[go: up one dir, main page]

HK1208164A1 - Compositions comprising short-acting benzodiazepines - Google Patents

Compositions comprising short-acting benzodiazepines Download PDF

Info

Publication number
HK1208164A1
HK1208164A1 HK15108782.8A HK15108782A HK1208164A1 HK 1208164 A1 HK1208164 A1 HK 1208164A1 HK 15108782 A HK15108782 A HK 15108782A HK 1208164 A1 HK1208164 A1 HK 1208164A1
Authority
HK
Hong Kong
Prior art keywords
composition
dextran
lactose
lyophilized
benzodiazepine
Prior art date
Application number
HK15108782.8A
Other languages
German (de)
English (en)
Chinese (zh)
Other versions
HK1208164B (en
Inventor
John Aitken Graham
Alan James Baillie
Kevin Richard WARD
Thomas Peacock
Original Assignee
武汉人福创新药物研发中心有限公司
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=48669863&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=HK1208164(A1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by 武汉人福创新药物研发中心有限公司 filed Critical 武汉人福创新药物研发中心有限公司
Publication of HK1208164A1 publication Critical patent/HK1208164A1/en
Publication of HK1208164B publication Critical patent/HK1208164B/en

Links

Classifications

    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/33Heterocyclic compounds
    • A61K31/395Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
    • A61K31/55Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having seven-membered rings, e.g. azelastine, pentylenetetrazole
    • A61K31/551Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having seven-membered rings, e.g. azelastine, pentylenetetrazole having two nitrogen atoms, e.g. dilazep
    • A61K31/55131,4-Benzodiazepines, e.g. diazepam or clozapine
    • A61K31/55171,4-Benzodiazepines, e.g. diazepam or clozapine condensed with five-membered rings having nitrogen as a ring hetero atom, e.g. imidazobenzodiazepines, triazolam
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K31/00Medicinal preparations containing organic active ingredients
    • A61K31/33Heterocyclic compounds
    • A61K31/395Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins
    • A61K31/55Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having seven-membered rings, e.g. azelastine, pentylenetetrazole
    • A61K31/551Heterocyclic compounds having nitrogen as a ring hetero atom, e.g. guanethidine or rifamycins having seven-membered rings, e.g. azelastine, pentylenetetrazole having two nitrogen atoms, e.g. dilazep
    • A61K31/55131,4-Benzodiazepines, e.g. diazepam or clozapine
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/06Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
    • A61K47/26Carbohydrates, e.g. sugar alcohols, amino sugars, nucleic acids, mono-, di- or oligo-saccharides; Derivatives thereof, e.g. polysorbates, sorbitan fatty acid esters or glycyrrhizin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/14Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles
    • A61K9/19Particulate form, e.g. powders, Processes for size reducing of pure drugs or the resulting products, Pure drug nanoparticles lyophilised, i.e. freeze-dried, solutions or dispersions
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P21/00Drugs for disorders of the muscular or neuromuscular system
    • A61P21/02Muscle relaxants, e.g. for tetanus or cramps
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P23/00Anaesthetics
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P25/00Drugs for disorders of the nervous system
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P25/00Drugs for disorders of the nervous system
    • A61P25/08Antiepileptics; Anticonvulsants
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P25/00Drugs for disorders of the nervous system
    • A61P25/20Hypnotics; Sedatives
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61PSPECIFIC THERAPEUTIC ACTIVITY OF CHEMICAL COMPOUNDS OR MEDICINAL PREPARATIONS
    • A61P25/00Drugs for disorders of the nervous system
    • A61P25/22Anxiolytics
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D243/00Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms
    • C07D243/06Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4
    • C07D243/10Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4 condensed with carbocyclic rings or ring systems
    • C07D243/141,4-Benzodiazepines; Hydrogenated 1,4-benzodiazepines
    • C07D243/161,4-Benzodiazepines; Hydrogenated 1,4-benzodiazepines substituted in position 5 by aryl radicals
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D243/00Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms
    • C07D243/06Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4
    • C07D243/10Heterocyclic compounds containing seven-membered rings having two nitrogen atoms as the only ring hetero atoms having the nitrogen atoms in positions 1 and 4 condensed with carbocyclic rings or ring systems
    • C07D243/141,4-Benzodiazepines; Hydrogenated 1,4-benzodiazepines
    • C07D243/161,4-Benzodiazepines; Hydrogenated 1,4-benzodiazepines substituted in position 5 by aryl radicals
    • C07D243/181,4-Benzodiazepines; Hydrogenated 1,4-benzodiazepines substituted in position 5 by aryl radicals substituted in position 2 by nitrogen, oxygen or sulfur atoms
    • C07D243/24Oxygen atoms
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D401/00Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/04Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings directly linked by a ring-member-to-ring-member bond
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/06Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite
    • A61K47/08Organic compounds, e.g. natural or synthetic hydrocarbons, polyolefins, mineral oil, petrolatum or ozokerite containing oxygen, e.g. ethers, acetals, ketones, quinones, aldehydes, peroxides
    • A61K47/12Carboxylic acids; Salts or anhydrides thereof
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K47/00Medicinal preparations characterised by the non-active ingredients used, e.g. carriers or inert additives; Targeting or modifying agents chemically bound to the active ingredient
    • A61K47/30Macromolecular organic or inorganic compounds, e.g. inorganic polyphosphates
    • A61K47/36Polysaccharides; Derivatives thereof, e.g. gums, starch, alginate, dextrin, hyaluronic acid, chitosan, inulin, agar or pectin
    • A61K47/40Cyclodextrins; Derivatives thereof

Landscapes

  • Health & Medical Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pharmacology & Pharmacy (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Medicinal Chemistry (AREA)
  • Epidemiology (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Bioinformatics & Cheminformatics (AREA)
  • Nuclear Medicine, Radiotherapy & Molecular Imaging (AREA)
  • Neurology (AREA)
  • Neurosurgery (AREA)
  • Biomedical Technology (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Biochemistry (AREA)
  • Molecular Biology (AREA)
  • Pain & Pain Management (AREA)
  • Anesthesiology (AREA)
  • Orthopedic Medicine & Surgery (AREA)
  • Physical Education & Sports Medicine (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Medicinal Preparation (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)
  • Plural Heterocyclic Compounds (AREA)

Claims (12)

  1. Composition lyophilisée ou séchée par atomisation comprenant au moins une benzodiazépine répondant à la formule (I) où
    W représente H ;
    X représente CH2; n est égal à 1 ;
    Y représente CH2; m est égal à 1 ;
    Z représente 0 ;
    R1 représente CH3, CH2CH3, CH2CH2CH3, CH(CH3)2 ou CH2CH(CH3)2 ;
    R2 représente un groupement 2-fluorophényle, 2-chlorophényle ou 2-pyridyle ;
    R3 représente Cl ou Br ;
    R4, R5 et R6 forment le groupement -CR8=U-V= où R6 représente un atome d'hydrogène ou un groupement alkyle en C1-4 ou hydroxyalkyle en C1-3, U représente N ou CR9 où R9 représente H ou un groupement alkyle en C1-4, hydroxyalkyle en C1-3 ou alkoxy en C1-4, V représente N ou CH et p est égal à zéro ou sel pharmaceutiquement acceptable de celui-ci, où la composition comprend au moins un excipient hygroscopique pharmaceutiquement acceptable, où l'excipient hygroscopique est un hydrate de carbone choisi dans le groupe constitué par les disaccharides et le dextrane, et éventuellement, la composition est au moins en partie amorphe.
  2. Composition selon la revendication 1, où la benzodiazépine répondant à la formule (I) est le 3-[(4S)-8-bromo-1-méthyl-6-(pyridin-2-yl)-4H-imidazo[1,2-a][1,4]benzodiazépin-4-yl]propanoate de méthyle (rémimazolam).
  3. Composition selon la revendication 2, où le sel pharmaceutiquement acceptable de la benzodiazépine est formulé sous forme cationique et le contre-ion est le benzènesulfonate (bésylate).
  4. Composition selon l'une quelconque des revendications 1 à 3, où le dextrane présente une masse moléculaire de moins de 150 kD.
  5. Composition selon l'une quelconque des revendications 1 à 3, où le disaccharide est choisi dans le groupe constitué par le lactose, le maltose, le sucrose et le tréhalose.
  6. Composition selon l'une quelconque des revendications 1 à 3, où la composition comprend un mélange d'un premier excipient hygroscopique et d'un second excipient hygroscopique.
  7. Composition selon la revendication 6, où la composition comprend un mélange d'un disaccharide et de dextrane, préférentiellement d'un mélange de lactose et de dextrane.
  8. Composition selon la revendication 7, où le rapport massique en % entre le lactose et le dextrane est compris entre 1:1,0 et 1:10, préférentiellement entre 1:1,2 et 1:5, et plus préférentiellement est de 1:1,5 ou de 1:4.
  9. Composition selon l'une quelconque des revendications 1 à 3, où le rapport massique en % entre la quantité totale d'excipients hygroscopiques et la quantité totale de benzodiazépines ou de sels de celui-ci, calculée pour la base, dans la composition, est compris entre 20:1 et 1:1, préférentiellement entre 12:1 et 3:1, le plus préférentiellement entre 9:1 et 3:1.
  10. Composition selon l'une quelconque des revendications 1 à 3, qui est une formule pharmaceutique.
  11. Utilisation d'un mélange d'au moins un disaccharide et d'au moins un dextrane pour la préparation d'une composition pharmaceutique lyophilisée ou séchée par atomisation comprenant une benzodiazépine avec une entité ester d'acide carboxylique selon la revendication 1 ou un sel pharmaceutiquement acceptable de celle-ci, en particulier le rémimazolam.
  12. Procédé d'élaboration d'une composition pharmaceutique comprenant les étapes suivantes :
    a) obtention d'une solution comprenant une benzodiazépine selon la revendication 1 ou un sel pharmaceutiquement acceptable de celle-ci, en particulier le rémimazolam ;
    b) ajout d'au moins un excipient hygroscopique, qui est un hydrate de carbone choisi dans le groupe constitué par les disaccharides et le dextrane ou un mélange de ceux-ci avec au moins un autre excipient hygroscopique ;
    c) séchage de la solution de l'étape b) par lyophilisation ou séchage par atomisation.
HK15108782.8A 2012-05-22 2013-05-22 Compositions comprising short-acting benzodiazepines HK1208164B (en)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP12168968 2012-05-22
EP12168968.1 2012-05-22
PCT/EP2013/060543 WO2013174883A1 (fr) 2012-05-22 2013-05-22 Compositions comprenant des benzodiazépines à action rapide

Publications (2)

Publication Number Publication Date
HK1208164A1 true HK1208164A1 (en) 2016-02-26
HK1208164B HK1208164B (en) 2018-06-29

Family

ID=

Also Published As

Publication number Publication date
US20220040198A1 (en) 2022-02-10
LTC2852389I2 (fr) 2024-11-25
NO2852389T3 (fr) 2018-03-17
PE20150683A1 (es) 2015-06-03
AU2013265295B2 (en) 2017-08-31
NL301130I1 (fr) 2021-09-22
UA115063C2 (uk) 2017-09-11
MA37581B1 (fr) 2016-07-29
IL235789B (en) 2019-07-31
DK2852389T3 (en) 2017-12-18
TW201400119A (zh) 2014-01-01
NO2021041I1 (no) 2021-09-20
LUC00230I2 (fr) 2022-10-07
EP2852389A1 (fr) 2015-04-01
TWI590826B (zh) 2017-07-11
ECSP14032553A (es) 2018-11-30
PT2852389T (pt) 2017-12-13
KR102116737B1 (ko) 2020-05-29
EA032119B1 (ru) 2019-04-30
PH12014502608A1 (en) 2015-01-21
FR21C1043I2 (fr) 2022-10-07
PL2852389T4 (pl) 2022-02-21
WO2013174883A1 (fr) 2013-11-28
MX2014014225A (es) 2015-06-17
MY185117A (en) 2021-04-30
MA20150233A1 (fr) 2015-07-31
RS56660B1 (sr) 2018-03-30
KR20150009601A (ko) 2015-01-26
EA201492160A1 (ru) 2015-10-30
HUS2100040I1 (hu) 2021-10-28
CA2874247C (fr) 2020-07-28
CL2014003171A1 (es) 2015-06-19
LT2852389T (lt) 2017-12-27
PH12014502608B1 (en) 2019-11-27
US20150148338A1 (en) 2015-05-28
CO7151503A2 (es) 2014-12-29
SG11201407710VA (en) 2015-01-29
CN104968348A (zh) 2015-10-07
HRP20171872T1 (hr) 2018-02-23
TN2014000479A1 (en) 2016-03-30
GEP20186852B (en) 2018-05-25
EP2852389B1 (fr) 2017-10-18
GEAP201813666A (en) 2018-01-25
FR21C1043I1 (fr) 2021-11-19
NL301130I2 (nl) 2021-10-25
JP2015517552A (ja) 2015-06-22
CN108578413A (zh) 2018-09-28
PL2852389T3 (pl) 2018-02-28
BR112014029108A2 (pt) 2017-06-27
NZ702063A (en) 2016-11-25
LTPA2021521I1 (fr) 2021-10-11
CA2874247A1 (fr) 2013-11-28
HUE037734T2 (hu) 2018-09-28
CN104968348B (zh) 2018-04-17
ZA201408412B (en) 2016-09-28
AR092008A1 (es) 2015-03-18
IL235789A0 (en) 2015-01-29
ES2651389T3 (es) 2018-01-26
AP2014008084A0 (en) 2014-11-30
JP6313286B2 (ja) 2018-04-18
AU2013265295A1 (en) 2015-01-22
BR112014029108B1 (pt) 2022-02-08
MX368854B (es) 2019-10-18
SI2852389T1 (en) 2018-02-28

Similar Documents

Publication Publication Date Title
EP2852389B1 (fr) Compositions comprenant des benzodiazépines à action brève
JP5380549B2 (ja) ボリコナゾール含有の薬物製剤及びその調製方法
Abed et al. Formulation and optimization of orodispersible tablets of diazepam
TW200944508A (en) Novel solid forms of bendamustine hydrochloride
ES2573982T3 (es) Proceso para la producción de coevaporados y complejos que comprenden voriconazol y ciclodextrina
EP2811984A1 (fr) Procédé pour préparer des compositions pharmaceutiques stables de composés sensibles à l'hydrolyse
BR112012009660B1 (pt) lipossoma tendo fase de água interna contendo sal de ciclodextrina de éter sulfobutílico, seu processo de preparação, seu uso e preparação farmacêutica lipossômica
TW201930285A (zh) 共晶體、其藥物組合物以及涉及其的治療方法
HK1208164B (en) Compositions comprising short-acting benzodiazepines
EP1945182B1 (fr) Préparation de tipifarnib pour l'application intraveineuse
CN108289897B (zh) 一种瑞马唑仑的药物组合物
JP2019512538A (ja) オリタバンシン製剤
CN112175029A (zh) 抗真菌的大环多烯类新化合物
US9308174B2 (en) Lyophilized formulations of bendamustine hydrochloride
OA20108A (en) Compositions Comprising Short-Acting Benzodiazepines.
Almarsson et al. Solid-state chemistry of a novel carbapenem with a releasable sidechain
Cutrignelli et al. Dasatinib/HP-ẞ-CD Inclusion Complex Based Aqueous Formulation as a Promising Tool for the
CN111100122A (zh) 左旋四氢帕马丁新化合物
HK40116191A (en) Platform drug delivery system utilizing crystal engineering and theanine dissolution
BR112015005489B1 (pt) Composição farmacêutica para administração oral com dissolução e/ou absorção aperfeiçoadas
EP2976067A1 (fr) Composition pharmaceutique comprenant un agent antibactérien de fluoroquinolone et son procédé de préparation