GB918168A - Improvements in feed supplements - Google Patents
Improvements in feed supplementsInfo
- Publication number
- GB918168A GB918168A GB16626/60A GB1662660A GB918168A GB 918168 A GB918168 A GB 918168A GB 16626/60 A GB16626/60 A GB 16626/60A GB 1662660 A GB1662660 A GB 1662660A GB 918168 A GB918168 A GB 918168A
- Authority
- GB
- United Kingdom
- Prior art keywords
- vitamin
- fat
- proteinaceous
- oil
- encased
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000006052 feed supplement Substances 0.000 title 1
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 abstract 9
- GVJHHUAWPYXKBD-UHFFFAOYSA-N (±)-α-Tocopherol Chemical compound OC1=C(C)C(C)=C2OC(CCCC(C)CCCC(C)CCCC(C)C)(C)CCC2=C1C GVJHHUAWPYXKBD-UHFFFAOYSA-N 0.000 abstract 4
- 239000011324 bead Substances 0.000 abstract 4
- 235000019197 fats Nutrition 0.000 abstract 4
- 239000000463 material Substances 0.000 abstract 4
- 239000000203 mixture Substances 0.000 abstract 4
- 235000020183 skimmed milk Nutrition 0.000 abstract 4
- 235000010469 Glycine max Nutrition 0.000 abstract 3
- QYSXJUFSXHHAJI-XFEUOLMDSA-N Vitamin D3 Natural products C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C/C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-XFEUOLMDSA-N 0.000 abstract 3
- 235000013312 flour Nutrition 0.000 abstract 3
- 239000000843 powder Substances 0.000 abstract 3
- 229940088594 vitamin Drugs 0.000 abstract 3
- 229930003231 vitamin Natural products 0.000 abstract 3
- 235000013343 vitamin Nutrition 0.000 abstract 3
- 239000011782 vitamin Substances 0.000 abstract 3
- QYSXJUFSXHHAJI-YRZJJWOYSA-N vitamin D3 Chemical compound C1(/[C@@H]2CC[C@@H]([C@]2(CCC1)C)[C@H](C)CCCC(C)C)=C\C=C1\C[C@@H](O)CCC1=C QYSXJUFSXHHAJI-YRZJJWOYSA-N 0.000 abstract 3
- 235000005282 vitamin D3 Nutrition 0.000 abstract 3
- 239000011647 vitamin D3 Substances 0.000 abstract 3
- 229940021056 vitamin d3 Drugs 0.000 abstract 3
- 150000003722 vitamin derivatives Chemical class 0.000 abstract 3
- 239000004255 Butylated hydroxyanisole Substances 0.000 abstract 2
- VYGQUTWHTHXGQB-FFHKNEKCSA-N Retinol Palmitate Chemical compound CCCCCCCCCCCCCCCC(=O)OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C VYGQUTWHTHXGQB-FFHKNEKCSA-N 0.000 abstract 2
- 229930003427 Vitamin E Natural products 0.000 abstract 2
- 229930003448 Vitamin K Natural products 0.000 abstract 2
- 229940043253 butylated hydroxyanisole Drugs 0.000 abstract 2
- 235000019282 butylated hydroxyanisole Nutrition 0.000 abstract 2
- CZBZUDVBLSSABA-UHFFFAOYSA-N butylated hydroxyanisole Chemical compound COC1=CC=C(O)C(C(C)(C)C)=C1.COC1=CC=C(O)C=C1C(C)(C)C CZBZUDVBLSSABA-UHFFFAOYSA-N 0.000 abstract 2
- 239000002285 corn oil Substances 0.000 abstract 2
- 235000005687 corn oil Nutrition 0.000 abstract 2
- 235000012343 cottonseed oil Nutrition 0.000 abstract 2
- 239000002385 cottonseed oil Substances 0.000 abstract 2
- 230000036425 denaturation Effects 0.000 abstract 2
- 238000004925 denaturation Methods 0.000 abstract 2
- 239000000839 emulsion Substances 0.000 abstract 2
- WIGCFUFOHFEKBI-UHFFFAOYSA-N gamma-tocopherol Natural products CC(C)CCCC(C)CCCC(C)CCCC1CCC2C(C)C(O)C(C)C(C)C2O1 WIGCFUFOHFEKBI-UHFFFAOYSA-N 0.000 abstract 2
- 238000010438 heat treatment Methods 0.000 abstract 2
- 238000002844 melting Methods 0.000 abstract 2
- 230000008018 melting Effects 0.000 abstract 2
- SHUZOJHMOBOZST-UHFFFAOYSA-N phylloquinone Natural products CC(C)CCCCC(C)CCC(C)CCCC(=CCC1=C(C)C(=O)c2ccccc2C1=O)C SHUZOJHMOBOZST-UHFFFAOYSA-N 0.000 abstract 2
