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HK1229643B - Low tar menthol cigarette - Google Patents

Low tar menthol cigarette Download PDF

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Publication number
HK1229643B
HK1229643B HK17103272.4A HK17103272A HK1229643B HK 1229643 B HK1229643 B HK 1229643B HK 17103272 A HK17103272 A HK 17103272A HK 1229643 B HK1229643 B HK 1229643B
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HK
Hong Kong
Prior art keywords
menthol
filter
cigarette
tar
low
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HK17103272.4A
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Chinese (zh)
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HK1229643A1 (en
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石川信幸
香川慎二郎
久保田啓之
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日本烟草产业株式会社
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Publication of HK1229643A1 publication Critical patent/HK1229643A1/en
Publication of HK1229643B publication Critical patent/HK1229643B/en

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Description

低焦油薄荷醇香烟low-tar menthol cigarettes

技术领域Technical Field

本发明涉及一种低焦油量、且添加有薄荷醇的带过滤嘴的香烟。The present invention relates to a low-tar cigarette with a filter tip and added with menthol.

背景技术Background Art

在带过滤嘴的香烟中,已知有以吸烟时的烟中成分的调整为目的,通过在过滤嘴上设置通气孔来调整流入空气的量的方法。In filter-tipped cigarettes, there is a known method of providing ventilation holes in the filter to adjust the amount of air flowing in for the purpose of adjusting the components in the smoke during smoking.

另外,在一般的带过滤嘴的香烟中,已知有根据烟中成分量来调整过滤嘴的通气阻力的方法。In general filter-tipped cigarettes, a method of adjusting the ventilation resistance of the filter according to the amount of components in the smoke is known.

在专利文献1中,公开了一种带过滤嘴的香烟,其具有过滤嘴的通气阻力为50mmH2O/100mm(相当于13.5mmH2O/27mm)、通气比例为20~80%的过滤嘴。Patent Document 1 discloses a filter-tipped cigarette having a filter with a ventilation resistance of 50 mmH 2 O/100 mm (equivalent to 13.5 mmH 2 O/27 mm) and a ventilation ratio of 20 to 80%.

另外,在专利文献2中,记载了具有2个过滤嘴部分的带过滤嘴的香烟,且记载了:将2个过滤嘴部分调整为其中1个过滤嘴部分比另一个的通气阻力大,并且将由卷装过滤嘴的接装纸流入的空气量调整为规定范围,由此不仅能降低主流烟中尼古丁及焦油的浓度,而且呈现充分的吸吮。Patent Document 2 describes a filter-tipped cigarette having two filter portions. The disclosure states that by adjusting the two filter portions so that one has a greater ventilation resistance than the other, and adjusting the amount of air flowing in through the tipping paper of the wrapped filter within a specified range, the concentrations of nicotine and tar in mainstream smoke can be reduced while also providing a sufficient draw.

另一方面,在日本市场上,薄荷醇香烟的需求逐年提高,目前没有的高薄荷醇的香烟被投入到市场。作为在过滤嘴中添加薄荷醇那样的香料的方法,在专利文献3中记载了将使薄荷醇溶解及分散于过滤嘴制造工序中所使用的增塑剂而成的加香液添加在醋酸纤维束中。Meanwhile, demand for menthol cigarettes is increasing year by year in the Japanese market, leading to the introduction of previously unavailable high-menthol cigarettes. Patent Document 3 describes a method for adding a flavoring agent, such as menthol, to filters. This method involves adding a flavoring liquid, prepared by dissolving and dispersing menthol in a plasticizer used in the filter manufacturing process, to acetate fiber bundles.

在专利文献4中记载了使薄荷醇保持于香料的担载体,防止薄荷醇量随着经过天数而减少的方法。Patent Document 4 describes a method of retaining menthol in a flavor carrier to prevent the amount of menthol from decreasing over time.

另外,在专利文献5中公开了使用具有保香性的片材来防止薄荷醇量因经过天数而减少的方法。Patent Document 5 discloses a method of preventing the decrease in menthol content over time by using a sheet having a flavor-retaining property.

另外,在专利文献6中记载了预先添加并吸附香料以防止烟中薄荷醇量随着经过天数而减少的过滤嘴制造方法等。Patent Document 6 also describes a filter manufacturing method in which flavoring is preliminarily added and adsorbed to prevent the amount of menthol in smoke from decreasing over time.

现有技术文献Prior art literature

专利文献Patent Literature

专利文献1:日本实开昭62-86894号公报Patent Document 1: Japanese Utility Model Publication No. 62-86894

专利文献2:日本特开平11-069965号公报Patent Document 2: Japanese Patent Application Laid-Open No. 11-069965

专利文献3:日本特公昭43-28077号公报Patent Document 3: Japanese Patent Publication No. 43-28077

专利文献4:日本特开2012-29637号公报Patent Document 4: Japanese Patent Application Laid-Open No. 2012-29637

专利文献5:国际公开第2011/118040号Patent Document 5: International Publication No. 2011/118040

专利文献6:国际公开第2012/004853号Patent Document 6: International Publication No. 2012/004853

发明内容Summary of the Invention

发明所要解决的课题Problems to be solved by the invention

上述专利文献1中记载的发明将过滤嘴的通气阻力和由设置于接装纸的开孔部流入空气的比例调整为规定范围,但并未阐明其目的。The invention described in Patent Document 1 adjusts the ventilation resistance of the filter and the ratio of air flowing in from the openings provided in the tipping paper within predetermined ranges, but the purpose thereof is not clarified.

另外,专利文献2中记载的发明的目的在于,通过降低作为烟中成分的尼古丁或焦油的量的同时提高香烟的制品通气阻力,呈现充分的吸吮。Furthermore, the invention described in Patent Document 2 aims to provide a sufficient suck by reducing the amount of nicotine or tar as components in smoke and increasing the product ventilation resistance of the cigarette.

作为香烟用过滤嘴的性质,通常在通气比例低且具有高焦油量的带过滤嘴的香烟中,使用低通气阻力的过滤嘴,而在高通气比例且具有低焦油量的带过滤嘴的香烟中,使用高通气阻力的过滤嘴。As for the properties of cigarette filters, generally, low ventilation resistance filters are used for filter-tipped cigarettes with low ventilation ratios and high tar content, while high ventilation resistance filters are used for filter-tipped cigarettes with high ventilation ratios and low tar content.

如上,虽然进行了着眼于过滤嘴的通气阻力、通气比例(空气流入量)的研究,但并未尝试将添加了薄荷醇的带过滤嘴的香烟、尤其是低焦油量的带过滤嘴的香烟特定化,并调整其通气阻力或通气比例。As mentioned above, although research has been conducted focusing on the ventilation resistance and ventilation ratio (air inflow) of filter tips, no attempt has been made to specify menthol-added filter cigarettes, especially low-tar filter cigarettes, and adjust their ventilation resistance or ventilation ratio.

