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IN2015DN02901A - - Google Patents

Info

Publication number
IN2015DN02901A
IN2015DN02901A IN2901DEN2015A IN2015DN02901A IN 2015DN02901 A IN2015DN02901 A IN 2015DN02901A IN 2901DEN2015 A IN2901DEN2015 A IN 2901DEN2015A IN 2015DN02901 A IN2015DN02901 A IN 2015DN02901A
Authority
IN
India
Prior art keywords
adsorption
stream
acidified
sent
spent caustic
Prior art date
Application number
Inventor
Bryan J Kumfer
Andrea J Larson
Chad L Felch
Mark Clark
Original Assignee
Siemens Energy Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Siemens Energy Inc filed Critical Siemens Energy Inc
Publication of IN2015DN02901A publication Critical patent/IN2015DN02901A/en

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/288—Treatment of water, waste water, or sewage by sorption using composite sorbents, e.g. coated, impregnated, multi-layered
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F9/00—Multistage treatment of water, waste water or sewage
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
    • B01D17/02—Separation of non-miscible liquids
    • B01D17/0208—Separation of non-miscible liquids by sedimentation
    • B01D17/0214—Separation of non-miscible liquids by sedimentation with removal of one of the phases
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00—Biological treatment of water, waste water, or sewage
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G19/00—Refining hydrocarbon oils in the absence of hydrogen, by alkaline treatment
    • C10G19/02—Refining hydrocarbon oils in the absence of hydrogen, by alkaline treatment with aqueous alkaline solutions
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G19/00—Refining hydrocarbon oils in the absence of hydrogen, by alkaline treatment
    • C10G19/08—Recovery of used refining agents
    • C—CHEMISTRY; METALLURGY
    • C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
    • C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
    • C10G25/00—Refining of hydrocarbon oils in the absence of hydrogen, with solid sorbents
    • C10G25/12—Recovery of used adsorbent
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/283—Treatment of water, waste water, or sewage by sorption using coal, charred products, or inorganic mixtures containing them
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/285—Treatment of water, waste water, or sewage by sorption using synthetic organic sorbents
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/28—Treatment of water, waste water, or sewage by sorption
    • C02F1/286—Treatment of water, waste water, or sewage by sorption using natural organic sorbents or derivatives thereof
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/40—Devices for separating or removing fatty or oily substances or similar floating material
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/66—Treatment of water, waste water, or sewage by neutralisation; pH adjustment
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F1/00—Treatment of water, waste water, or sewage
    • C02F1/72—Treatment of water, waste water, or sewage by oxidation
    • C02F1/74—Treatment of water, waste water, or sewage by oxidation with air
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/10—Inorganic compounds
    • C02F2101/101—Sulfur compounds
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/30—Organic compounds
    • C02F2101/32—Hydrocarbons, e.g. oil
    • C02F2101/327—Polyaromatic Hydrocarbons [PAH's]
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2101/00—Nature of the contaminant
    • C02F2101/30—Organic compounds
    • C02F2101/34—Organic compounds containing oxygen
    • C02F2101/345—Phenols
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2103/00—Nature of the water, waste water, sewage or sludge to be treated
    • C02F2103/34—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32
    • C02F2103/36—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds
    • C02F2103/365—Nature of the water, waste water, sewage or sludge to be treated from industrial activities not provided for in groups C02F2103/12 - C02F2103/32 from the manufacture of organic compounds from petrochemical industry (e.g. refineries)
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00—Controlling or monitoring parameters in water treatment
    • C02F2209/06—Controlling or monitoring parameters in water treatment pH
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2209/00—Controlling or monitoring parameters in water treatment
    • C02F2209/08—Chemical Oxygen Demand [COD]; Biological Oxygen Demand [BOD]
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F2303/00—Specific treatment goals
    • C02F2303/16—Regeneration of sorbents, filters
    • C—CHEMISTRY; METALLURGY
    • C02—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
    • C02F3/00—Biological treatment of water, waste water, or sewage
    • C02F3/02—Aerobic processes
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
    • Y02W10/00—Technologies for wastewater treatment
    • Y02W10/10—Biological treatment of water, waste water, or sewage

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • Biodiversity & Conservation Biology (AREA)
  • Microbiology (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Water Treatment By Sorption (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Analytical Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Method and apparatus to treat a spent caustic from the petroleum industry , which may comprise sulfides, mercaptans , cresylic and naphtenic acids and phenols. The spent caustic is first acidified with an acid to produce an acidified stream. The acidified stream may be separated into an oily phase, a solid phase and an aqueous phase. The aqueous phase is sent to an adsorption stage. The adsorption stage may comprise a pre -filter such as a walnut shell filter. It comprises a main filtering stage in one or more adsorption vessels connected in parallel and/or in series. The vessels may comprise granular activated carbon and/or an adsorption polymer such as a styrene- divinylbenzen polymer. A polished stream is produced which is neutralized with a base and then sent to a biological treatment step. Regeneration of the adsorption media is carried out using the spent caustic stream itself and/or using steam. The waste regeneration effluent is sent back to the beginning of the treatment method.
IN2901DEN2015 2012-10-26 2013-10-22 IN2015DN02901A (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201261718774P 2012-10-26 2012-10-26
PCT/US2013/066102 WO2014066338A1 (en) 2012-10-26 2013-10-22 Methods and systems for treating spent caustic and regenerating media

Publications (1)

Publication Number Publication Date
IN2015DN02901A true IN2015DN02901A (en) 2015-09-11

Family

ID=49515558

Family Applications (1)

Application Number Title Priority Date Filing Date
IN2901DEN2015 IN2015DN02901A (en) 2012-10-26 2013-10-22

Country Status (8)

Country Link
US (1) US10053375B2 (en)
EP (1) EP2911984A1 (en)
KR (1) KR20150077460A (en)
CN (1) CN104870380B (en)
BR (1) BR112015009248A2 (en)
IN (1) IN2015DN02901A (en)
RU (1) RU2015119652A (en)
WO (1) WO2014066338A1 (en)

Families Citing this family (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US9718712B2 (en) * 2013-07-12 2017-08-01 Uop Llc Methods and systems for treating caustic materials
CN105278330A (en) * 2015-11-06 2016-01-27 哈尔滨商业大学 Oil sewage treatment system and treatment method based on WebAccess
CN106746100B (en) * 2015-11-19 2020-09-11 中国石油化工股份有限公司 Treatment method of ethylene refining waste alkali liquor
CN106746101B (en) * 2015-11-19 2020-09-11 中国石油化工股份有限公司 Method for treating ethylene waste alkali liquor
EP3468924B1 (en) * 2016-08-31 2023-05-03 Siemens Energy, Inc. Process for treatment of high total dissolved solids wastewater
US10435362B2 (en) 2016-12-21 2019-10-08 Uop Llc Process for oxidizing one or more thiol compounds and subsequent separation in a single vessel
US10240096B1 (en) * 2017-10-25 2019-03-26 Saudi Arabian Oil Company Integrated process for activating hydroprocessing catalysts with in-situ produced sulfides and disulphides
US12139425B2 (en) * 2018-08-28 2024-11-12 Lummus Technology Llc Wet air oxidation of a spent material with spent caustic addition
CN109777741B (en) * 2019-01-15 2022-01-04 昆明理工大学 Method for efficiently utilizing walnut shells
CN110317963B (en) * 2019-08-13 2021-07-13 包头稀土研究院 Method for extracting and separating rare earth chloride solution prepared by acid method
CN110331302B (en) * 2019-08-13 2021-06-08 包头稀土研究院 Method for reducing acid dosage in extraction separation of medium and heavy rare earth
CN110331285B (en) * 2019-08-13 2020-10-02 包头稀土研究院 Method for extracting and separating light rare earth chloride solution from rare earth chloride solution prepared by alkali method
CN110306050B (en) * 2019-08-13 2021-04-16 包头稀土研究院 Method for extraction and separation of medium and heavy rare earths
CN110306045B (en) * 2019-08-13 2021-04-16 包头稀土研究院 Method for removing organic impurities in medium and heavy rare earth chloride solution
CN110813983B (en) * 2019-10-31 2021-09-17 金能科技股份有限公司 Method and device for recycling solid waste phenol residues produced in alkylphenol production process
FR3124744A1 (en) * 2021-07-02 2023-01-06 Suez Groupe PROCESS FOR IN SITU REGENERATION OF AN ADSORBENT MEDIA
WO2024206639A1 (en) * 2023-03-31 2024-10-03 Carollo Engineers, Inc. Systems and methods for water treatment using ion exchange and water softening techniques
CN117964178B (en) * 2024-03-25 2024-06-21 矿冶科技集团有限公司 A method for removing oil from raffinate by steam