- 235000019165 vitamin E Nutrition 0.000 abstract 2
- 239000011709 vitamin E Substances 0.000 abstract 2
- 229940046009 vitamin E Drugs 0.000 abstract 2
- 235000019168 vitamin K Nutrition 0.000 abstract 2
- 239000011712 vitamin K Substances 0.000 abstract 2
- 150000003721 vitamin K derivatives Chemical class 0.000 abstract 2
- 229940046010 vitamin k Drugs 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- FPIPGXGPPPQFEQ-UHFFFAOYSA-N 13-cis retinol Natural products OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-UHFFFAOYSA-N 0.000 abstract 1
- 241000251468 Actinopterygii Species 0.000 abstract 1
- 108010068370 Glutens Proteins 0.000 abstract 1
- 244000068988 Glycine max Species 0.000 abstract 1
- VYGQUTWHTHXGQB-UHFFFAOYSA-N Retinol hexadecanoate Natural products CCCCCCCCCCCCCCCC(=O)OCC=C(C)C=CC=C(C)C=CC1=C(C)CCCC1(C)C VYGQUTWHTHXGQB-UHFFFAOYSA-N 0.000 abstract 1
- 241000209140 Triticum Species 0.000 abstract 1
- 235000021307 Triticum Nutrition 0.000 abstract 1
- FPIPGXGPPPQFEQ-BOOMUCAASA-N Vitamin A Natural products OC/C=C(/C)\C=C\C=C(\C)/C=C/C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-BOOMUCAASA-N 0.000 abstract 1
- FPIPGXGPPPQFEQ-OVSJKPMPSA-N all-trans-retinol Chemical compound OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C FPIPGXGPPPQFEQ-OVSJKPMPSA-N 0.000 abstract 1
- 239000003963 antioxidant agent Substances 0.000 abstract 1
- 230000003078 antioxidant effect Effects 0.000 abstract 1
- 235000006708 antioxidants Nutrition 0.000 abstract 1
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000010480 babassu oil Substances 0.000 abstract 1
- 239000003240 coconut oil Substances 0.000 abstract 1
- 235000019864 coconut oil Nutrition 0.000 abstract 1
- 239000012141 concentrate Substances 0.000 abstract 1
- 230000000694 effects Effects 0.000 abstract 1
- 235000021312 gluten Nutrition 0.000 abstract 1
- 239000008173 hydrogenated soybean oil Substances 0.000 abstract 1
- 210000004185 liver Anatomy 0.000 abstract 1
- 239000003921 oil Substances 0.000 abstract 1
- 235000019198 oils Nutrition 0.000 abstract 1
- 150000008442 polyphenolic compounds Chemical class 0.000 abstract 1
- 235000013824 polyphenols Nutrition 0.000 abstract 1
- 235000008476 powdered milk Nutrition 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 229960000342 retinol acetate Drugs 0.000 abstract 1
- 235000019173 retinyl acetate Nutrition 0.000 abstract 1
- 239000011770 retinyl acetate Substances 0.000 abstract 1
- QGNJRVVDBSJHIZ-QHLGVNSISA-N retinyl acetate Chemical compound CC(=O)OC\C=C(/C)\C=C\C=C(/C)\C=C\C1=C(C)CCCC1(C)C QGNJRVVDBSJHIZ-QHLGVNSISA-N 0.000 abstract 1
- 229940108325 retinyl palmitate Drugs 0.000 abstract 1
- 235000019172 retinyl palmitate Nutrition 0.000 abstract 1
- 239000011769 retinyl palmitate Substances 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 238000001694 spray drying Methods 0.000 abstract 1
- 235000019155 vitamin A Nutrition 0.000 abstract 1
- 239000011719 vitamin A Substances 0.000 abstract 1
- 235000019156 vitamin B Nutrition 0.000 abstract 1
- 239000011720 vitamin B Substances 0.000 abstract 1
- 229940045997 vitamin a Drugs 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/59—Compounds containing 9, 10- seco- cyclopenta[a]hydrophenanthrene ring systems
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/158—Fatty acids; Fats; Products containing oils or fats
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K20/00—Accessory food factors for animal feeding-stuffs
- A23K20/10—Organic substances
- A23K20/174—Vitamins
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23K—FODDER
- A23K40/00—Shaping or working-up of animal feeding-stuffs
- A23K40/30—Shaping or working-up of animal feeding-stuffs by encapsulating; by coating
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K9/00—Medicinal preparations characterised by special physical form
- A61K9/48—Preparations in capsules, e.g. of gelatin, of chocolate
- A61K9/50—Microcapsules having a gas, liquid or semi-solid filling; Solid microparticles or pellets surrounded by a distinct coating layer, e.g. coated microspheres, coated drug crystals
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Polymers & Plastics (AREA)
- Engineering & Computer Science (AREA)
- Zoology (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Animal Husbandry (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Feed For Specific Animals (AREA)
- Fodder In General (AREA)
Abstract
Dry, discrete beads containing stabilized fat-soluble vitamin comprising a fat core containing at least one fat-soluble vitamin encased within a heat-denatured, water-resistant, proteinaceous digestible shell are made by mixing a solution of the fat-soluble vitamin in molten fat having a melting point of at least 35 DEG C with an aqueous solution of a heatcoagulable, proteinaceous material consisting of one or more of the following viz., soy flour, wheat gluten, skim milk powder and skim milk, heating the mixture to effect incipient denaturation, homogenising the mixture to form an emulsion with the fat as the finely dispersed internal phase, and spray-drying the heated emulsion to complete the denaturation. Under preferred conditions, the mixing is effected at a temperature of about 10 DEG C above the melting point of the fat; the mixture contains citric acid, has a pH of 6,0-6,3 and a total solids content of 30-40%; and the heating of the mixture is to a temperature of 65-85 DEG C for about 10-30 minutes. The beads may include any antioxidant material customarily used for vitaminized feeds other than polyphenols. It is stated that proteinaceous material that has already been denatured by heat-processing, so that the material is no longer soluble in water, cannot be used in making the beads. Examples describe in detail the preparation of beads containing: (1) a hydrogenated coconut oil core containing crystalline Vitamin D3, Vitamin A palmitate in corn oil and butylated hydroxyanisole encased with a proteinaceous shell derived from solvent-extracted non-heat-processed soy flour and containing citric acid, (2) a hydrogenated soybean oil core containing Vitamin D3 in corn oil, Vitamin A in fish liver oil, Vitamin E in cottonseed oil and Vitamin K encased within a proteinaceous shell derived from skim milk powder, and (3) a hydrogenated babassu oil core containing crystalline Vitamin D3, Vitamin A acetate concentrate, Vitamin E in cottonseed oil, crystalline Vitamin K, and butylated hydroxyanisole encased within a proteinaceous shell derived from solvent-extracted non-heat-processed soybean flour and skim milk powder, and including also citric acid and specified B vitamins.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB16626/60A GB918168A (en) | 1960-05-11 | 1960-05-11 | Improvements in feed supplements |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB16626/60A GB918168A (en) | 1960-05-11 | 1960-05-11 | Improvements in feed supplements |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB918168A true GB918168A (en) | 1963-02-13 |
Family