另一方面,具有薄荷醇的带过滤嘴的香烟在吸烟时烟中的薄荷醇量根据添加于香烟的薄荷醇的加香量而进行调整,但使简单地添加于香烟的香料量增加的情况下,在包覆香烟烟丝的卷纸上产生溶解有烟草色素的薄荷醇的渗出而附着于卷纸,因此,成为外观上不优选的状态。另外,烟中薄荷醇量与香烟的焦油量成正比地升高,因此,关于一般被称为低焦油的焦油量为5mg以下的香烟,一般烟中薄荷醇量会变低,作为该解决策略,只能在香烟中添加不引起渗出等问题所能添加的最大量的薄荷醇,此外别无他法。On the other hand, the amount of menthol in menthol-filtered cigarettes is adjusted by the amount of menthol flavoring added to the cigarettes during smoking. However, simply increasing the amount of flavoring added to the cigarettes causes menthol, dissolved in tobacco pigment, to bleed out of the cigarette wrapping paper and adhere to the wrapping paper, resulting in an undesirable appearance. Furthermore, the amount of menthol in the smoke increases proportionally with the tar content of the cigarette. Therefore, cigarettes with a tar content of 5 mg or less, generally known as low-tar cigarettes, typically contain a low menthol content. As a solution to this problem, there is no alternative but to add the maximum amount of menthol that can be added to the cigarettes without causing bleed-out or other problems.

专利文献3中记载的方法产生如下问题:添加于过滤嘴部的薄荷醇在制品的贮藏中被吸附于过滤嘴的丝束,烟中薄荷醇量随着经过天数而显著地降低。The method described in Patent Document 3 has the following problem: menthol added to the filter is adsorbed to the filter tow during storage of the product, and the amount of menthol in the smoke decreases significantly over time.

专利文献4中记载的方法可举出如下等问题:使用香料的担载体会导致成本增加;而在过滤嘴内部添加担载体的情况下,需要另外设置担载体的添加工序,因此,制造适性变得复杂且困难。The method described in Patent Document 4 has the following problems: using a flavoring carrier increases costs; and when adding the carrier inside the filter, a separate carrier addition step is required, making manufacturing complicate and difficult.

关于专利文献5中记载的发明,也与专利文献4中记载的发明同样地,担心成本的增加、因向香烟烟丝中添加保香性片材而产生的香烟制造适性方面的问题等。The invention described in Patent Document 5, like the invention described in Patent Document 4, has concerns about increased costs and problems with cigarette manufacturing suitability caused by adding a flavor-retaining sheet to shredded cigarette tobacco.

作为用于使烟中薄荷醇量增加的方法,专利文献6中记载的发明中公开了增加过滤嘴中薄荷醇添加量的方法,但为了在过滤嘴的增塑剂中添加薄荷醇,需要选择能溶解薄荷醇的增塑剂。一般而言,由于薄荷醇难溶于作为增塑剂所使用的甘油醋酸酯,因此,需要混合聚乙二醇那样的溶剂,使薄荷醇溶解来制备加香液。另外,在不打算添加比较大量的薄荷醇量的情况下,需要大量的增塑剂及可溶解薄荷醇的其它溶剂,因此,担心对加香液的渗出、过滤嘴的硬度等的影响。另外,在欲使薄荷醇吸附于过滤嘴内部的情况下,仅在增塑剂中混合薄荷醇而添加,效果低,另外,花费比较长的时间,例如在醋酸酯纤维中一同添加增塑剂和薄荷醇时,需要实施高温处理。但是,这些工序需要在过滤嘴的制造时或制造之后另设工序,很难说是可适用于实际工序的技术。As a method for increasing the amount of menthol in tobacco, the invention described in Patent Document 6 discloses a method for increasing the amount of menthol added to filters. However, in order to add menthol to the filter's plasticizer, a plasticizer that can dissolve menthol is required. Generally, menthol is poorly soluble in the glycerol acetate used as a plasticizer, so a solvent such as polyethylene glycol must be mixed to dissolve the menthol in order to prepare the flavoring liquid. Furthermore, if a relatively large amount of menthol is not intended to be added, a large amount of plasticizer and other menthol-soluble solvents are required, which raises concerns about the effects on the flavoring liquid's oozing out and the filter's hardness. Furthermore, if menthol is to be adsorbed into the filter, simply mixing it with the plasticizer is ineffective and time-consuming. For example, when adding the plasticizer and menthol to acetate fibers simultaneously, a high-temperature treatment is required. However, these steps require separate steps during or after filter manufacturing, making them difficult to describe as practically applicable technologies.

尚无将过滤嘴的通气阻力及带过滤嘴的香烟的通气比例与吸烟时的烟中薄荷醇浓度关联起来研究的实例,需要一种能提高薄荷醇制品中薄荷醇量的稳定性,特别是能提高低焦油香烟吸烟时的烟中薄荷醇量、或贮藏后的烟中薄荷醇量的稳定性的技术。There are no studies that correlate the ventilation resistance of filter tips and the ventilation ratio of filter-tipped cigarettes with the menthol concentration in the smoke during smoking. Therefore, there is a need for a technology that can improve the stability of the menthol content in menthol products, particularly the stability of the menthol content in the smoke of low-tar cigarettes during smoking or after storage.

在本发明中,提供一种低焦油薄荷醇香烟,其不仅能提高吸烟时的烟中薄荷醇量,并且贮藏后的烟中薄荷醇量的变化也少。The present invention provides a low-tar menthol cigarette that not only increases the amount of menthol in smoke during smoking but also minimizes changes in the amount of menthol in the smoke after storage.

用于解决课题的方案Solutions to Problems

本发明人深入研究的结果可知:一种低焦油薄荷醇香烟可以解决上述课题,所述低焦油薄荷醇香烟为具有烟杆部和用接装纸卷装成的过滤嘴部、且焦油量为5mg以下的低焦油薄荷醇香烟,所述过滤嘴部含有由醋酸纤维素丝束构成的单一区段,所述过滤嘴部的通气阻力为25~80mmH2O/27mm,并且来自穿设于所述接装纸的通气孔的流入空气的通气比例为55%以上,在所述过滤嘴部中添加有薄荷醇,直至完成本发明。As a result of intensive research, the present inventors have discovered a low-tar menthol cigarette that can solve the above-mentioned problems. The low-tar menthol cigarette comprises a cigarette stem and a filter wrapped with tipping paper, and has a tar yield of 5 mg or less. The filter comprises a single segment formed of cellulose acetate tow, has an airflow resistance of 25 to 80 mmH2O /27 mm, and a ventilation ratio of inflowing air through ventilation holes formed in the tipping paper of 55% or greater. Menthol is added to the filter, leading to the completion of the present invention.

即,本发明如下所述。That is, the present invention is as follows.

[1]一种低焦油薄荷醇香烟,其为具有烟杆部和用接装纸卷装成的过滤嘴部、且焦油量为5mg以下的低焦油薄荷醇香烟,其中,所述过滤嘴部含有由醋酸纤维素丝束构成的单一区段,所述过滤嘴部的通气阻力为25~80mmH2O/27mm,并且来自穿设于所述接装纸的通气孔的流入空气的通气比例为55%以上,在所述过滤嘴部中添加有薄荷醇。[1] A low-tar menthol cigarette comprising a cigarette rod and a filter wrapped with tipping paper, and having a tar content of 5 mg or less, wherein the filter comprises a single segment formed of cellulose acetate tow, the filter having an air flow resistance of 25 to 80 mmH2O /27 mm, and a ventilation ratio of inflowing air from ventilation holes formed in the tipping paper of 55% or more, and menthol is added to the filter.

