s以内というような短時間
で、直ちに急冷を行っているとは考えにくい。また、焼
鈍の際の加熱速度も100℃/sまでであり、本来細粒化を
意図したものではないこともあり、細粒化は不十分と考
えられ、加工性も劣ることが予想される。In the technique disclosed in Japanese Patent Publication No. 1-25381, it is unlikely that the rapid cooling is carried out immediately in a short time such as within 1 second after the end of hot rolling. In addition, the heating rate during annealing is up to 100 ° C / s, and it may not be intended for fine graining, so graining is considered to be insufficient, and workability is expected to be poor. .
【0015】本発明は、上記の課題を解決し、通常、細
粒化が困難な冷延鋼板において細粒化を実現するもので
あり、加工性、溶接性に優れ、引張強度が340MPaを超え
る高強度冷延鋼板の製造方法を提供することを目的とす
る。The present invention solves the above problems and realizes grain refinement in a cold-rolled steel sheet, which is usually difficult to grain refine, has excellent workability and weldability, and has a tensile strength of more than 340 MPa. An object is to provide a method for manufacturing a high strength cold rolled steel sheet.
【0016】[0016]
【課題を解決するための手段】上記の課題は、次の発明
により解決される。その発明は、低炭素鋼を、仕上温度
Ar3〜Ar3+80℃で熱間圧延し、最終圧延後1s以内に100℃
/s以上の冷却速度で80℃以上の温度範囲にわたって冷却
し、650℃以下で巻き取り、酸洗、冷間圧延を行った
後、600℃から再結晶終了までの温度域を100℃/sより大
きい加熱速度で焼鈍することを特徴とする高強度冷延鋼
板の製造方法である。The above problems can be solved by the following inventions. The invention uses low-carbon steel at a finishing temperature
Ar 3 to Ar 3 + at 80 ° C. and hot rolling, 100 ° C. within the final rolling after 1s
After cooling at a cooling rate of / s or more over a temperature range of 80 ° C or more, winding at 650 ° C or less, pickling and cold rolling, the temperature range from 600 ° C to the end of recrystallization is 100 ° C / s. A method for producing a high-strength cold-rolled steel sheet, characterized by annealing at a higher heating rate.
【0017】この発明は、上述した問題を解決すべく鋭
意研究を重ねた結果なされた。研究の過程で、延性や穴
拡げ性を指標とする加工性や溶接性の観点から、組織の
細粒化による高強度化を指向した。すなわち、熱間圧延
段階では圧延後の即時急冷により未再結晶オーステナイ
トからのフェライト変態を生じさせ、さらに、冷間圧延
後の再結晶焼鈍過程において急速加熱を行うことで、組
織が飛躍的に細粒化し、加工性および溶接性の良好な高
強度冷延鋼板が得られることを見出した。The present invention has been made as a result of intensive studies to solve the above-mentioned problems. In the process of research, from the viewpoint of workability and weldability using ductility and hole expandability as indicators, we aimed to increase the strength by making the structure finer. That is, in the hot rolling stage, immediate rapid cooling after rolling causes ferrite transformation from unrecrystallized austenite, and further rapid heating in the recrystallization annealing process after cold rolling leads to a dramatically finer structure. It has been found that a high-strength cold-rolled steel sheet that is granulated and has good workability and weldability can be obtained.
【0018】なお、本発明が対象とする冷延鋼板の中に
は、溶融亜鉛メッキ材や電気亜鉛メッキ材などの表面処
理を施した鋼板も含む。以下、本発明の製造条件につい
て説明する。The cold-rolled steel sheet targeted by the present invention includes a steel sheet having a surface treatment such as a hot dip galvanized material or an electrogalvanized material. Hereinafter, the manufacturing conditions of the present invention will be described.
【0019】熱間圧延の最終圧延の温度: Ar3〜Ar3+8
0℃
熱間圧延の最終圧延の温度(仕上温度)がAr3変態点を
下回った場合には、粗大なフェライト粒が生成するた
め、その後の製造過程で冷延鋼板の組織を細粒化するこ
とは困難となる。一方、最終圧延の温度がAr3+80℃を上
回ると、加工されたオーステナイトの再結晶が進行する
ため、未再結晶オーステナイトからの変態で微細なフェ
ライト粒を生成させることができなくなる。従って、熱
間圧延の最終圧延の温度(仕上温度)は、Ar3〜Ar3+80
℃の範囲内とする。Final rolling temperature of hot rolling: Ar 3 to Ar 3 +8
When the final rolling temperature (finishing temperature) of 0 ° C hot rolling is below the Ar 3 transformation point, coarse ferrite grains are generated, so the microstructure of the cold rolled steel sheet is refined in the subsequent manufacturing process. Things will be difficult. On the other hand, if the temperature of the final rolling exceeds Ar 3 + 80 ° C., recrystallization of the processed austenite proceeds, so that it becomes impossible to generate fine ferrite grains by transformation from unrecrystallized austenite. Therefore, the final rolling temperature (finishing temperature) of hot rolling is Ar 3 to Ar 3 +80.
Within the range of ° C.