ID=10080712
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB16626/60A Expired GB918168A (en) | 1960-05-11 | 1960-05-11 | Improvements in feed supplements |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB918168A (en) |
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0357169A1 (en) * | 1988-08-30 | 1990-03-07 | Asama Chemical Co., Ltd. | Stabilized vitamin powder |
| US5756719A (en) * | 1996-09-03 | 1998-05-26 | Basf Corporation | Double emulsion techniques for making novel compositions containing gluten and polysaccharides that contain uronic acid residues useful for encapsulating fats, oils and solids |
| US5767107A (en) * | 1996-09-03 | 1998-06-16 | Basf Corporation | Compositions containing gluten and polysaccharides that contain uronic acid residues useful for encapsulating fats, oils and solids |
| WO2008072270A3 (en) * | 2006-12-11 | 2008-08-21 | John S Chen | Method for producing a proteic net able to trap nutrients and/or pharmacologically active substances |
| US9084944B2 (en) | 2010-09-03 | 2015-07-21 | Bend Research, Inc. | Spray-drying apparatus and methods of using the same |
| US9084976B2 (en) | 2010-09-03 | 2015-07-21 | Bend Research, Inc. | Spray-drying apparatus and methods of using the same |
| US9248584B2 (en) | 2010-09-24 | 2016-02-02 | Bend Research, Inc. | High-temperature spray drying process and apparatus |
| US9724664B2 (en) | 2009-03-27 | 2017-08-08 | Bend Research, Inc. | Spray-drying process |
| US11364203B2 (en) | 2014-10-31 | 2022-06-21 | Bend Reserch, Inc. | Process for forming active domains dispersed in a matrix |
-
1960
- 1960-05-11 GB GB16626/60A patent/GB918168A/en not_active Expired
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0357169A1 (en) * | 1988-08-30 | 1990-03-07 | Asama Chemical Co., Ltd. | Stabilized vitamin powder |
| US5756719A (en) * | 1996-09-03 | 1998-05-26 | Basf Corporation | Double emulsion techniques for making novel compositions containing gluten and polysaccharides that contain uronic acid residues useful for encapsulating fats, oils and solids |
| US5767107A (en) * | 1996-09-03 | 1998-06-16 | Basf Corporation | Compositions containing gluten and polysaccharides that contain uronic acid residues useful for encapsulating fats, oils and solids |
| WO2008072270A3 (en) * | 2006-12-11 | 2008-08-21 | John S Chen | Method for producing a proteic net able to trap nutrients and/or pharmacologically active substances |
| US9724664B2 (en) | 2009-03-27 | 2017-08-08 | Bend Research, Inc. | Spray-drying process |
| US10300443B2 (en) | 2009-03-27 | 2019-05-28 | Bend Research, Inc. | Spray-drying process |
| US10675602B2 (en) | 2009-03-27 | 2020-06-09 | Bend Research, Inc. | Spray-drying process |
| US9084976B2 (en) | 2010-09-03 | 2015-07-21 | Bend Research, Inc. | Spray-drying apparatus and methods of using the same |
| US9205345B2 (en) | 2010-09-03 | 2015-12-08 | Bend Research, Inc. | Spray-drying apparatus and methods of using the same |
| US9358478B2 (en) | 2010-09-03 | 2016-06-07 | Bend Research, Inc. | Spray-drying apparatus and methods of using the same |
| US9084944B2 (en) | 2010-09-03 | 2015-07-21 | Bend Research, Inc. | Spray-drying apparatus and methods of using the same |
| US9248584B2 (en) | 2010-09-24 | 2016-02-02 | Bend Research, Inc. | High-temperature spray drying process and apparatus |
| US11364203B2 (en) | 2014-10-31 | 2022-06-21 | Bend Reserch, Inc. | Process for forming active domains dispersed in a matrix |
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