[2]如[1]所述的低焦油薄荷醇香烟,其中,所述过滤嘴部中薄荷醇的添加量为每1根低焦油薄荷醇香烟8mg/根以上。[2] The low-tar menthol cigarette according to [1], wherein the amount of menthol added to the filter is 8 mg or more per low-tar menthol cigarette.

[3]如[1]或[2]所述的低焦油薄荷醇香烟,其中,所述烟杆部或过滤嘴部具有阻力体。[3] The low-tar menthol cigarette according to [1] or [2], wherein the cigarette rod or filter has a resistance body.

[4]如[3]所述的低焦油薄荷醇香烟,其中,所述阻力体为胶囊或节流孔。[4] The low-tar menthol cigarette according to [3], wherein the resistance body is a capsule or a throttle hole.

[5]如[1]~[4]中任一项所述的低焦油薄荷醇香烟,其中,所述过滤嘴部的通气阻力为25~50mmH2O/27mm,并且空气流入的通气比例为70%以上。[5] The low-tar menthol cigarette according to any one of [1] to [4], wherein the filter portion has a ventilation resistance of 25 to 50 mmH 2 O/27 mm and a ventilation ratio of air inflow of 70% or more.

[6]如[1]~[5]中任一项所述的低焦油薄荷醇香烟,其中,所述低焦油薄荷醇香烟的圆周长度为20.0~27.0mm。[6] The low-tar menthol cigarette according to any one of [1] to [5], wherein the circumference of the low-tar menthol cigarette is 20.0 to 27.0 mm.

发明的效果Effects of the Invention

本发明的低焦油薄荷醇香烟提高了吸烟时的烟中薄荷醇量,并且贮藏后的烟中薄荷醇量的变化少。The low-tar menthol cigarette of the present invention increases the amount of menthol in the smoke during smoking and has little change in the amount of menthol in the smoke after storage.

附图说明BRIEF DESCRIPTION OF THE DRAWINGS

图1是表示带过滤嘴的香烟的贮藏期间和烟中薄荷醇量的减少率的关系的图。FIG. 1 is a graph showing the relationship between the storage period of filter-tipped cigarettes and the rate of decrease in the amount of menthol in the smoke.

图2是表示贮藏后的带过滤嘴的香烟中的初期薄荷醇添加量和薄荷醇释放率的关系的图。FIG. 2 is a graph showing the relationship between the initial menthol addition amount and the menthol release rate in stored filter-tipped cigarettes.

具体实施方式DETAILED DESCRIPTION

以下,对本发明示出实施方式及例示物等详细地进行说明,但本发明并不限定于以下的实施方式及例示物等,在不脱离本发明的要点的范围内可以任意地变更而实施。Hereinafter, the present invention will be described in detail with reference to embodiments and examples. However, the present invention is not limited to the following embodiments and examples, and can be implemented with arbitrary modifications without departing from the gist of the present invention.

本发明的低焦油薄荷醇香烟为具有烟杆部和用接装纸卷装成的过滤嘴部的带过滤嘴的香烟,所述过滤嘴部含有由单一的醋酸纤维素丝束构成的单一区段,所述过滤嘴部的通气阻力为25~80mmH2O/27mm,并且来自穿设于所述接装纸的通气孔的流入空气的通气比例为55%以上,在所述过滤嘴部添加有薄荷醇。The low-tar menthol cigarette of the present invention is a filter-tipped cigarette having a tobacco rod and a filter wrapped with tipping paper. The filter comprises a single segment formed from a single cellulose acetate tow. The filter has an airflow resistance of 25 to 80 mmH2O /27 mm, and the ventilation ratio of inflowing air through ventilation holes formed in the tipping paper is 55% or more. Menthol is added to the filter.

烟杆可以采用公知的方式。作为香烟的烟草烟丝的种类,可以没有特别限定地使用公知的烟草烟丝,将用卷纸卷装烟草烟丝而成的结构设为烟杆。在烟杆中,为了调整低焦油薄荷醇香烟(带过滤嘴的香烟)的通气阻力,可以在烟杆的内部配置胶囊或节流孔那样的阻力体。The cigarette rod can be made of a known type. The type of tobacco used in the cigarette can be any known type, and the cigarette rod is formed by wrapping the tobacco in rolling paper. To adjust the ventilation resistance of low-tar menthol cigarettes (filtered cigarettes), a resistance element such as a capsule or a throttle hole can be placed inside the cigarette rod.

构成本发明的低焦油薄荷醇香烟的过滤嘴部用接装纸卷装。本发明中可以使用的接装纸没有特别限制,可以使用空气不透过性的纸。The filter portion of the low-tar menthol cigarette of the present invention is wrapped with tipping paper. The tipping paper that can be used in the present invention is not particularly limited, and air-impermeable paper can be used.

通过在接装纸上沿卷装的过滤嘴的周向穿设多个开孔(通气孔)而设置空气流入方式,可以调整由穿设于低焦油薄荷醇香烟的所述接装纸的通气孔流入的空气的通气比例。作为开孔的方式,可以举出,沿着过滤嘴的周向以成为一列以上的方式设置。By providing a plurality of openings (ventilation holes) in the tipping paper along the circumference of the wrapped filter, an air inflow pattern is established. This allows for adjustment of the ventilation ratio of air flowing in through the ventilation holes in the tipping paper of a low-tar menthol cigarette. Examples of the opening pattern include providing the openings in one or more rows along the circumference of the filter.

形成有被穿设的多个开孔的接装纸的通气度通常为100~7000C.U.。在此,C.U.表示差压为100mmH2O(980.665Pa)时、在1分钟(60秒)内通过接装纸1cm2(100mm2)的流量(mL、(0.001L))。Tipping paper having a plurality of perforated openings generally has an air permeability of 100 to 7000 C.U. Here, CU represents the flow rate (mL, (0.001 L)) of fluid passing through 1 cm 2 (100 mm 2 ) of tipping paper in 1 minute (60 seconds) at a differential pressure of 100 mmH 2 O (980.665 Pa).

本发明的低焦油薄荷醇香烟的流入空气的通气比例为55%以上。该通气比例优选为61%以上,进一步优选为70%以上。达到该通气比例时,吸烟者会更强地感觉到薄荷醇的香味。该通气比例时的过滤嘴的通气阻力如后所述,为80mmH2O/27mm以下。The low-tar menthol cigarette of the present invention has an inflow air ventilation ratio of 55% or greater. This ventilation ratio is preferably 61% or greater, and more preferably 70% or greater. At this ventilation ratio, smokers experience a stronger sense of menthol flavor. As described below, the filter's ventilation resistance at this ventilation ratio is 80 mmH₂O /27 mm or less.

本发明中的流入空气的通气比例是指:将通过(具有空气流入方式)接装纸且进入带过滤嘴的香烟内部的空气流量与以标准流量17.5cm3/秒抽吸带过滤嘴的香烟(制品)时吸口端的空气流量之比以百分率表示。The ventilation ratio of inflow air in the present invention refers to the ratio, expressed as a percentage, of the air flow rate passing through the tipping paper (with air inflow) and entering the interior of the filter-tipped cigarette to the air flow rate at the mouth end when the filter-tipped cigarette (product) is smoked at a standard flow rate of 17.5 cm 3 /s.