【0020】圧延後の冷却開始時期: 最終圧延後1s以
内
圧延後の冷却条件は、本発明の根幹をなす技術の1つで
ある。 圧延後の冷却を開始する時期が最終圧延後1sを
過ぎると、オーステナイト域での圧延で蓄積された歪が
回復ないしは再結晶することがあり、フェライト変態に
よる細粒化にとって好ましくない。従って、圧延後の冷
却開始時期は、最終圧延後1s以内とする。Cooling start time after rolling: Within 1 s after final rolling The cooling condition after rolling is one of the technologies forming the basis of the present invention. If the time to start cooling after rolling exceeds 1 s after the final rolling, the strain accumulated during rolling in the austenite region may be recovered or recrystallized, which is not preferable for grain refinement due to ferrite transformation. Therefore, the cooling start time after rolling should be within 1 s after the final rolling.
【0021】圧延後の冷却条件: 80℃以上の温度範囲
にわたって冷却速度100℃/s以上
冷却開始後は、組織の微細化のため、冷却速度の確保と
共に冷却前後の温度差を確保する必要がある。冷却速度
が100℃/s未満では、オーステナイトに蓄積された歪が
回復ないしは再結晶し、変態後のフェライト粒が微細化
しない。また、冷却前後の温度差(降下温度)が80℃未
満では、やはり歪が回復ないしは再結晶し、変態後のフ
ェライト粒が微細化しない。従って、圧延後の冷却条件
を、80℃以上の温度範囲にわたって冷却速度100℃/s以
上とする。Cooling condition after rolling: Cooling rate over a temperature range of 80 ° C. or more After cooling starts at 100 ° C./s or more, it is necessary to secure a cooling rate and a temperature difference before and after cooling in order to refine the structure. is there. When the cooling rate is less than 100 ° C / s, the strain accumulated in austenite is recovered or recrystallized, and the ferrite grains after transformation are not refined. When the temperature difference (falling temperature) before and after cooling is less than 80 ° C, the strain is recovered or recrystallized, and the ferrite grains after transformation are not refined. Therefore, the cooling condition after rolling is set to a cooling rate of 100 ° C./s or more over a temperature range of 80 ° C. or more.
【0022】巻取温度:650℃以下
熱間圧延後の巻き取りにおいて、650℃を超える高温で
巻き取った場合には、フェライト粒の粒成長が起こり、
その後の製造工程で冷延鋼板の組織を細粒化することが
できなくなる。従って、熱間圧延後は650℃以下で巻き
取ることとする。巻取温度の下限はとくに規定せず、材
料特性の観点からは室温で巻き取っても構わないが、冷
却能力、操業性等の観点から決めればよい。Winding temperature: 650 ° C. or less In winding after hot rolling, if the winding is carried out at a high temperature exceeding 650 ° C., grain growth of ferrite grains occurs,
In the subsequent manufacturing process, the structure of the cold rolled steel sheet cannot be refined. Therefore, after hot rolling, the coil is wound at 650 ° C or lower. The lower limit of the coiling temperature is not particularly specified, and the coiling may be carried out at room temperature from the viewpoint of material properties, but it may be determined from the viewpoints of cooling capacity, operability and the like.
【0023】焼鈍における加熱速度: 600℃から再結
晶終了まで100℃/sより大
冷間圧延後の再結晶焼鈍における加熱過程は、熱間圧延
後の冷却条件とともに本発明の根幹をなす部分である。
この加熱速度が遅い場合、加熱途中で歪の回復が進行
し、焼鈍目標温度に達したときには再結晶核発生のため
の駆動力が低下するため、微細粒を得ることができなく
なる。この問題は、600℃以上の温度範囲で顕著とな
る。Heating Rate in Annealing: Greater than 100 ° C./s from 600 ° C. to the end of recrystallization The heating process in recrystallization annealing after cold rolling is a part that forms the basis of the present invention together with the cooling conditions after hot rolling. is there.
When this heating rate is slow, the recovery of strain progresses during heating, and when the annealing target temperature is reached, the driving force for generating recrystallization nuclei decreases, and it becomes impossible to obtain fine grains. This problem becomes remarkable in the temperature range of 600 ° C or higher.
【0024】加熱速度を100℃/sより大きくすること
で、加熱途中での歪の回復を抑制し、焼鈍目標温度でフ
ェライト粒界からの再結晶核を一気にランダムに生成さ
せることができ、超微細組織が得られる。この加熱速度
は、歪の回復を抑制する観点から、再結晶終了温度まで
確保する必要がある。By making the heating rate higher than 100 ° C./s, the recovery of strain during heating can be suppressed, and recrystallized nuclei from ferrite grain boundaries can be randomly generated at a target annealing temperature. A fine structure is obtained. From the viewpoint of suppressing the recovery of strain, this heating rate needs to be secured up to the recrystallization end temperature.
【0025】従って、焼鈍における加熱速度を、600℃
から再結晶終了まで100℃/sより大とする。なお、生産
性の点からは室温から焼鈍温度まで100℃/sより大きい
加熱速度で加熱するのが好ましいが、室温から600℃ま
での範囲においては、低速加熱であっても歪の回復量自
体が小さいため、100℃/s以下でも構わない。また、加
熱方法はとくに限定しないが、誘導加熱や直接通電等に
よって加熱してもよい。Therefore, the heating rate in annealing is 600 ° C.
To 100 ° C / s from the end to recrystallization. From the viewpoint of productivity, it is preferable to heat from room temperature to the annealing temperature at a heating rate higher than 100 ° C./s, but in the range from room temperature to 600 ° C., the strain recovery amount itself even at low speed heating. Since it is small, 100 ° C / s or less is acceptable. The heating method is not particularly limited, but the heating may be performed by induction heating, direct energization, or the like.
