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GB703407A - Improvements in or relating to a process of making synthetic resins and the productsresulting therefrom - Google Patents

Improvements in or relating to a process of making synthetic resins and the productsresulting therefrom

Info

Publication number
GB703407A
GB703407A GB25485/50A GB2548550A GB703407A GB 703407 A GB703407 A GB 703407A GB 25485/50 A GB25485/50 A GB 25485/50A GB 2548550 A GB2548550 A GB 2548550A GB 703407 A GB703407 A GB 703407A
Authority
GB
United Kingdom
Prior art keywords
acid
etherifying
mono
reacted
reaction
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB25485/50A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Standard Dyewood Co
Original Assignee
Standard Dyewood Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Standard Dyewood Co filed Critical Standard Dyewood Co
Publication of GB703407A publication Critical patent/GB703407A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G8/00Condensation polymers of aldehydes or ketones with phenols only
    • C08G8/28Chemically modified polycondensates
    • C08G8/36Chemically modified polycondensates by etherifying
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G8/00Condensation polymers of aldehydes or ketones with phenols only
    • C08G8/04Condensation polymers of aldehydes or ketones with phenols only of aldehydes
    • C08G8/08Condensation polymers of aldehydes or ketones with phenols only of aldehydes of formaldehyde, e.g. of formaldehyde formed in situ
    • C08G8/18Condensation polymers of aldehydes or ketones with phenols only of aldehydes of formaldehyde, e.g. of formaldehyde formed in situ with phenols substituted by carboxylic or sulfonic acid groups
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08GMACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G8/00Condensation polymers of aldehydes or ketones with phenols only
    • C08G8/04Condensation polymers of aldehydes or ketones with phenols only of aldehydes
    • C08G8/08Condensation polymers of aldehydes or ketones with phenols only of aldehydes of formaldehyde, e.g. of formaldehyde formed in situ
    • C08G8/20Condensation polymers of aldehydes or ketones with phenols only of aldehydes of formaldehyde, e.g. of formaldehyde formed in situ with polyhydric phenols

Landscapes

  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Treatment And Processing Of Natural Fur Or Leather (AREA)

Abstract

A synthetic resin is made by etherifying at least one phenolic hydroxyl group of a natural catechol tanning agent with mono-chloro- or mono-bromoacetic or propionic acid, by reaction in an alkaline medium with not more than 2 mols. of the acid per mol. of tanning agent and etherifying at least one of the remaining phenolic hydroxyl groups by reaction with an aralkyl halide in an alkaline aqueous medium. The products are soluble in organic solvents such as mixtures of benzene or toluene and methyl or ethyl alcohol. In the example, quebracho extract is reacted with monochloracetic acid in the presence of caustic soda, and the resulting product is reacted with benzyl chloride; the product is poured and allowed to solidify in a tray, the resulting soapy mass being added to cold aqueous hydrochloric acid and the resin removed by filtration. The final product is considered to be a quebrachomonocarboxymethyl dibenzyl- or -di(carboxymethyl) monobenzyl-tri-ether according to the molar proportions of the reactants employed. The products may be used in compositions for coating leather, cloth and paper.ALSO:A synthetic resin is made by etherifying at least one phenolic hydroxyl group of a natural catechol tanning agent with mono-chloro- or mono-bromo-acetic or propionic acid by reaction in p an alkaline medium with not more than 2 mols. of the acid per mol. of tanning agent, and etherifying at least one of the remaining phenolic hydroxyl groups by reaction with an aralkyl halide in an alkaline aqueous medium. In the example, quebracho extract is reacted with monochloracetic acid in the presence of caustic soda, and the resulting product is reacted with benzyl chloride; the product is poured and allowed to solidify in a tray, the resulting soapy mass being added to cold aqueous hydrochloric acid and the resin removed by filtration. The final product is considered to be a quebracho-monocarboxymethyldibenzyl- or -di (carboxymethyl) monobenzyl-triether, according to the molar proportions of the reactants employed.
GB25485/50A 1950-07-14 1950-10-19 Improvements in or relating to a process of making synthetic resins and the productsresulting therefrom Expired GB703407A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
US703407XA 1950-07-14 1950-07-14

Publications (1)

Publication Number Publication Date
GB703407A true GB703407A (en) 1954-02-03

Family

ID=22094693

Family Applications (1)

Application Number Title Priority Date Filing Date
GB25485/50A Expired GB703407A (en) 1950-07-14 1950-10-19 Improvements in or relating to a process of making synthetic resins and the productsresulting therefrom

Country Status (1)

Country Link
GB (1) GB703407A (en)

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