空气流入的通气比例例如通过改变上述的多个开孔的大小、数目及列数、或改变接装纸的原料并改变通气度而进行调整。例如,开孔的位置可以配置于距吸口端12~20mm的位置。The ventilation ratio of air inflow can be adjusted by, for example, changing the size, number, and number of rows of the plurality of openings, or by changing the material of the tipping paper and changing the air permeability. For example, the openings can be positioned 12 to 20 mm from the suction port.

本发明中的过滤嘴部的通气阻力是指:用空气不透过性的橡胶包覆过滤嘴部以使空气不从其侧面流入,并从其一端以17.5cm3/秒的流量抽吸时,过滤嘴部的差压PD(mmH2O)。The air flow resistance of the filter in the present invention refers to the differential pressure PD (mmH 2 O) of the filter when the filter is covered with air-impermeable rubber to prevent air from flowing in from the sides and inhaled from one end at a flow rate of 17.5 cm 3 / sec.

构成本发明的低焦油薄荷醇香烟的过滤嘴部含有单一区段。即,用于本发明的带过滤嘴的香烟的过滤嘴部具有一个由醋酸纤维素丝束构成的单一区段。另外,由醋酸纤维素丝束构成的区段可以具有胶囊或节流孔那样的阻力体。The filter portion of the low-tar menthol cigarette of the present invention comprises a single segment. Specifically, the filter portion of the filter-tipped cigarette of the present invention comprises a single segment made of cellulose acetate tow. Furthermore, the segment made of cellulose acetate tow may include a resistance member such as a capsule or an orifice.

就本发明的低焦油薄荷醇香烟的过滤嘴部的通气阻力而言,过滤嘴部配置胶囊、节流孔那样的阻力体的情况下,以不含有其阻力体的过滤嘴本身的值为基准。Regarding the ventilation resistance of the filter of the low-tar menthol cigarette of the present invention, when a resistance member such as a capsule or an orifice is provided in the filter, the value of the filter itself without the resistance member is used as a reference.

胶囊或节流孔的形状没有特别限制,可以适用公知的形状。The shape of the capsule or the orifice is not particularly limited, and known shapes can be applied.

构成用于本发明的过滤嘴部的由醋酸纤维素丝束构成的单一区段的材料为醋酸纤维素。作为构成醋酸纤维素丝束的醋酸纤维素纤维,可以举出例如单丝纤度为1.0~8.0旦尼尔左右、总纤度为15000~70000旦尼尔的方式,另外,可以举出圆形、椭圆形、Y字型、X字型、I字型的纤维截面形状的方式。过滤嘴内部可以举出例如用醋酸纤维素丝束均匀地填充成的方式。The material constituting the individual segments of cellulose acetate tow used in the filter portion of the present invention is cellulose acetate. Examples of the cellulose acetate fibers constituting the cellulose acetate tow include, for example, those having a single-filament fineness of approximately 1.0 to 8.0 denier and a total fineness of 15,000 to 70,000 denier. Examples include those having circular, oval, Y-shaped, X-shaped, and I-shaped fiber cross-sectional shapes. For example, the interior of the filter can be uniformly filled with cellulose acetate tow.

用于本发明的低焦油薄荷醇香烟的过滤嘴部的通气阻力为25~80mmH2O/27mm。需要说明的是,用于通气阻力的单位的“27mm”是指过滤嘴部的纵向的长度。The air flow resistance of the filter used in the low-tar menthol cigarette of the present invention is 25 to 80 mmH 2 O/27 mm. It should be noted that the unit "27 mm" used for the air flow resistance refers to the longitudinal length of the filter.

由于过滤嘴的通气阻力为25mmH2O/27mm以上,从而可以充分地进行吸烟时的烟的过滤。另一方面,由于过滤嘴的通气阻力为80mmH2O/27mm以下,从而在吸烟时不引起烟的过度过滤,可以有效地降低薄荷醇的滤过率。另外,由于过滤嘴的密度低,因此在贮藏时难以引起薄荷醇的吸附。The filter's air resistance is 25 mmH₂O /27 mm or greater, ensuring adequate filtration of smoke during smoking. Meanwhile, a filter's air resistance is 80 mmH₂O /27 mm or less, preventing excessive filtration of smoke during smoking and effectively reducing the filtration rate of menthol. Furthermore, the filter's low density reduces menthol adsorption during storage.

由于过滤嘴的通气阻力为该范围、且将带过滤嘴的香烟的通气比例设定为后述规定的范围,从而可以将烟中薄荷醇浓度纳入期望的范围。另外,在所述过滤嘴部的通气阻力为25~50mmH2O/27mm、并且空气流入的通气比例为70%以上的情况下,可以更良好地得到该效果。By setting the ventilation resistance of the filter within this range and the ventilation ratio of the filter-tipped cigarette within the range specified below, the menthol concentration in the smoke can be kept within a desired range. This effect is further enhanced when the ventilation resistance of the filter portion is 25-50 mmH₂O /27 mm and the ventilation ratio of air inflow is 70% or greater.

关于过滤嘴的通气阻力的调整,如目前已知的那样,可以通过例如适当地选择醋酸纤维素丝束的总纤度(填充量)及单丝纤度而调整。具体而言,作为醋酸纤维素丝束的规格,增大单丝纤度、减小总纤度时,可以降低通气阻力。As is known, the ventilation resistance of the filter can be adjusted by, for example, appropriately selecting the total fineness (filling amount) and the single filament fineness of the cellulose acetate tow. Specifically, increasing the single filament fineness and decreasing the total fineness of the cellulose acetate tow can reduce the ventilation resistance.

用于过滤嘴的丝束重量作为将过滤嘴的长度设为27mm时的值,可以举出例如0.100~0.200g,也可以在该范围内调节重量而调整过滤嘴的密度。The tow weight used for the filter can be, for example, 0.100 to 0.200 g when the filter length is 27 mm. The density of the filter can be adjusted by adjusting the weight within this range.

就本发明的低焦油薄荷醇香烟而言,作为其每1根的通气阻力(带过滤嘴的香烟1根的通气阻力),不存在阻力体的情况下,可以举出大概为20~70mmH2O的方式。The ventilation resistance per cigarette of the low-tar menthol cigarette of the present invention (the ventilation resistance of a single filter cigarette) is approximately 20 to 70 mmH 2 O when no resistor is present.

在此,1根带过滤嘴的香烟的通气阻力是指包含从过滤嘴的一端以17.5cm3/秒的流量抽吸时的通气效果的每1根带过滤嘴的香烟中的差压PD(mmH2O)。即,带过滤嘴的香烟1根的通气阻力为在以连接了烟杆部和过滤嘴部的制品的状态下测定的通气阻力。Here, the ventilation resistance of a single filter-tipped cigarette refers to the differential pressure PD (mmH 2 O) per filter-tipped cigarette, including the ventilation effect when inhaled from one end of the filter at a flow rate of 17.5 cm 3 /sec. In other words, the ventilation resistance of a single filter-tipped cigarette is the ventilation resistance measured with the cigarette body and filter connected.

本发明的低焦油薄荷醇香烟的焦油量为5mg以下。本发明中所说的焦油量是指在吸烟时吸烟者吸入的焦油量。The tar content of the low-tar menthol cigarette of the present invention is 5 mg or less. The tar content in the present invention refers to the amount of tar inhaled by the smoker when smoking.