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4049546A (en) 1974-11-11 1977-09-20 Rohm And Haas Company Decolorization of effluents from pulp mills
JPS5778927U (en) * 1980-11-01 1982-05-15
JPS5778927A (en) * 1980-11-04 1982-05-17 Hitachi Ltd Treatment of offensive odor
US4695386A (en) * 1985-05-20 1987-09-22 Advanced Separation Technologies Incorporated Process for the decolorization of pulp mill process streams
US5635078A (en) * 1993-05-12 1997-06-03 Mobil Oil Corporation Rejuvenated catalytic oxidation of waste water, particularly for removal of cyanide and sulfur compounds
US6398965B1 (en) * 1998-03-31 2002-06-04 United States Filter Corporation Water treatment system and process
US6929942B2 (en) * 1999-08-10 2005-08-16 Council Of Scientific And Industrial Research Process for the treatment of industrial effluents using marine algae to produce potable wafer
US7005076B2 (en) * 2003-06-06 2006-02-28 Rmt, Inc. Caustic solution treatment process
CN1187275C (en) 2003-06-19 2005-02-02 上海交通大学 Treatment process for two stage recycling alkali waste liquid drained off by process system of synthesizing octanol
US8097163B1 (en) * 2006-04-06 2012-01-17 Produced Water Development, Llc Purification of oil field production water for beneficial use
CN101134616B (en) 2006-08-30 2011-02-09 中国石油天然气股份有限公司 An equipment system for comprehensive treatment of waste liquid containing acid and alkali in refinery
US20100051556A1 (en) * 2008-08-29 2010-03-04 Grott Gerald J Methods of purifiying water using waste brines to regenerate ion-exchange resins
US7828962B2 (en) * 2008-11-20 2010-11-09 Merichem Company Apparatus for treating a waste stream
CN101475274A (en) * 2008-12-31 2009-07-08 大连力达环境工程有限公司 Integrative electroplating waste treatment process
CN101570370B (en) * 2009-04-26 2011-08-10 赵志军 Method for high resource treatment of cyclohexanone waste saponification lye
EA025298B1 (en) * 2009-07-08 2016-12-30 Сауди Арабиан Ойл Компани Low concentration wastewater treatment system and process
CN201648046U (en) 2009-12-08 2010-11-24 江苏三星化工有限公司 Nutshell filtering sewage treatment device
US8734650B2 (en) 2010-12-01 2014-05-27 Veolia Water Solutions & Technologies North America, Inc. Method for recovering gas from shale reservoirs and purifying resulting produced water to allow the produced water to be used as drilling or frac water, or discharged to the environment

Also Published As

Publication number Publication date
WO2014066338A1 (en) 2014-05-01
US10053375B2 (en) 2018-08-21
KR20150077460A (en) 2015-07-07
US20150284264A1 (en) 2015-10-08
CN104870380B (en) 2017-08-04
EP2911984A1 (en) 2015-09-02
BR112015009248A2 (en) 2017-07-04
RU2015119652A (en) 2016-12-20
CN104870380A (en) 2015-08-26

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