GB2002020A - Conditioning of 4,4',7,7'- Tetrachlorothioindigo - Google Patents
Conditioning of 4,4',7,7'- TetrachlorothioindigoInfo
- Publication number
- GB2002020A GB2002020A GB7831912A GB7831912A GB2002020A GB 2002020 A GB2002020 A GB 2002020A GB 7831912 A GB7831912 A GB 7831912A GB 7831912 A GB7831912 A GB 7831912A GB 2002020 A GB2002020 A GB 2002020A
- Authority
- GB
- United Kingdom
- Prior art keywords
- large amounts
- kneaded
- acid
- pigment
- tetrachlorothioindigo
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- KZFMOINJHMONLW-FOCLMDBBSA-N (2e)-4,7-dichloro-2-(4,7-dichloro-3-oxo-1-benzothiophen-2-ylidene)-1-benzothiophen-3-one Chemical compound S\1C(C(=CC=C2Cl)Cl)=C2C(=O)C/1=C1/C(=O)C(C(Cl)=CC=C2Cl)=C2S1 KZFMOINJHMONLW-FOCLMDBBSA-N 0.000 title 1
- 230000003750 conditioning effect Effects 0.000 title 1
- 239000000203 mixture Substances 0.000 abstract 2
- 239000000049 pigment Substances 0.000 abstract 2
- 235000000177 Indigofera tinctoria Nutrition 0.000 abstract 1
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 230000001143 conditioned effect Effects 0.000 abstract 1
- 239000000975 dye Substances 0.000 abstract 1
- 229940097275 indigo Drugs 0.000 abstract 1
- COHYTHOBJLSHDF-UHFFFAOYSA-N indigo powder Natural products N1C2=CC=CC=C2C(=O)C1=C1C(=O)C2=CC=CC=C2N1 COHYTHOBJLSHDF-UHFFFAOYSA-N 0.000 abstract 1
- 238000004898 kneading Methods 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 235000011149 sulphuric acid Nutrition 0.000 abstract 1
- 239000001117 sulphuric acid Substances 0.000 abstract 1
- 238000011282 treatment Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0017—Influencing the physical properties by treatment with an acid, H2SO4
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B7/00—Indigoid dyes
- C09B7/10—Bis-thionapthene indigos
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Disintegrating Or Milling (AREA)
Abstract
The raw pigment is kneaded with sulphuric acid at a viscosity sufficient to permit sheering forces to be exerted upon the mixture during kneading and subsequently the kneaded mixture hydrolyzed by the addition of water. The conditioned indigo pigment is an effective commercial dyeing agent and the disadvantages of earlier known treatments which require large amounts of acid or large amounts of solvents are overcome.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19772734951 DE2734951C2 (en) | 1977-08-03 | 1977-08-03 | Process for the aftertreatment of 4,4 ', 7,7'-tetrachlorothioindigo |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB2002020A true GB2002020A (en) | 1979-02-14 |
Family
ID=6015518
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB7831912A Withdrawn GB2002020A (en) | 1977-08-03 | 1978-08-02 | Conditioning of 4,4',7,7'- Tetrachlorothioindigo |
Country Status (3)
| Country | Link |
|---|---|
| DE (1) | DE2734951C2 (en) |
| FR (1) | FR2399468A1 (en) |
| GB (1) | GB2002020A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1037187C (en) * | 1991-04-15 | 1998-01-28 | Basf公司 | Purification method of indigo |
| CN1037450C (en) * | 1991-04-15 | 1998-02-18 | Basr公司 | Process for preparing purified indigo |
| CN1043651C (en) * | 1991-07-17 | 1999-06-16 | Basf公司 | A method for preparing purified indigo |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2916400A1 (en) * | 1979-04-23 | 1980-11-13 | Basf Ag | METHOD FOR PRODUCING LASING PIGMENT FORMS OF 4,4 ', 7,7'-TETRACHLORTHIOINDIGO |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1156998A (en) * | 1956-07-26 | 1958-05-23 | Gen Aniline & Film Corp | Acid mashing of organic compounds in the tank |
| US3022299A (en) * | 1958-12-30 | 1962-02-20 | Gen Aniline & Film Corp | Conditioning of pigments |
-
1977
- 1977-08-03 DE DE19772734951 patent/DE2734951C2/en not_active Expired
-
1978
- 1978-08-02 GB GB7831912A patent/GB2002020A/en not_active Withdrawn
- 1978-08-03 FR FR7822988A patent/FR2399468A1/en not_active Withdrawn
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1037187C (en) * | 1991-04-15 | 1998-01-28 | Basf公司 | Purification method of indigo |
| CN1037450C (en) * | 1991-04-15 | 1998-02-18 | Basr公司 | Process for preparing purified indigo |
| CN1043651C (en) * | 1991-07-17 | 1999-06-16 | Basf公司 | A method for preparing purified indigo |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2734951B1 (en) | 1978-12-07 |
| DE2734951C2 (en) | 1979-08-09 |
| FR2399468A1 (en) | 1979-03-02 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| WAP | Application withdrawn, taken to be withdrawn or refused ** after publication under section 16(1) |