为了使焦油量为5mg以下、即为了使目标焦油量为5mg以下,可以通过改变烟杆中所含的烟草烟丝的组成、或改变过滤嘴部的通气阻力、低焦油薄荷醇香烟的通气比例而进行调整。In order to make the tar amount below 5 mg, that is, to make the target tar amount below 5 mg, it can be adjusted by changing the composition of the tobacco shreds contained in the cigarette rod, or changing the ventilation resistance of the filter tip, and the ventilation ratio of the low-tar menthol cigarette.

作为5mg以下的焦油量的方式,可以在例如0.5~5mg的范围内适当调整。本发明的低焦油薄荷醇香烟即使为这种低焦油量的香烟,也可以给吸烟者以充分的薄荷醇香味感。As an embodiment of a tar amount of 5 mg or less, it can be appropriately adjusted within the range of 0.5 to 5 mg, for example. The low-tar menthol cigarette of the present invention can provide smokers with a sufficient menthol flavor even with such a low-tar cigarette.

带过滤嘴的香烟的焦油量根据ISO吸烟条件(ISO4387)将例如20根作为1个测定单元来进行测定。测定使用气相色谱法。The tar content of filter-tipped cigarettes is measured according to ISO smoking conditions (ISO 4387), using, for example, 20 cigarettes as one measurement unit. The measurement is performed using gas chromatography.

本发明的低焦油薄荷醇香烟的薄荷醇被添加于过滤嘴。过滤嘴中薄荷醇的添加场所,可以举出,例如添加于构成过滤嘴的醋酸纤维素丝束的10~100体积%部分的方式。作为其添加方法,可以举出,在制成带过滤嘴的香烟前预先添加于过滤嘴的醋酸纤维素丝束的方法,也可以举出在制成带过滤嘴的香烟后添加的方法。The menthol in the low-tar menthol cigarette of the present invention is added to the filter. Menthol can be added to the filter, for example, by adding it to 10 to 100% by volume of the cellulose acetate tow constituting the filter. Menthol can be added to the cellulose acetate tow in advance of manufacturing the filter-tipped cigarette, or after manufacturing the filter-tipped cigarette.

作为薄荷醇的添加方法,可以没有特别限制地使用公知的方法。薄荷醇可以为合成的薄荷醇,也可以为源自天然物的薄荷醇。As a method for adding menthol, a known method can be used without particular limitation. Menthol may be synthetic menthol or menthol derived from a natural product.

在本发明的低焦油薄荷醇香烟中,被添加于过滤嘴的薄荷醇的量优选为8mg/根以上。薄荷醇的添加量为8mg/根以上时,贮藏后的烟中薄荷醇量变得更稳定。贮藏后的烟中薄荷醇量变得更稳定是指:虽然经过贮藏时间,带过滤嘴的香烟在贮藏后,吸烟时薄荷醇从过滤嘴局部释放的量仍保持在接近于一定的量。过滤嘴部中薄荷醇的添加量更优选为10mg/根以上,特别优选为12mg/根以上。另一方面,作为薄荷醇量的上限,可以举出为20mg/根以下的方式。In the low-tar menthol cigarettes of the present invention, the amount of menthol added to the filter is preferably 8 mg/cigarette or more. When the amount of menthol added is 8 mg/cigarette or more, the amount of menthol in the cigarette after storage becomes more stable. The fact that the amount of menthol in the cigarette after storage becomes more stable means that, despite the storage period, the amount of menthol released from the filter portion of the cigarette after storage remains close to a certain amount when smoking. The amount of menthol added to the filter portion is more preferably 10 mg/cigarette or more, and particularly preferably 12 mg/cigarette or more. On the other hand, the upper limit of the amount of menthol can be 20 mg/cigarette or less.

本发明的低焦油薄荷醇香烟中可以使用的过滤嘴的轴向(纵向)长度可以使用例如15~35mm的长度。The filter that can be used in the low-tar menthol cigarette of the present invention can have an axial (vertical) length of, for example, 15 to 35 mm.

另外,关于本发明的低焦油薄荷醇香烟的圆周长度长度,可以举出20.0~27.0mm的方式,更优选可以举出24.0~26.0mm的方式。其为上述范围内时,有利于烟中高薄荷醇浓度的确保和贮藏后薄荷醇浓度的稳定保存。The circumferential length of the low-tar menthol cigarette of the present invention can be 20.0 to 27.0 mm, more preferably 24.0 to 26.0 mm. This range is advantageous for ensuring a high menthol concentration in the smoke and maintaining a stable menthol concentration after storage.

关于本发明的低焦油薄荷醇香烟的全长,可以举出80~100mm的方式。The total length of the low-tar menthol cigarette of the present invention may be 80 to 100 mm.

<低焦油薄荷醇香烟的制造方法><Method for producing low-tar menthol cigarettes>

本发明的低焦油薄荷醇香烟在过滤嘴中添加薄荷醇,使用给定范围的通气阻力作为过滤嘴的通气阻力,并且将空气流入的通气比例设定为给定范围,除此之外,可以使用公知的方法来制造。The low-tar menthol cigarette of the present invention can be manufactured using a known method except that menthol is added to the filter, the ventilation resistance of the filter is within a predetermined range, and the ventilation ratio of air inflow is set within a predetermined range.

在烟杆中设置节流孔那样的阻力体的情况下,也可以使用公知的方法。When a resistance body such as a throttle hole is provided in the cigarette rod, a known method can also be used.

作为构成本发明的低焦油薄荷醇香烟的烟杆部,可以举出,包含形成烟杆的烟草烟丝和卷装烟草烟丝的卷纸的方式,其材料或形状只要能实现本发明中给定的低焦油,就可以没有限定地使用公知的材料或形状。As the cigarette rod portion constituting the low-tar menthol cigarette of the present invention, there can be cited a method comprising tobacco shreds forming the cigarette rod and rolling paper for wrapping the tobacco shreds. As long as the material or shape can achieve the low tar given in the present invention, known materials or shapes can be used without limitation.

烟杆部的圆周长度可以举出上述中说明的与本发明低焦油薄荷醇香烟的圆周长度相同的范围。The circumferential length of the cigarette stem portion can be within the same range as that of the circumferential length of the low-tar menthol cigarette of the present invention as described above.

烟杆部的轴向长度可以举出例如50~75mm。The axial length of the cigarette rod portion can be, for example, 50 to 75 mm.

实施例Example

通过实施例更具体地说明本发明,但本发明只要不超过其要点,并不限定于以下的实施例的记载。The present invention will be described in more detail with reference to Examples. However, the present invention is not limited to the description of the following Examples unless the gist of the invention is exceeded.

