GB1513525A - Method for manufacturing polyurethane films and surface coatings from tall oil pitch - Google Patents
Method for manufacturing polyurethane films and surface coatings from tall oil pitchInfo
- Publication number
- GB1513525A GB1513525A GB1246476A GB1246476A GB1513525A GB 1513525 A GB1513525 A GB 1513525A GB 1246476 A GB1246476 A GB 1246476A GB 1246476 A GB1246476 A GB 1246476A GB 1513525 A GB1513525 A GB 1513525A
- Authority
- GB
- United Kingdom
- Prior art keywords
- tall oil
- oil pitch
- weight
- esterified
- triisocyanate
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003784 tall oil Substances 0.000 title abstract 10
- 238000000576 coating method Methods 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 238000000034 method Methods 0.000 title abstract 2
- 229920006264 polyurethane film Polymers 0.000 title abstract 2
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 abstract 3
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 abstract 3
- 125000002887 hydroxy group Chemical group [H]O* 0.000 abstract 3
- 239000000203 mixture Substances 0.000 abstract 3
- 239000002253 acid Substances 0.000 abstract 2
- 125000001931 aliphatic group Chemical group 0.000 abstract 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 abstract 1
- MQIUGAXCHLFZKX-UHFFFAOYSA-N Di-n-octyl phthalate Natural products CCCCCCCCOC(=O)C1=CC=CC=C1C(=O)OCCCCCCCC MQIUGAXCHLFZKX-UHFFFAOYSA-N 0.000 abstract 1
- 102100031605 Dolichol kinase Human genes 0.000 abstract 1
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 abstract 1
- 239000005977 Ethylene Substances 0.000 abstract 1
- 101000845698 Homo sapiens Dolichol kinase Proteins 0.000 abstract 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 abstract 1
- -1 aliphatic alcohols Chemical class 0.000 abstract 1
- BJQHLKABXJIVAM-UHFFFAOYSA-N bis(2-ethylhexyl) phthalate Chemical compound CCCCC(CC)COC(=O)C1=CC=CC=C1C(=O)OCC(CC)CCCC BJQHLKABXJIVAM-UHFFFAOYSA-N 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 abstract 1
- 239000003085 diluting agent Substances 0.000 abstract 1
- 239000000975 dye Substances 0.000 abstract 1
- 230000032050 esterification Effects 0.000 abstract 1
- 238000005886 esterification reaction Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- IQPQWNKOIGAROB-UHFFFAOYSA-N isocyanate group Chemical group [N-]=C=O IQPQWNKOIGAROB-UHFFFAOYSA-N 0.000 abstract 1
- 239000000463 material Substances 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- WXZMFSXDPGVJKK-UHFFFAOYSA-N pentaerythritol Chemical compound OCC(CO)(CO)CO WXZMFSXDPGVJKK-UHFFFAOYSA-N 0.000 abstract 1
- 239000011527 polyurethane coating Substances 0.000 abstract 1
- JOXIMZWYDAKGHI-UHFFFAOYSA-N toluene-4-sulfonic acid Chemical compound CC1=CC=C(S(O)(=O)=O)C=C1 JOXIMZWYDAKGHI-UHFFFAOYSA-N 0.000 abstract 1
- 239000008096 xylene Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
- C08G18/30—Low-molecular-weight compounds
- C08G18/36—Hydroxylated esters of higher fatty acids
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyurethanes Or Polyureas (AREA)
Abstract
1513525 Polyurethane coatings from tall oil pitch M DOLK V ERA and J J LINDBERG 29 March 1976 12464/76 Heading C3R A method for the manufacture of polyurethane films and coatings from tall oil pitch comprises esterifying a tall oil pitch, having an acid number of 30-60 and a hydroxyl number of 60-90 with from 5-15 wt. per cent based on the weight of tall oil pitch, of an aliphatic alcohol having at least three hydroxy groups to give an esterified tall oil pitch having an acid number of 5-35 and a hydroxyl number of 200-350; adding to the esterified tall oil pitch an aliphatic triisocyanate in an ambient sufficient to give 10-35 parts by weight of isocyanate groups per 100 parts by weight of esterified tall oil pitch; spreading the mixture on a base material and curing the coating or film at room temperature or above. Suitable aliphatic alcohols are glycerol or pentaerythritol. The esterification may be carried out by heating under reduced pressure in the presence of 0À1-0À5 wt. per cent p-toluene-sulphonic acid based on the weight of tall oil pitch. The aliphatic triisocyanate may be added as a solution in an inert organic solvent, e.g. a 1 : 1 mixture of ethylene glycolacetate and xylene. Diluents, e.g. ethyl acetate, softeners, e.g. dioctyl phthalate and dyes may be added to the triisocyanate/esterified tall oil pitch mixture before curing which may take from 1-3 days at room temperature or 1-10 hours at 100‹ C.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1246476A GB1513525A (en) | 1976-03-29 | 1976-03-29 | Method for manufacturing polyurethane films and surface coatings from tall oil pitch |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1246476A GB1513525A (en) | 1976-03-29 | 1976-03-29 | Method for manufacturing polyurethane films and surface coatings from tall oil pitch |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1513525A true GB1513525A (en) | 1978-06-07 |
Family
ID=10005091
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1246476A Expired GB1513525A (en) | 1976-03-29 | 1976-03-29 | Method for manufacturing polyurethane films and surface coatings from tall oil pitch |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB1513525A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2165772A (en) * | 1984-09-07 | 1986-04-23 | Nippon Steel Corp | Steel article having heavy-duty anticorrosive coating |
| EP0230301A3 (en) * | 1986-01-22 | 1988-02-17 | Oy Lohja Ab | A process for the preparation of an isocyanurate modified polyurethane foam and a polyurethane foam prepared by the process |
| EP2657268A1 (en) * | 2012-04-25 | 2013-10-30 | Arkema France | Polyurethane for non-aqueous, bio-sourced, hydroxylated fatty polyester coatings, modified with rosin |
-
1976
- 1976-03-29 GB GB1246476A patent/GB1513525A/en not_active Expired
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2165772A (en) * | 1984-09-07 | 1986-04-23 | Nippon Steel Corp | Steel article having heavy-duty anticorrosive coating |
| EP0230301A3 (en) * | 1986-01-22 | 1988-02-17 | Oy Lohja Ab | A process for the preparation of an isocyanurate modified polyurethane foam and a polyurethane foam prepared by the process |
| EP2657268A1 (en) * | 2012-04-25 | 2013-10-30 | Arkema France | Polyurethane for non-aqueous, bio-sourced, hydroxylated fatty polyester coatings, modified with rosin |
| FR2989975A1 (en) * | 2012-04-25 | 2013-11-01 | Arkema France | POLYURETHANE FOR NON-AQUEOUS COATINGS BASED ON BIOSOURCE HYDROXYL FATTY POLYESTER, MODIFIED WITH COLOPHANE |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |