GB1535485A - Isolation of epsilon-caprolactam - Google Patents
Isolation of epsilon-caprolactamInfo
- Publication number
- GB1535485A GB1535485A GB2272777A GB2272777A GB1535485A GB 1535485 A GB1535485 A GB 1535485A GB 2272777 A GB2272777 A GB 2272777A GB 2272777 A GB2272777 A GB 2272777A GB 1535485 A GB1535485 A GB 1535485A
- Authority
- GB
- United Kingdom
- Prior art keywords
- caprolactam
- epsilon
- isolation
- toluene
- lactam
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- JBKVHLHDHHXQEQ-UHFFFAOYSA-N epsilon-caprolactam Chemical compound O=C1CCCCCN1 JBKVHLHDHHXQEQ-UHFFFAOYSA-N 0.000 title abstract 4
- 238000002955 isolation Methods 0.000 title 1
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 6
- 150000003951 lactams Chemical class 0.000 abstract 2
- 238000000034 method Methods 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 238000001953 recrystallisation Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
- C07D201/16—Separation or purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Other In-Based Heterocyclic Compounds (AREA)
- Polyamides (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pyrrole Compounds (AREA)
Abstract
Process for purifying epsilon -caprolactam by extraction and recrystallisation, wherein a crude lactam is extracted with toluene and recrystallised from toluene. The process is particularly simple to carry out continuously with high yield without distillation to obtain ultrapure lactam.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19762625402 DE2625402A1 (en) | 1976-06-05 | 1976-06-05 | CLEANING EPSILON CAPROLACTAM |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1535485A true GB1535485A (en) | 1978-12-13 |
Family
ID=5979933
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2272777A Expired GB1535485A (en) | 1976-06-05 | 1977-05-30 | Isolation of epsilon-caprolactam |
Country Status (10)
| Country | Link |
|---|---|
| JP (1) | JPS52151186A (en) |
| BE (1) | BE855367A (en) |
| BR (1) | BR7703572A (en) |
| CH (1) | CH626339A5 (en) |
| DD (1) | DD132491A5 (en) |
| DE (1) | DE2625402A1 (en) |
| ES (1) | ES459328A1 (en) |
| FR (1) | FR2353535A1 (en) |
| GB (1) | GB1535485A (en) |
| NL (1) | NL7706080A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115253380A (en) * | 2022-08-19 | 2022-11-01 | 清元智能科技研究院(湖北)有限公司 | Caprolactam extraction system and method |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2845075A1 (en) * | 1978-10-17 | 1980-05-08 | Basf Ag | METHOD FOR PURIFYING ROHCAPROLACTAM |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH522649A (en) * | 1970-04-17 | 1973-04-13 | Buchs Metallwerk Ag | Caprolactam purification - by solvent extn and crystallisation using same solvent |
| SU387996A1 (en) * | 1971-04-30 | 1973-06-22 | METHOD OF CLEANING CAPROLACTAM | |
| CH564528A5 (en) * | 1972-06-14 | 1975-07-31 | Buchs Metallwerk Ag | Purification of caprolactam freed from water - by counter-current multi-stage cystallisation from the melt using a solvent |
-
1976
- 1976-06-05 DE DE19762625402 patent/DE2625402A1/en not_active Withdrawn
-
1977
- 1977-05-30 GB GB2272777A patent/GB1535485A/en not_active Expired
- 1977-05-31 ES ES459328A patent/ES459328A1/en not_active Expired
- 1977-06-02 NL NL7706080A patent/NL7706080A/en not_active Application Discontinuation
- 1977-06-02 BR BR7703572A patent/BR7703572A/en unknown
- 1977-06-03 JP JP6492777A patent/JPS52151186A/en active Pending
- 1977-06-03 CH CH689777A patent/CH626339A5/en not_active IP Right Cessation
- 1977-06-03 BE BE178173A patent/BE855367A/en not_active IP Right Cessation
- 1977-06-03 FR FR7717079A patent/FR2353535A1/en active Granted
- 1977-06-03 DD DD19929277A patent/DD132491A5/en unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN115253380A (en) * | 2022-08-19 | 2022-11-01 | 清元智能科技研究院(湖北)有限公司 | Caprolactam extraction system and method |
| CN115253380B (en) * | 2022-08-19 | 2023-09-01 | 清元智能科技研究院(湖北)有限公司 | Caprolactam extraction system and method |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2353535A1 (en) | 1977-12-30 |
| DE2625402A1 (en) | 1977-12-22 |
| CH626339A5 (en) | 1981-11-13 |
| BE855367A (en) | 1977-12-05 |
| ES459328A1 (en) | 1978-03-16 |
| FR2353535B1 (en) | 1982-07-02 |
| JPS52151186A (en) | 1977-12-15 |
| DD132491A5 (en) | 1978-10-04 |
| BR7703572A (en) | 1978-03-21 |
| NL7706080A (en) | 1977-12-07 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |