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GB938824A - Preparation of vinyl chloride - Google Patents

Preparation of vinyl chloride

Info

Publication number
GB938824A
GB938824A GB33017/61A GB3301761A GB938824A GB 938824 A GB938824 A GB 938824A GB 33017/61 A GB33017/61 A GB 33017/61A GB 3301761 A GB3301761 A GB 3301761A GB 938824 A GB938824 A GB 938824A
Authority
GB
United Kingdom
Prior art keywords
tower
vinyl chloride
quench
leave
dew point
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB33017/61A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Goodrich Corp
Original Assignee
BF Goodrich Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BF Goodrich Corp filed Critical BF Goodrich Corp
Publication of GB938824A publication Critical patent/GB938824A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2415—Tubular reactors
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J12/00—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor
    • B01J12/005—Chemical processes in general for reacting gaseous media with gaseous media; Apparatus specially adapted therefor carried out at high temperatures, e.g. by pyrolysis
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C17/00—Preparation of halogenated hydrocarbons
    • C07C17/25—Preparation of halogenated hydrocarbons by splitting-off hydrogen halides from halogenated hydrocarbons
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00058—Temperature measurement
    • B01J2219/00063—Temperature measurement of the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00054—Controlling or regulating the heat exchange system
    • B01J2219/00056—Controlling or regulating the heat exchange system involving measured parameters
    • B01J2219/00067—Liquid level measurement
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
    • B01J2219/00103—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor in a heat exchanger separate from the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00157—Controlling the temperature by means of a burner
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C21/00—Acyclic unsaturated compounds containing halogen atoms
    • C07C21/02—Acyclic unsaturated compounds containing halogen atoms containing carbon-to-carbon double bonds
    • C07C21/04—Chloro-alkenes
    • C07C21/06—Vinyl chloride

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Vinyl chloride is prepared by passing 1,2-ethylene dichloride through a tube of internal diameter 2.42 to 8.5 cm. at 20-38 atmos. pressure and 900-1000 DEG F., condensing the products and distilling the vinyl chloride from the condensate. The pyrolysis tube is preferably centrally located along the longitudinal plane of a box type radiant furnace with side burners (see Group XII) and the gaseous products are preferably passed into a quench tower with means for removing superheat only to ensure that they leave said tower at their dew point, measurement of which gives the degree of conversion of the ethylene dichloride. The gases may be made to leave the quench tower at their dew point by arranging for any change in level of liquid at the base of the tower to alter the temperature of the quench liquid entering the tower by adjusting the proportion of the circulating liquid passing through a heat exchanger (see Group XIII).
GB33017/61A 1960-11-10 1961-09-14 Preparation of vinyl chloride Expired GB938824A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US6853860A 1960-11-10 1960-11-10

Publications (1)

Publication Number Publication Date
GB938824A true GB938824A (en) 1963-10-09

Family

ID=22083204

Family Applications (1)

Application Number Title Priority Date Filing Date
GB33017/61A Expired GB938824A (en) 1960-11-10 1961-09-14 Preparation of vinyl chloride

Country Status (6)

Country Link
BE (1) BE610112A (en)
DE (1) DE1213838B (en)
FR (1) FR1302458A (en)
GB (1) GB938824A (en)
NL (1) NL132330C (en)
SE (1) SE218376C1 (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3468967A (en) * 1964-04-27 1969-09-23 Ethyl Corp Production and purification of vinyl chloride
US3476955A (en) * 1965-09-11 1969-11-04 Knapsack Ag Process for the manufacture of vinyl chloride from contaminated 1,2-dichloroethane
DE2313037A1 (en) * 1973-03-16 1974-09-19 Knapsack Ag PROCESS FOR THE PRODUCTION OF VINYL CHLORIDE BY THERMAL CLEAVAGE OF 1,2-DICHLORAETHANE
JPS5024935B1 (en) * 1965-09-20 1975-08-20
US4225520A (en) * 1974-04-06 1980-09-30 Hoechst Aktiengesellschaft Process for the manufacture of vinyl chloride
WO2003093206A1 (en) * 2002-05-02 2003-11-13 Uhde Gmbh Method for the production of unsaturated hydrocarbons containing halogen and suitable device therefor

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL82990C (en) * 1950-12-27

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3468967A (en) * 1964-04-27 1969-09-23 Ethyl Corp Production and purification of vinyl chloride
US3476955A (en) * 1965-09-11 1969-11-04 Knapsack Ag Process for the manufacture of vinyl chloride from contaminated 1,2-dichloroethane
JPS5024935B1 (en) * 1965-09-20 1975-08-20
DE2313037A1 (en) * 1973-03-16 1974-09-19 Knapsack Ag PROCESS FOR THE PRODUCTION OF VINYL CHLORIDE BY THERMAL CLEAVAGE OF 1,2-DICHLORAETHANE
US4225520A (en) * 1974-04-06 1980-09-30 Hoechst Aktiengesellschaft Process for the manufacture of vinyl chloride
WO2003093206A1 (en) * 2002-05-02 2003-11-13 Uhde Gmbh Method for the production of unsaturated hydrocarbons containing halogen and suitable device therefor

Also Published As

Publication number Publication date
FR1302458A (en) 1962-08-31
DE1213838B (en) 1966-04-07
SE218376C1 (en) 1968-01-23
NL271082A (en) 1964-07-27
NL132330C (en) 1971-08-17
BE610112A (en) 1962-03-01

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