<实施例1><Example 1>

实施例1、2及比较例1、2Examples 1, 2 and Comparative Examples 1, 2

为了验证设计为过滤嘴的通气阻力低、空气流入的通气比例高的香烟能够提高烟中薄荷醇量,制作具有表1所示的过滤嘴通气阻力及通气比例的香烟,对每1根香烟的烟中薄荷醇量及焦油量实施测定。此时,制作的过滤嘴在温度22℃湿度60%的条件下贮藏保管3周,使薄荷醇充分地吸附于醋酸纤维素丝束并使其稳定化后,用于香烟的烟卷。另外,将制作的香烟进行通常的铝包装后,在温度22℃、湿度60%的条件下贮藏保管3周,对烟中的薄荷醇量及焦油量进行测定。需要说明的是,表中的丝束规格表示单丝纤度、截面形状、总纤度,例如5.9Y35000是指单丝纤度为5.9旦尼尔、截面形状为Y型及总纤度为35000旦尼尔的醋酸纤维素丝束。To verify that cigarettes designed with filters featuring low airflow resistance and high airflow ratios can increase the amount of menthol in smoke, cigarettes with the filter airflow resistance and airflow ratio shown in Table 1 were produced, and the menthol and tar levels in the smoke of each cigarette were measured. The produced filters were stored at 22°C and 60% humidity for three weeks to allow the menthol to fully adsorb and stabilize on the cellulose acetate tow, before being used in cigarette rods. Separately, the produced cigarettes were packaged in standard aluminum packaging and stored at 22°C and 60% humidity for three weeks, and the menthol and tar levels in the smoke were measured. The tow specifications in the table indicate the single-filament fineness, cross-sectional shape, and total fineness. For example, 5.9Y35000 refers to a cellulose acetate tow with a single-filament fineness of 5.9 denier, a Y-shaped cross-sectional shape, and a total fineness of 35,000 denier.

用于试验的香烟的总长长度为84mm,过滤嘴长度为27mm。烟丝使用美国混合型,烟丝的填充量设为0.580g,相对于烟丝重量,加香12000ppm的薄荷醇。另外,各香烟以过滤嘴出口处的焦油量为5mg的方式设定过滤嘴的通气阻力及通气的比例。The cigarettes used in the tests were 84 mm in total length and 27 mm in filter length. The tobacco used was an American blend, with a filler weight of 0.580 g. Menthol was added at a concentration of 12,000 ppm per weight of the tobacco. The filter resistance and ventilation ratio of each cigarette were set to achieve a tar content of 5 mg at the filter outlet.

[表1][Table 1]

香烟的吸烟根据ISO吸烟条件而实施,关于薄荷醇测定,将20根作为1个测定单元的根数,重复测定2次,关于焦油测定,将20根作为1个测定单元的根数,实施1次测定。关于烟中薄荷醇量及焦油量,使用Agilent社制的GC-FID7693(薄荷醇测定、尼古丁测定)、Agilent社制的GC-TCD-7890A(水分测定),对每1根香烟的薄荷醇量及焦油量实施测定。关于通气比例,使用SODIM社制的SODIMAX测定从接装纸的开孔部流入的空气流入比例。Cigarette smoking was conducted according to ISO smoking conditions. Menthol was measured twice, with 20 cigarettes as one measurement unit. Tar was measured once, with 20 cigarettes as one measurement unit. Menthol and tar levels in smoke were measured per cigarette using an Agilent GC-FID7693 (menthol and nicotine) and an Agilent GC-TCD-7890A (moisture). Ventilation ratios were measured using a SODIMAX (SODIM) instrument.

另外,同时对制作的表1所示的4种香烟进行薄荷醇的感官评价。就评价方法而言,在4种香烟中,将条件最普通的组合的比较例1作为对照,询问对其它3种的薄荷醇感受是同等或高于对照,还是低于对照,二选一。在本评价时,对象人数为10人,利用累积二项分布概率(单侧)以显著水平5%进行显著性差别确认。In addition, sensory evaluations of menthol were conducted on the four cigarettes listed in Table 1. The evaluation method involved using Comparative Example 1, the most common combination of conditions, as a control. Participants were asked to choose whether their menthol perception for the other three cigarettes was equal to, greater than, or less than the control. Ten participants were evaluated, and significant differences were confirmed using a one-sided cumulative binomial probability distribution at a 5% significance level.

以下的表2中,除烟中薄荷醇量及焦油量之外,还示出了用薄荷醇量除以焦油量所得的值(以下,记载为M/T比),对于可得到同等焦油量时的薄荷醇量差异,可成为指标。一般而言,烟中薄荷醇量与焦油量成正比而升高,因此,在此使用以焦油量进行了规格化的值,由此比较薄荷醇量。另外,关于一并进行感官评价的结果,记载有无显著性差别。Table 2 below shows, in addition to the menthol and tar levels in the smoke, the value obtained by dividing the menthol level by the tar level (hereinafter referred to as the M/T ratio). This serves as an indicator of the difference in menthol levels when equivalent tar levels are achieved. Generally, the menthol level in smoke increases in direct proportion to the tar level, so the values normalized by the tar level are used here to compare menthol levels. The results of the sensory evaluation are also reported, indicating whether there were significant differences.

[表2][Table 2]

由表2可知:过滤嘴的通气阻力越低、空气流入的通气比例越高的香烟设计,烟中薄荷醇量及M/T比越成为高的值。认为这是因为,在过滤嘴的通气阻力和通气比例的关系中,焦油和薄荷醇的滤过率不同。具体而言,在使用低通气阻力的过滤嘴的情况下,除过滤嘴内部烟的物理过滤现象之外,凝缩/吸附于过滤嘴的丝束纤维的薄荷醇的量因丝束的总量少而被降低,烟中薄荷醇量及M/T比升高。此外,在为高通气比例的设计的情况下,过滤嘴内部烟的通过时间变长,一般而言,焦油和薄荷醇的滤过率升高,但丝束的总量少的低通气阻力的过滤嘴中,薄荷醇的滤过率不易升高,M/T比增加。结果,与焦油的滤过率相比,可以使薄荷醇的滤过率降低。在感官评价中,也可得到在薄荷醇感受方面存在差异的结果,确认到实施例1及2的薄荷醇感受显著高于比较例1。As shown in Table 2, the lower the filter's ventilation resistance and the higher the ventilation ratio of air flow into the cigarette design, the higher the menthol content and M/T ratio in the smoke. This is believed to be because the filtration rates of tar and menthol differ depending on the relationship between the filter's ventilation resistance and ventilation ratio. Specifically, when using a filter with low ventilation resistance, in addition to the physical filtration of smoke within the filter, the amount of menthol condensed/adsorbed on the filter's tow fibers is reduced due to the small total amount of tow, resulting in an increase in the menthol content and M/T ratio in the smoke. Furthermore, in designs with a high ventilation ratio, the time it takes for smoke to pass through the filter increases, generally increasing the filtration rates of tar and menthol. However, in low ventilation resistance filters with a small total amount of tow, the menthol filtration rate is less likely to increase, and the M/T ratio increases. As a result, the menthol filtration rate can be reduced compared to the tar filtration rate. In the sensory evaluation, a difference in menthol perception was also obtained, and it was confirmed that the menthol perception of Examples 1 and 2 was significantly higher than that of Comparative Example 1.

本实施例及相比于比较例更优选的范围设想为过滤嘴的通气阻力为80mmH2O/27mm以下、且通气比例为55%以上、优选为61%以上,进一步优选的范围设想为作为实施例1的条件的50mmH2O/27mm以下、且通气比例为70%以上。考虑到过滤嘴的实际制造工序,可制造的通气阻力的范围为25mmH2O/27mm以上为现实的范围。过滤嘴的原料的特征在于,由醋酸纤维素丝束构成。In this embodiment and the comparative example, a more preferable range is a filter airflow resistance of 80 mmH2O /27 mm or less and an airflow ratio of 55% or greater, preferably 61% or greater. A further preferable range is 50 mmH2O /27 mm or less and an airflow ratio of 70% or greater, as in Example 1. Considering the actual filter manufacturing process, a practical range of airflow resistance of 25 mmH2O /27 mm or greater is considered feasible. The filter material is characterized by being composed of cellulose acetate tow.