【0026】上記の発明においてさらに、低炭素鋼は、
mass%で、C: 0.2%以下、Si: 2.0%以下、Mn: 2.5%以
下、P: 0.1%以下、S: 0.03%以下、sol.Al: 0.1%以
下、N: 0.01%以下を含有し、残部が実質的に鉄からな
ることを特徴とする高強度冷延鋼板の製造方法とするこ
ともできる。Further, in the above invention, the low carbon steel is
Mass%, C: 0.2% or less, Si: 2.0% or less, Mn: 2.5% or less, P: 0.1% or less, S: 0.03% or less, sol.Al: 0.1% or less, N: 0.01% or less Also, the manufacturing method of the high-strength cold-rolled steel sheet may be characterized in that the balance is substantially made of iron.
【0027】この発明においては、さらに化学成分を規
定しているので、より効率的に高強度冷延鋼板を製造す
ることができる。以下、化学成分について説明する。In the present invention, since the chemical composition is further specified, the high strength cold rolled steel sheet can be manufactured more efficiently. The chemical components will be described below.
【0028】C:0.2%以下
Cは、鋼の強度を高める上で、安価で有効な元素であ
る。しかし、0.2%を超える多量のC添加は、パーライト
量の増大を招き、延性、伸びフランジ性が劣化するのみ
ならず、溶接性にも悪影響をおよぼす。そのため、C量
は0.2%以下とする。C: 0.2% or less C is an inexpensive and effective element for increasing the strength of steel. However, addition of a large amount of C exceeding 0.2% causes an increase in the amount of pearlite, which not only deteriorates the ductility and stretch flangeability but also adversely affects the weldability. Therefore, the C content is 0.2% or less.
【0029】Si: 2.0%以下
Siは加工性を劣化することなくフェライトを固溶強化
し、強度と加工性のバランスを向上させるので、要求さ
れる強度レベルに応じて添加する。ただし、2.0%を超
える多量のSi添加は、靭性および溶接性を劣化させる。
従って、Si量は 2.0%を上限とする。Si: 2.0% or less Si solid-solution strengthens ferrite without deteriorating workability and improves the balance between strength and workability, so Si is added according to the required strength level. However, addition of a large amount of Si exceeding 2.0% deteriorates toughness and weldability.
Therefore, the upper limit of Si content is 2.0%.
【0030】Mn : 2.5%以下
Mnは固溶強化元素として、高強度化に有効であり、要求
される強度レベルに応じて添加するのが好ましい。ただ
し、2.5%を超える多量のMn添加は溶接性の劣化を招
く。従って、Mn 量は2.5%を上限とする。Mn: 2.5% or less Mn is a solid solution strengthening element and is effective in increasing strength. It is preferable to add Mn according to the required strength level. However, addition of a large amount of Mn exceeding 2.5% causes deterioration of weldability. Therefore, the upper limit of Mn content is 2.5%.
【0031】P : 0.1%以下
Pは固溶強化元素として、高強度化に有効であり、さら
に、Si添加鋼の場合には、赤スケールの発生を抑制する
ことから、必要に応じて添加するのが好ましい。ただ
し、0.1%を超える多量のP添加は、粒界への偏析を助長
し、延性、靭性を低下させる。従って、P量は0.1%を上
限とする。P: 0.1% or less P is a solid solution strengthening element and is effective for increasing strength. Further, in the case of Si-added steel, it suppresses the generation of red scale, so P is added as necessary. Is preferred. However, addition of a large amount of P exceeding 0.1% promotes segregation at grain boundaries, and reduces ductility and toughness. Therefore, the upper limit of P content is 0.1%.
【0032】S : 0.03%以下
Sは、熱間での延性を著しく低下させることで、熱間割
れを誘発し、表面性状を著しく劣化させる。さらに、S
は、強度にほとんど寄与しないばかりか、不純物元素と
して粗大なMnSを形成したり、Ti添加鋼の場合には、多
量の粗大なTi系硫化物を生成することで、延性、伸びフ
ランジ性を低下させる。これらの問題はS量が0.03%を
超えると顕著となり、極力低減することが望ましい。従
って、S量は0.03%を上限とする。さらに、延性および
伸びフランジ性を向上させる観点からは、S量を0.01%
以下とすることが好ましい。S: 0.03% or less S significantly reduces hot ductility, induces hot cracking, and significantly deteriorates surface properties. Furthermore, S
Not only contributes to the strength, but also forms coarse MnS as an impurity element and, in the case of Ti-added steel, reduces the ductility and stretch flangeability by forming a large amount of coarse Ti-based sulfide. Let These problems become remarkable when the S content exceeds 0.03%, and it is desirable to reduce them as much as possible. Therefore, the upper limit of S content is 0.03%. Furthermore, from the viewpoint of improving ductility and stretch flangeability, the S content is 0.01%.
The following is preferable.
【0033】sol.Al : 0.1%以下
sol.Alは、脱酸元素として鋼中の介在物を減少させる作
用を有しているが、0.1%を超えて多量に添加した場合
にはアルミナ系介在物が増加し、延性が低下する。従っ
て、sol.Al量は0.1%を上限とする。Sol.Al: 0.1% or less sol.Al has a function of reducing inclusions in steel as a deoxidizing element, but when added in excess of 0.1%, alumina-based inclusions The number of products increases and the ductility decreases. Therefore, the upper limit of the sol.Al content is 0.1%.
