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GB917916A - Process and apparatus for the separation of substances by fractional crystallisationfrom melts - Google Patents

Process and apparatus for the separation of substances by fractional crystallisationfrom melts

Info

Publication number
GB917916A
GB917916A GB30378/61A GB3037861A GB917916A GB 917916 A GB917916 A GB 917916A GB 30378/61 A GB30378/61 A GB 30378/61A GB 3037861 A GB3037861 A GB 3037861A GB 917916 A GB917916 A GB 917916A
Authority
GB
United Kingdom
Prior art keywords
fractional
crystallisationfrom
melts
substances
separation
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB30378/61A
Inventor
Adolf Meier
Ludwig Raichle
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Badische Anilin and Sodafabrik AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE, Badische Anilin and Sodafabrik AG filed Critical BASF SE
Publication of GB917916A publication Critical patent/GB917916A/en
Expired legal-status Critical Current

Links

Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0004Crystallisation cooling by heat exchange
    • B01D9/0013Crystallisation cooling by heat exchange by indirect heat exchange
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/004Fractional crystallisation; Fractionating or rectifying columns
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D9/00Crystallisation
    • B01D9/0072Crystallisation in microfluidic devices

Landscapes

  • Chemical & Material Sciences (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)

Abstract

<FORM:0917916/III/1> In the fractional crystallization process such as are described in Figs. 6-8 (not shown) wherein the crystals are separated out in each stage by means of a trough similar to that of Fig. 1. The crystals are melted and at least partially returned to a preceding stage. The fused mixture is contained in trough 1 while internally cooled disc becomes coated with crystal layer 4 which is melted in device 5 and the purified melt is withdrawn through pipe 6. The heating and cooling of the disc may be by electric means or by using hollow constructions with heat exchange liquids.
GB30378/61A 1960-08-27 1961-08-23 Process and apparatus for the separation of substances by fractional crystallisationfrom melts Expired GB917916A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEB0059144 1960-08-27

Publications (1)

Publication Number Publication Date
GB917916A true GB917916A (en) 1963-02-06

Family

ID=6972341

Family Applications (1)

Application Number Title Priority Date Filing Date
GB30378/61A Expired GB917916A (en) 1960-08-27 1961-08-23 Process and apparatus for the separation of substances by fractional crystallisationfrom melts

Country Status (1)

Country Link
GB (1) GB917916A (en)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0521499A1 (en) * 1991-07-05 1993-01-07 Hoechst Aktiengesellschaft Process and device for the separation and purification of substances by fractional crystallization from melts
NL1006181C2 (en) * 1997-05-30 1998-12-01 Goudsche Machinefabriek Bv Crystalliser with rotating plates and scraper blades mounted on shaft above trough
WO2015189223A1 (en) * 2014-06-12 2015-12-17 Basf Se Crystallisation apparatus and process

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0521499A1 (en) * 1991-07-05 1993-01-07 Hoechst Aktiengesellschaft Process and device for the separation and purification of substances by fractional crystallization from melts
NL1006181C2 (en) * 1997-05-30 1998-12-01 Goudsche Machinefabriek Bv Crystalliser with rotating plates and scraper blades mounted on shaft above trough
WO2015189223A1 (en) * 2014-06-12 2015-12-17 Basf Se Crystallisation apparatus and process
CN106457062A (en) * 2014-06-12 2017-02-22 巴斯夫欧洲公司 Crystallisation apparatus and process
CN106457062B (en) * 2014-06-12 2019-08-06 巴斯夫欧洲公司 Crystallization apparatus and method

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