由以上证实:通过设计为空气流入的通气比例高的香烟,烟中薄荷醇量升高。在本实施例中,使用过滤嘴长度为27mm的香烟,但并不限于本形态,在任意的长度中,均可以期待同样的效果。另外,关于该香烟的圆周长度,本实施例中使用24.8mm的条件,但在接近于本实施例的圆周长度范围、具体而言20.0mm~27.0mm的范围内可以期待同样的效果,更优选为24.0mm~26.0mm的范围。The above demonstrates that cigarettes designed with a high ventilation ratio for air inflow increase the menthol content in the smoke. In this example, a cigarette with a filter length of 27 mm was used, but this is not limiting; similar effects can be expected with any filter length. Furthermore, while the circumferential length of the cigarette was 24.8 mm in this example, similar effects can be expected with a range close to the circumferential length of this example, specifically, 20.0 mm to 27.0 mm, with a range of 24.0 mm to 26.0 mm being more preferred.

<参考例1~4>Reference Examples 1 to 4

为了验证使用通气阻力低的过滤嘴能够使经薄荷醇加香的过滤嘴在贮藏时烟中薄荷醇量变得稳定,变更过滤嘴的贮藏期间及以香烟包装形态的贮藏期间,根据表3所示的过滤嘴的通气阻力及过滤嘴加香量,对伴有过滤嘴及香烟的贮藏期间的变更的烟中薄荷醇量实施试验。在此,为了除去其它因子的影响,不设置过滤嘴部的通气孔,仅变更过滤嘴的通气阻力,实施试验。To verify that using a filter with low airflow resistance stabilizes the menthol content in cigarette smoke during storage of a menthol-flavored filter, tests were conducted by varying the filter storage period and the storage period in the packaged cigarette form. The airflow resistance of the filter and the amount of filter flavoring shown in Table 3 were used to measure the menthol content in the cigarette smoke as the filter and cigarette storage periods varied. To eliminate the influence of other factors, the tests were conducted without providing ventilation holes in the filter and only varying the airflow resistance of the filter.

除过滤嘴的贮藏条件、通气阻力及通气比例以外,按照与前面的实施例1、2及比较例1、2同样的顺序实施试验。The test was conducted in the same procedure as in Examples 1 and 2 and Comparative Examples 1 and 2 above, except for the storage conditions, ventilation resistance, and ventilation ratio of the filter.

[表3][Table 3]

表4示出了过滤嘴及以香烟包装形态的贮藏期间的条件。作为最短期间的贮藏条件,可举出在制作过滤嘴之后马上用于香烟的制造、且不进行香烟包装形态的贮藏的条件(条件A),另一方面,可举出在最长期间的贮藏条件下,在过滤嘴制作后贮藏2个月,使用该过滤嘴制作香烟之后,进一步以包装形态贮藏该香烟2个月的条件(条件G)。对经过了条件A~G的各香烟实施对烟中薄荷醇量及焦油量的测定。Table 4 shows the storage conditions for the filter tips and their packaging. The shortest storage period involves using the filter tips immediately after manufacture in cigarette production and not storing them in cigarette packaging (Condition A). The longest storage period involves storing the filter tips for two months after manufacture, using them to manufacture cigarettes, and then storing the cigarettes in packaging for another two months (Condition G). Menthol and tar levels were measured for each cigarette that had been subjected to Conditions A through G.

[表4][Table 4]

表4Table 4

表5及图1示出试验的结果。表5所示的降低率为表示与没有实施过滤嘴贮藏及以香烟包装形态的贮藏的条件A的M/T比相比较时,各条件下的M/T比的降低率的值。图1示出了各条件下的M/T比的降低率。Table 5 and Figure 1 show the test results. The reduction rates shown in Table 5 represent the reduction rates of the M/T ratio under each condition, compared to the M/T ratio under Condition A, which involves storage without filters and in cigarette packaging. Figure 1 shows the reduction rates of the M/T ratio under each condition.

[表5][Table 5]

根据表5及图1可得到下述结果:过滤嘴的贮藏期间及以香烟的包装形态的贮藏期间越长,得到的薄荷醇量的值越小。另外,确认过滤嘴的通气阻力越大,M/T比的降低率越大,可知:参考例2~4与满足权利要求1的过滤嘴通气阻力的主要条件的参考例1相比,M/T比的降低率大。认为这是因为,低通气阻力的过滤嘴由于丝束重量低,因此,与高通气阻力的过滤嘴相比,可以降低薄荷醇对过滤嘴的吸附,每单位薄荷醇量的释放效率高。Table 5 and Figure 1 show the following results: the longer the filter storage period and the storage period in cigarette packaging, the lower the menthol content. Furthermore, it was confirmed that the greater the airflow resistance of the filter, the greater the rate of reduction in the M/T ratio. Reference Examples 2 to 4 showed a greater rate of reduction in the M/T ratio than Reference Example 1, which met the key requirements for airflow resistance of claim 1. This is believed to be because filters with low airflow resistance have a lower tow weight, thus reducing menthol adsorption to the filter compared to filters with high airflow resistance, resulting in a higher efficiency of menthol release per unit volume.

由以上的结果证实:通过使用过滤嘴的通气阻力低的过滤嘴,容易稳定地保持烟中的薄荷醇量。在将通气阻力低的过滤嘴与通气比例高的条件组合的情况下,也可以同样地得到该效果,可以制作烟中薄荷醇的量升高,且在贮藏后也容易稳定地保持薄荷醇的香烟。The above results demonstrate that using a filter with low airflow resistance facilitates stable menthol content in smoke. Combining a filter with low airflow resistance and a high airflow ratio also achieves the same effect, enabling the production of cigarettes that increase the menthol content in smoke and readily maintain menthol content even after storage.

<参考例5~8>Reference Examples 5 to 8

过滤嘴中的薄荷醇加香量设为每1根中所含有的量为8mg以上的情况下,为了验证烟中薄荷醇的量变得更稳定,将过滤嘴通气阻力设为恒定,实施变更了过滤嘴中的薄荷醇加香量及过滤嘴的贮藏期间的试验。表6示出了过滤嘴中的薄荷醇加香量。需要说明的是,在此也与参考例1~4同样地,为了除去其它影响因子的影响,在过滤嘴部不设置通气孔,仅变更过滤嘴的通气阻力,实施试验。To verify that the menthol content in the smoke is more stable when the menthol flavoring in the filter is set to 8 mg or more per cigarette, tests were conducted with varying filter airflow resistance and varying filter flavoring levels. Table 6 shows the menthol flavoring levels in the filter. As in Reference Examples 1 to 4, to eliminate the influence of other factors, the filter was tested without ventilation holes and only with varying filter airflow resistance.

[表6][Table 6]

过滤嘴的贮藏环境与参考例1~4同样地,在温度22℃、湿度60%下实施,关于过滤嘴的贮藏期间,在从不实施贮藏(标记为0)开始、至贮藏2周(标记为2W)、5周(标记为5W)、最长2个月(标记为2M)的条件下实施试验,根据过滤嘴中的薄荷醇加香量,通过以烟中薄荷醇量的形式被释放的比例以百分率表示的释放率进行比较。在此,由前面的参考例1~4预想到:不实施以香烟包装形态的贮藏,通过仅变更过滤嘴的贮藏期间,仅调查过滤嘴贮藏导致的影响,但通过进一步实施以香烟包装形态的贮藏,释放率进一步降低。因此,在此的试验不实施对烟杆部的烟丝的薄荷醇加香,仅由过滤嘴部释放薄荷醇。除烟丝/过滤嘴的薄荷醇加香量、通气比例及过滤嘴的贮藏期间以外,按照与前面的实施例1、2及比较例1、2同样的步骤实施试验。将试验结果示于表7及图2。The filter storage environment was similar to that of Reference Examples 1-4, at a temperature of 22°C and a humidity of 60%. The tests were conducted under varying storage conditions, starting with no storage (denoted as 0) and continuing through two weeks (denoted as 2W), five weeks (denoted as 5W), and finally two months (denoted as 2M). The release rate, expressed as a percentage of the amount of menthol released from the smoke, was compared based on the amount of menthol flavoring added to the filter. Based on the previous Reference Examples 1-4, it was expected that the effects of filter storage alone would be investigated by varying the filter storage period without storing the filter in cigarette packaging. However, further storage in cigarette packaging would further reduce the release rate. Therefore, in this test, menthol flavoring was not applied to the tobacco shreds in the cigarette stem, and menthol was released only from the filter. The tests were conducted according to the same procedures as in Examples 1 and 2 and Comparative Examples 1 and 2, with the exception of the amount of menthol flavoring added to the tobacco/filter, the ventilation ratio, and the filter storage period. The test results are shown in Table 7 and FIG2 .

[表7][Table 7]

由表7及图2可知:过滤嘴的薄荷醇加香量越多,伴有经时变化的释放率越稳定,与参考例5、6相比,可以说参考例7、8的经时变化耐性强。这是因为,通过大量添加薄荷醇使添加的薄荷醇量为被丝束吸附的量以上,可以缩小薄荷醇的吸附导致的影响。可以设想在使用通气阻力比参考例5~8更低的过滤嘴的情况下,由于被丝束吸附的薄荷醇量自身降低,因此该效果会更加明显。由以上的结果证实:过滤嘴中的薄荷醇加香量为每1根中所含有的量为8mg以上的情况下,烟中薄荷醇的量变得稳定。更优选的过滤嘴中的薄荷醇加香量为10mg以上,进一步优选为相当于参考例8的条件的12mg以上。As shown in Table 7 and Figure 2, the greater the amount of menthol flavoring added to the filter, the more stable the release rate over time. Compared to Reference Examples 5 and 6, Reference Examples 7 and 8 are more resistant to changes over time. This is because by adding a large amount of menthol, the amount of menthol added exceeds the amount adsorbed by the tow, minimizing the effects of menthol adsorption. It is conceivable that this effect is more pronounced when using filters with lower airflow resistance than Reference Examples 5-8, as the amount of menthol adsorbed by the tow itself is reduced. These results confirm that the amount of menthol in the smoke is stabilized when the amount of menthol flavoring in the filter is 8 mg or more per cigarette. A more preferred menthol flavoring amount in the filter is 10 mg or more, and even more preferably, 12 mg or more, equivalent to the conditions in Reference Example 8.

<实施例3及比较例3、4><Example 3 and Comparative Examples 3 and 4>

实施例1、2及比较例1、2为焦油量为5mg时的比较试验,为了验证本技术在以作为更低的焦油量的1mg为目标的情况下也是有效的,以表8所示的试验水准实施与实施例1、2及比较例1、2同样的试验。另外,同样地,一并进行感官评价。Examples 1 and 2 and Comparative Examples 1 and 2 were comparative tests performed at a tar content of 5 mg. To verify the effectiveness of this technology even when targeting a lower tar content of 1 mg, similar tests as those for Examples 1 and 2 and Comparative Examples 1 and 2 were conducted using the test levels shown in Table 8. Sensory evaluations were also performed in the same manner.

[表8][Table 8]

表9示出试验结果,除烟中薄荷醇量及焦油量之外,还示出M/T比。Table 9 shows the test results, which include the M/T ratio in addition to the menthol and tar amounts in the smoke.

[表9][Table 9]

由表9可知:实施例3的薄荷醇量最高,在以M/T比进行比较的情况下,也可得到最高的结果。关于感官评价对薄荷醇的感受评价,在实施例3中也可得到显著高的薄荷醇的感受,与前面实施的实施例1、2及比较例1、2的评价同样地,薄荷醇量的值大幅不同,因此,认为存在显著性差别。由以上确认:在焦油量非常低的范围内,本技术是有效的。As shown in Table 9, Example 3 has the highest menthol content, and also achieves the highest result when comparing the M/T ratio. Regarding the sensory evaluation of menthol perception, Example 3 also exhibits a significantly higher menthol perception. Similar to the evaluations of Examples 1 and 2 and Comparative Examples 1 and 2 conducted previously, the menthol content values differ significantly, indicating a significant difference. This confirms that the present technology is effective within the very low tar content range.

Claims (5)

1.一种低焦油薄荷醇香烟,其为具有烟杆部和用接装纸卷装成的过滤嘴部、且焦油量为5mg以下的低焦油薄荷醇香烟,其中,所述过滤嘴部包含由醋酸纤维素丝束构成的单一区段,所述过滤嘴部的通气阻力为25~50mmH2O/27mm,并且来自穿设于所述接装纸的通气孔的流入空气的通气比例为70%以上,通过吸附于所述过滤嘴部的醋酸纤维素丝束而添加薄荷醇。1. A low-tar menthol cigarette, comprising a stem portion and a filter portion rolled with tipping paper, and having a tar content of 5 mg or less, wherein the filter portion comprises a single section composed of cellulose acetate tow, the air resistance of the filter portion is 25-50 mmH₂O/27 mm, and the airflow ratio from the air holes passing through the tipping paper is 70% or more, and menthol is added by adsorbing the cellulose acetate tow of the filter portion. 2.如权利要求1所述的低焦油薄荷醇香烟,其中,每1根低焦油薄荷醇香烟的所述过滤嘴部中薄荷醇的添加量为8mg/根以上。2. The low-tar menthol cigarette as described in claim 1, wherein the amount of menthol added to the filter portion of each low-tar menthol cigarette is 8 mg or more per cigarette. 3.如权利要求1或2所述的低焦油薄荷醇香烟,其中,所述烟杆部或过滤嘴部具有阻力体。3. The low-tar menthol cigarette as described in claim 1 or 2, wherein the stem portion or filter portion has a resistance body. 4.如权利要求3所述的低焦油薄荷醇香烟,其中,所述阻力体为胶囊或节流孔。4. The low-tar menthol cigarette as described in claim 3, wherein the resistance body is a capsule or a throttling orifice. 5.如权利要求1或2所述的低焦油薄荷醇香烟,其中,所述低焦油薄荷醇香烟的圆周长度为20.0~27.0mm。5. The low-tar menthol cigarette as described in claim 1 or 2, wherein the circumference length of the low-tar menthol cigarette is 20.0 to 27.0 mm.
HK17103272.4A 2014-04-03 2015-03-26 Low tar menthol cigarette HK1229643B (en)

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