【0034】N : 0.01%以下
Nは0.01%を超えて多量に含有すると、熱間圧延中にス
ラブ割れを伴い、表面疵が発生する恐れがある。従っ
て、N量は0.01%を上限とする。N: 0.01% or less When N is contained in a large amount exceeding 0.01%, slab cracks may occur during hot rolling and surface defects may occur. Therefore, the upper limit of N content is 0.01%.
【0035】なお、これらの手段において「残部が実質
的に鉄である」とは、本発明の作用・効果を損なわない
限り、不可避的不純物をはじめ、他の微量元素を含有す
るものが本発明の範囲に含まれることを意味する。In these means, "the balance is substantially iron" means that the content of inevitable impurities and other trace elements is included in the present invention unless the action and effect of the present invention are impaired. It means that it is included in the range of.
【0036】[0036]
【発明の実施の形態】発明の実施に当たっては、目的と
する強度レベルに応じた化学成分の低炭素鋼又は上記の
化学成分の鋼を溶製する。溶製方法は、通常の転炉法、
電炉法等、適宜適用することができる。その他の元素は
とくに規定しないが、本発明の高強度冷延鋼板の製造に
おいては、以下の成分を調整あるいは添加することがで
きる。BEST MODE FOR CARRYING OUT THE INVENTION In carrying out the invention, a low carbon steel having a chemical composition corresponding to a desired strength level or a steel having the above chemical composition is melted. The melting method is a normal converter method,
The electric furnace method or the like can be appropriately applied. Other elements are not particularly specified, but the following components can be adjusted or added in the production of the high strength cold rolled steel sheet of the present invention.
【0037】Si: 好ましくは0.5%、さらに0.2%
一般に、多量のSi添加は、熱延加熱時におけるスラブ表
面にファイヤライトの生成を促進し、いわゆる赤スケー
ルと呼ばれる表面模様の発生を助長するとともに、溶融
亜鉛メッキ鋼板として使用される場合には、Siによる不
メッキの不良も誘発することから、表面性状を必要とす
る鋼板や溶融亜鉛メッキ鋼板の場合には、0.5%程度を
上限に、さらに望ましくは0.2%程度を上限にする。Si: preferably 0.5%, more preferably 0.2% Generally, addition of a large amount of Si promotes the formation of firelite on the surface of the slab during heating by hot rolling, and promotes the generation of a surface pattern called so-called red scale. When it is used as a hot-dip galvanized steel sheet, it also induces a non-plating defect due to Si, so in the case of a steel sheet or hot-dip galvanized steel sheet that requires surface texture, the upper limit is about 0.5%, and Desirably, the upper limit is about 0.2%.
【0038】Ti、Nb、V、Cu、Ni、Cr、Mo、B: 必要に
応じ添加
さらに、要求される強度レベルに応じて、Ti、Nb、V 、
Cu、Ni、Cr、Mo、B等の添加元素を添加してもよい。添
加量の上限は、Ti、V、Cu、Ni、Cr、Moは1%以下、Nbは
1.5%以下、Bは0.01%以下とすることが望ましい。Ti, Nb, V, Cu, Ni, Cr, Mo, B: added as required, and further Ti, Nb, V, depending on the required strength level.
Additional elements such as Cu, Ni, Cr, Mo and B may be added. The upper limit of the addition amount is 1% or less for Ti, V, Cu, Ni, Cr, Mo, and Nb
It is desirable that the content be 1.5% or less and B be 0.01% or less.
【0039】溶製された鋼は、スラブに鋳造後、そのま
ま又は冷却して加熱し、熱間圧延を施す。仕上圧延後の
熱延鋼板は前述の巻取温度で巻き取り、通常の冷間圧延
を施す。After the molten steel is cast into a slab, it is heated as it is or after cooling and hot rolling. The hot-rolled steel sheet after finish rolling is wound at the above-mentioned winding temperature and subjected to ordinary cold rolling.
【0040】焼鈍については、前述の加熱条件で急速加
熱を行う。焼鈍温度(再結晶温度)はとくに規定しない
が、各化学成分について再結晶焼鈍に必要な温度まで昇
温することとし、その範囲においては、極力低温にする
のが好ましい。焼鈍時間もとくに規定しないが、再結晶
温度以上の温度域に滞在する時間はとくに必要ない。For annealing, rapid heating is performed under the above heating conditions. Although the annealing temperature (recrystallization temperature) is not particularly specified, it is preferable to raise the temperature of each chemical component to the temperature required for recrystallization annealing, and it is preferable to make the temperature as low as possible within that range. The annealing time is not specified, but the time to stay in the temperature range above the recrystallization temperature is not particularly required.
【0041】焼鈍後の冷却も、放冷でも急冷でも構わな
い。とくに溶融亜鉛メッキ鋼板や合金化溶融亜鉛メッキ
鋼板として製造される場合は、そのプロセスにおける熱
履歴で構わない。Cooling after annealing may be either cooling or quenching. Especially when manufactured as a hot-dip galvanized steel sheet or an alloyed hot-dip galvanized steel sheet, the heat history in the process may be used.
【0042】このようにして、本発明により、降伏比が
低く、かつ、加工性、溶接性に優れる引張強度の高い冷
延鋼板の製造が可能となる。この理由に関しては、本発
明の請求範囲を限定するものではないが、つぎのように
考えられる。As described above, according to the present invention, it is possible to manufacture a cold rolled steel sheet having a low yield ratio, excellent workability and weldability, and high tensile strength. The reason for this is not limited to the scope of the claims of the present invention, but is considered as follows.
【0043】すなわち、冷間圧延後の再結晶焼鈍過程に
おいて、徐加熱をおこなった場合には、その加熱途中に
歪の回復が進行し、冷間圧延で蓄積された歪の多くが消
失するため、再結晶には、高温かつ長時間の保持が必要
となる。そのため、大きな再結晶粒が生成することが避
けられず、粒成長により再結晶粒の寸法も不均一とな
る。That is, in the recrystallization annealing process after cold rolling, when gradual heating is performed, recovery of strain progresses during heating, and most of the strain accumulated in cold rolling disappears. However, recrystallization requires holding at a high temperature for a long time. Therefore, generation of large recrystallized grains is unavoidable, and the size of the recrystallized grains becomes nonuniform due to grain growth.
【0044】一方、急速加熱をおこなった場合には、加
熱途中で歪の回復が進行することなく再結晶温度域に達
することができる。そして、歪が回復することなく即座
に高温域に移行することから、その再結晶核生成のため
の駆動力は莫大となり、大傾角のフェライト粒界からだ
けでなく、冷間圧延時に比較的歪の入り難い小傾角のフ
ェライト粒界からも、瞬時に核発生が進行するものと考
えられる。On the other hand, when the rapid heating is performed, the recrystallization temperature range can be reached without the recovery of the strain during the heating. Then, since the strain immediately shifts to the high temperature range without recovery, the driving force for the recrystallization nucleation becomes enormous, and not only from the ferrite grain boundary with a large tilt angle, but also the strain at the time of cold rolling is relatively high. It is considered that nucleation proceeds instantaneously even from a small-angled ferrite grain boundary where it is hard to enter.
【0045】ここで、通常の大傾角のフェライト粒界が
オーステナイト粒界からの核発生に対応するのとは異な
り、小傾角のフェライト粒界は熱間圧延時の未再結晶オ
ーステナイト粒の粒内からの核発生に対応するものであ
る。本発明では、前述のように熱間圧延および圧延後の
急冷により組織に制御しており、熱延鋼板の組織を小傾
角粒界を有するフェライト組織としている。Here, unlike the usual case where a large tilt ferrite grain boundary corresponds to the nucleation from the austenite grain boundary, a small tilt ferrite grain boundary is inside the unrecrystallized austenite grain during hot rolling. It corresponds to the nuclear generation from. In the present invention, the structure is controlled by hot rolling and rapid cooling after rolling as described above, and the structure of the hot-rolled steel sheet is a ferrite structure having a low-angle grain boundary.
【0046】この、小傾角のフェライト粒界に生成した
再結晶核は、隣り合う粒同士の方位差が小さいことか
ら、特に優先方位を持たずランダムに成長しようとす
る。ところが、再結晶核は莫大な数で一斉に生成するこ
とから、結果的に再結晶粒同士は対等に粒成長しようと
するため、互いにほとんど成長することができなくな
り、超微細組織が形成されると推定される。The recrystallized nuclei formed in the ferrite grain boundaries with a small tilt angle tend to grow randomly without any preferential orientation because the orientation difference between adjacent grains is small. However, since recrystallized nuclei are simultaneously produced in an enormous number, recrystallized grains try to grow equally, and as a result, they can hardly grow each other and an ultrafine structure is formed. It is estimated to be.
【0047】それに対して、本発明とは異なり通常の大
傾角粒界からなるフェライト組織の熱延鋼板を冷間圧延
して、急速加熱による再結晶焼鈍を行った場合は、隣り
合う粒同士の方位差が大きいことから、優先方位を持っ
て粒成長が進行することになる。その結果、再結晶核が
一斉に生成した場合でも、一部の再結晶粒が優先的に成
長するため、全体としての粒径は不均一となり、細粒組
織を形成することができないものと考えられる。On the other hand, unlike the present invention, when a hot-rolled steel sheet having a ferritic structure having a normal high-angle grain boundary is cold-rolled and recrystallized by rapid heating, the adjacent grains are Since the difference in orientation is large, the grain growth proceeds with the preferred orientation. As a result, even if the recrystallized nuclei are generated all at once, some of the recrystallized grains preferentially grow, so the overall grain size is nonuniform, and it is considered that a fine grain structure cannot be formed. To be
【0048】[0048]
【実施例】本発明の実施例について説明する。なお、本
発明はこれらの実施例のみに限定されるものではない。EXAMPLES Examples of the present invention will be described. The present invention is not limited to these examples.
【0049】まず、表1に示す成分の鋼を実験室真空溶
解炉にて溶製し、一旦室温まで冷却した。First, steels having the components shown in Table 1 were melted in a laboratory vacuum melting furnace and once cooled to room temperature.
【0050】[0050]
【表1】 [Table 1]
【0051】その後、鋼塊を1250℃で再加熱しラボ熱間
圧延をおこなった。圧延後は種々の水冷条件で一旦冷却
したのち、続けて巻取り相当温度まで空冷し、その温度
の炉で1時間保持したのち炉冷をおこなうことで巻き取
り相当の熱処理とした。熱間圧延後は、冷圧率60%で冷
間圧延し、板厚1.2mmの冷延鋼板を得た。その後、種々
の加熱条件で再結晶焼鈍をおこなった。表2に実験条件
を示す。Then, the steel ingot was reheated at 1250 ° C. and subjected to lab hot rolling. After rolling, it was once cooled under various water-cooling conditions, then continuously air-cooled to a temperature equivalent to the coiling temperature, held in a furnace at that temperature for 1 hour, and then cooled in the furnace to obtain a heat treatment equivalent to the coiling. After the hot rolling, cold rolling was performed at a cold rolling rate of 60% to obtain a cold rolled steel sheet having a sheet thickness of 1.2 mm. Then, recrystallization annealing was performed under various heating conditions. Table 2 shows the experimental conditions.
【0052】[0052]
【表2】 [Table 2]
【0053】ここで、鋼板No.1,2,5,8,10,12,14〜16は
発明鋼板である。それ以外は比較鋼板であり、鋼板No.
3,4は仕上圧延の最終温度、No.6は仕上圧延後の冷却開
始時間、No.7は仕上圧延後の冷却速度、鋼板No.9は冷却
の降下温度、鋼板No.11は巻取温度、No.13は焼鈍におけ
る加熱速度が、それぞれ本発明範囲外である。なお、鋼
板No.1〜15については、焼鈍後1000℃/sで急冷し、350
℃で60sの焼戻し処理を行い、鋼板No.16については焼鈍
後10℃/sでそのまま室温まで冷却した。Here, the steel plates No. 1, 2, 5, 8, 10, 12, 14 to 16 are invention steel plates. The others are comparative steel plates, and the steel plate No.
3 and 4 are the final temperature of finish rolling, No. 6 is the cooling start time after finish rolling, No. 7 is the cooling rate after finish rolling, Steel plate No. 9 is the cooling down temperature, and steel plate No. 11 is winding. For temperature and No. 13, the heating rate in annealing is outside the scope of the present invention. For steel sheets Nos. 1 to 15, after annealing, quenching was performed at 1000 ° C / s, and 350
The steel sheet No. 16 was annealed at 60 ° C. for 60 s, and after annealing, it was cooled to room temperature at 10 ° C./s.
【0054】焼鈍後のサンプルを用いて、引張特性、穴
拡げ特性(伸びフランジ特性)、溶接性を調査した。こ
こで、溶接性は、TIGビードオン溶接で溶接部の硬度分
布を調査し、母材部に対するHAZ軟化部の硬度比(HAZ軟
化部硬度/母材部硬度)で評価した。表3に、試験調査
により得られた特性値をまとめて示す。Tensile properties, hole expansion properties (stretch flange properties), and weldability were investigated using the annealed samples. Here, the weldability was evaluated by examining the hardness distribution of the welded portion by TIG bead-on welding and by the hardness ratio of the HAZ softened portion to the base material portion (HAZ softened portion hardness / base material hardness). Table 3 collectively shows the characteristic values obtained by the test investigation.
【0055】[0055]
【表3】 [Table 3]
【0056】以下、試験調査結果に基づき、製造条件と
特性値の関係を、図を用いて説明する。ここでは、熱延
条件として最終仕上温度が830℃、冷却開始時間が0.8
s、冷却速度が150℃/s、降下温度が100℃、巻取処理温
度が600℃、焼鈍条件として加熱速度が150℃/s、焼鈍温
度が760℃、焼鈍時間が1s、焼鈍後の冷却速度が1000℃/
sをベース(基準条件)としたときの、引張強度におよ
ぼす各製造条件の影響を示す。The relationship between the manufacturing conditions and the characteristic values will be described below with reference to the drawings based on the test survey results. Here, as the hot rolling conditions, the final finishing temperature is 830 ° C and the cooling start time is 0.8
s, cooling rate is 150 ° C / s, falling temperature is 100 ° C, coiling temperature is 600 ° C, heating rate is 150 ° C / s, annealing temperature is 760 ° C, annealing time is 1s, cooling after annealing Speed is 1000 ℃ /
The influence of each manufacturing condition on the tensile strength when s is used as a base (standard condition) is shown.
【0057】図1に引張強度におよぼす仕上最終温度の
影響を示す。ここでは、仕上最終温度のみを変化させ、
他の製造条件は上記ベース条件(基準条件)とした。ま
た、用いた鋼のAr3変態点は800℃であり、熱間圧延の仕
上温度の本発明範囲は800〜880℃となる。図に示すよう
に、引張強度は、仕上最終温度が本発明範囲の下限800
℃を下回るときや上限880℃を上回るとき540〜550MPaで
あるのに対し、本発明の範囲800〜880℃では600〜610MP
aと60MPa前後高くなった。FIG. 1 shows the influence of the final finishing temperature on the tensile strength. Here, only the final finishing temperature is changed,
The other manufacturing conditions were the above-mentioned base conditions (standard conditions). The Ar 3 transformation point of the steel used is 800 ° C., and the finishing temperature range of the present invention for hot rolling is 800 to 880 ° C. As shown in the figure, the tensile strength is the lower limit of the final finish temperature of the present invention range 800
When the temperature is below ℃ or above the upper limit of 880 ℃, it is 540 to 550MPa, whereas in the range of the present invention 800 to 880 ℃, it is 600 to 610MPa.
It became higher around a and 60MPa.
【0058】図2に引張強度におよぼす最終圧延後の急
冷における冷却開始時間の影響を示す。図に示すよう
に、引張強度は、冷却開始時間が本発明範囲の上限1sを
上回るとき550MPaであるのに対し、本発明範囲の1s以下
では610〜620MPaと60MPa以上高くなった。FIG. 2 shows the influence of the cooling start time in the quenching after the final rolling on the tensile strength. As shown in the figure, the tensile strength was 550 MPa when the cooling start time exceeded the upper limit of 1 s in the range of the present invention, whereas it was 610 to 620 MPa and 60 MPa or higher at 1 s or less of the range of the present invention.
【0059】図3に引張強度におよぼす熱間圧延後の急
冷における冷却速度の影響を示す。図に示すように、引
張強度は、冷却速度が本発明範囲の下限100℃/sを下回
るとき540MPaであるのに対し、本発明範囲の100℃/s 以
上では610〜620MPaと70MPa以上高くなった。FIG. 3 shows the influence of the cooling rate in the quenching after hot rolling on the tensile strength. As shown in the figure, the tensile strength is 540 MPa when the cooling rate is below the lower limit of 100 ° C./s of the present invention range, whereas it is 610 to 620 MPa and 70 MPa or more at 100 ° C./s or more of the present invention range. It was
【0060】図4に引張強度におよぼす熱間圧延後の急
冷における降下温度の影響を示す。図に示すように、引
張強度は、降下温度が本発明範囲の下限80℃を下回ると
き555MPaであるのに対し、本発明範囲の80℃以上では61
0〜620MPaと60MPa前後高くなった。FIG. 4 shows the influence of the temperature drop during quenching after hot rolling on the tensile strength. As shown in the figure, the tensile strength is 555 MPa when the falling temperature is below the lower limit of 80 ° C. of the present invention range, while it is 61 at 80 ° C. or higher of the present invention range.
It became higher around 0 to 620MPa and 60MPa.
【0061】図5に引張強度におよぼす巻取り処理温度
の影響を示す。図に示すように、引張強度は、巻取り処
理温度が本発明範囲の上限650℃を上回るとき545MPaで
あるのに対し、本発明範囲の650℃以下では610〜620MPa
と70MPa前後高くなった。FIG. 5 shows the influence of the winding treatment temperature on the tensile strength. As shown in the figure, the tensile strength is 545 MPa when the winding temperature exceeds the upper limit of 650 ° C. of the present invention range, whereas it is 610 to 620 MPa at 650 ° C. or less of the present invention range.
And it became high around 70MPa.
【0062】図6に、引張強度におよぼす冷間圧延後の
焼鈍時の加熱速度の影響を示す。図に示すように、引張
強度は、加熱速度が本発明範囲の下限100℃/s以下のと
き550MPaであるのに対し、本発明範囲の100℃/sを上回
るときは610〜620MPaと60MPa以上高くなった。FIG. 6 shows the influence of the heating rate during annealing after cold rolling on the tensile strength. As shown in the figure, the tensile strength is 550 MPa when the heating rate is lower than the lower limit of 100 ° C./s of the present invention range, whereas it is 610 to 620 MPa and 60 MPa or more when the heating rate exceeds 100 ° C./s of the present invention range. It became high.
【0063】さらに、表3に示すように、本発明鋼板
は、いずれの製造条件についても比較鋼より優れた延
性、穴拡げ性、および耐HAZ軟化特性を有している。さ
らに、発明鋼板の中でも、鋼板No.15に示すように、冷
間圧延後の焼鈍温度を720℃、焼鈍時間を10sとした場
合、および鋼板No.16に示すように、焼鈍後の冷却速度
を10℃/sとした場合においても、優れた引張強度と延性
のバランス、穴拡げ性、耐HAZ軟化特性が得られてい
る。Further, as shown in Table 3, the steel sheet of the present invention has superior ductility, hole expandability, and HAZ softening resistance to the comparative steel under any of the manufacturing conditions. Further, among the invention steel sheets, as shown in Steel sheet No. 15, when the annealing temperature after cold rolling is 720 ° C., when the annealing time is 10 s, and as shown in Steel sheet No. 16, the cooling rate after annealing is shown. Even at 10 ° C / s, an excellent balance between tensile strength and ductility, hole expandability, and HAZ softening resistance are obtained.
【0064】[0064]
【発明の効果】以上のように、本発明では、熱延仕上条
件、冷却条件、巻取条件および冷間圧延後の焼鈍条件を
限定することにより、熱間圧延段階では未再結晶オース
テナイトからの微細なフェライト組織を生成させ、それ
に続く冷間圧延後の再結晶焼鈍過程において急速加熱を
おこなうことにより、組織を飛躍的に細粒化させ、大幅
な強度上昇が得られる。その結果、加工性、溶接性に優
れた高強度冷延鋼板の製造方法が提供され、工業上有効
な効果がもたらされる。As described above, according to the present invention, by limiting the hot rolling finishing condition, the cooling condition, the winding condition and the annealing condition after the cold rolling, in the hot rolling stage, unrecrystallized austenite By generating a fine ferrite structure and performing rapid heating in the subsequent recrystallization annealing process after cold rolling, the structure is dramatically fine-grained and a large increase in strength can be obtained. As a result, a method for producing a high-strength cold-rolled steel sheet excellent in workability and weldability is provided, and an industrially effective effect is brought about.
【図1】引張強度におよぼす仕上最終温度の影響を示す
図。FIG. 1 is a diagram showing the influence of final finishing temperature on tensile strength.
【図2】引張強度におよぼす最終圧延後の急冷における
冷却開始時間の影響を示す図。FIG. 2 is a diagram showing the influence of cooling start time in quenching after final rolling on tensile strength.
【図3】引張強度におよぼす熱間圧延後の急冷の冷却速
度の影響を示す図。FIG. 3 is a diagram showing the influence of the cooling rate of quenching after hot rolling on the tensile strength.
【図4】引張強度におよぼす熱間圧延後の急冷における
降下温度の影響を示す図。FIG. 4 is a diagram showing the influence of the temperature drop during quenching after hot rolling on the tensile strength.
【図5】引張強度におよぼす巻取り処理温度の影響を示
す図。FIG. 5 is a diagram showing the influence of the winding treatment temperature on the tensile strength.
【図6】引張強度におよぼす冷間圧延後の焼鈍時の加熱
速度の影響を示す図。FIG. 6 is a diagram showing an influence of a heating rate during annealing after cold rolling on tensile strength.
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Claims (2)
熱間圧延し、最終圧延後1s以内に100℃/s以上の冷却速
度で80℃以上の温度範囲にわたって冷却し、650℃以下
で巻き取り、酸洗、冷間圧延を行った後、600℃から再
結晶終了までの温度域を100℃/sより大きい加熱速度で
焼鈍することを特徴とする高強度冷延鋼板の製造方法。1. A low carbon steel is hot-rolled at a finishing temperature of Ar 3 to Ar 3 + 80 ° C. and cooled within a temperature range of 80 ° C. or more at a cooling rate of 100 ° C./s or more within 1 s after final rolling. , High strength cold rolling characterized by winding at 650 ° C or less, pickling, cold rolling, and annealing in a temperature range from 600 ° C to the end of recrystallization at a heating rate higher than 100 ° C / s. Steel plate manufacturing method.
Si: 2.0%以下、Mn:2.5%以下、P: 0.1%以下、S: 0.03
%以下、sol.Al: 0.1%以下、N: 0.01%以下を含有し、
残部が実質的に鉄からなることを特徴とする請求項1記
載の高強度冷延鋼板の製造方法。2. The low carbon steel is mass%, C: 0.2% or less,
Si: 2.0% or less, Mn: 2.5% or less, P: 0.1% or less, S: 0.03
% Or less, sol.Al: 0.1% or less, N: 0.01% or less,
The method for producing a high-strength cold-rolled steel sheet according to claim 1, wherein the balance is substantially iron.
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| JP2001223740A JP2003034825A (en) | 2001-07-25 | 2001-07-25 | Manufacturing method of high strength cold rolled steel sheet |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2001223740A JP2003034825A (en) | 2001-07-25 | 2001-07-25 | Manufacturing method of high strength cold rolled steel sheet |
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ID=19057020
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004059021A1 (en) * | 2002-12-24 | 2004-07-15 | Nippon Steel Corporation | High strength steel sheet exhibiting good burring workability and excellent resistance to softening in heat-affected zone and method for production thereof |
| WO2008105524A1 (en) | 2007-02-28 | 2008-09-04 | Jfe Steel Corporation | Steel sheet for cans, hot-rolled steel sheet to be used as the base metal and processes for production of both |
| JP2008291304A (en) * | 2007-05-24 | 2008-12-04 | Jfe Steel Kk | High-strength cold-rolled steel sheet and high-strength hot-dip galvanized steel sheet excellent in deep drawability and strength-ductility balance and manufacturing method thereof |
| KR101344565B1 (en) | 2011-10-28 | 2013-12-26 | 현대제철 주식회사 | Method for manufacturing steel sheet |
| EP2610357A4 (en) * | 2010-08-23 | 2017-11-08 | Nippon Steel & Sumitomo Metal Corporation | Cold-rolled steel sheet and process for production thereof |
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2001
- 2001-07-25 JP JP2001223740A patent/JP2003034825A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2004059021A1 (en) * | 2002-12-24 | 2004-07-15 | Nippon Steel Corporation | High strength steel sheet exhibiting good burring workability and excellent resistance to softening in heat-affected zone and method for production thereof |
| US7749338B2 (en) | 2002-12-24 | 2010-07-06 | Nippon Steel Corporation | High burring, high strength steel sheet excellent in softening resistance of weld heat affected zone and method of production of same |
| WO2008105524A1 (en) | 2007-02-28 | 2008-09-04 | Jfe Steel Corporation | Steel sheet for cans, hot-rolled steel sheet to be used as the base metal and processes for production of both |
| JP2008291304A (en) * | 2007-05-24 | 2008-12-04 | Jfe Steel Kk | High-strength cold-rolled steel sheet and high-strength hot-dip galvanized steel sheet excellent in deep drawability and strength-ductility balance and manufacturing method thereof |
| EP2610357A4 (en) * | 2010-08-23 | 2017-11-08 | Nippon Steel & Sumitomo Metal Corporation | Cold-rolled steel sheet and process for production thereof |
| KR101344565B1 (en) | 2011-10-28 | 2013-12-26 | 현대제철 주식회사 | Method for manufacturing steel sheet |
| CN107858586A (en) * | 2017-11-07 | 2018-03-30 | 东北大学 | A kind of preparation method of high strength and ductility without yield point elongation cold rolling medium managese steel plate |
| CN107858586B (en) * | 2017-11-07 | 2019-05-03 | 东北大学 | A kind of preparation method of high-strength plastic product no-yield flat plate cold-rolled medium manganese steel plate |
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