GB1499217A - Preparation of hydrazodicarbonamide - Google Patents
Preparation of hydrazodicarbonamideInfo
- Publication number
- GB1499217A GB1499217A GB30807/75A GB3080775A GB1499217A GB 1499217 A GB1499217 A GB 1499217A GB 30807/75 A GB30807/75 A GB 30807/75A GB 3080775 A GB3080775 A GB 3080775A GB 1499217 A GB1499217 A GB 1499217A
- Authority
- GB
- United Kingdom
- Prior art keywords
- hydrazodicarbonamide
- ketazine
- preparation
- urea
- uniroyal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- ULUZGMIUTMRARO-UHFFFAOYSA-N (carbamoylamino)urea Chemical compound NC(=O)NNC(N)=O ULUZGMIUTMRARO-UHFFFAOYSA-N 0.000 title abstract 3
- PFLUPZGCTVGDLV-UHFFFAOYSA-N acetone azine Chemical compound CC(C)=NN=C(C)C PFLUPZGCTVGDLV-UHFFFAOYSA-N 0.000 abstract 3
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 abstract 2
- 239000004202 carbamide Substances 0.000 abstract 2
- 125000004209 (C1-C8) alkyl group Chemical group 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 125000001931 aliphatic group Chemical group 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C281/00—Derivatives of carbonic acid containing functional groups covered by groups C07C269/00 - C07C279/00 in which at least one nitrogen atom of these functional groups is further bound to another nitrogen atom not being part of a nitro or nitroso group
- C07C281/06—Compounds containing any of the groups, e.g. semicarbazides
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
1499217 Hydrazodicarbonamide UNIROYAL Inc 23 July 1975 [9 Sept 1974] 30807/75 Heading C2C Hydrazodicarbonamide, is obtained by reacting urea, water and a ketazine in the absence of acid at a temperature above 50‹ C., the molar ratio of urea to ketazine being at least 2 : 1, and the ketazine having the Formula I: in which R 1 , R 2 , R 3 and R 4 are C 1-8 alkyl groups or R 1 and R 2 and/or R 3 and R 4 together form a 5- or 6-membered aliphatic ring.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/504,015 US3969466A (en) | 1974-09-09 | 1974-09-09 | Preparation of hydrazodicarbonamide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1499217A true GB1499217A (en) | 1978-01-25 |
Family
ID=24004513
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB30807/75A Expired GB1499217A (en) | 1974-09-09 | 1975-07-23 | Preparation of hydrazodicarbonamide |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3969466A (en) |
| JP (1) | JPS5724340B2 (en) |
| BE (1) | BE832951A (en) |
| CA (1) | CA1022566A (en) |
| FR (1) | FR2283889A1 (en) |
| GB (1) | GB1499217A (en) |
| IT (1) | IT1041584B (en) |
| NL (1) | NL7508949A (en) |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5928546B2 (en) * | 1977-03-24 | 1984-07-13 | 大塚化学薬品株式会社 | Production method of hydrazodicarbonamide |
| US5057601A (en) * | 1989-11-06 | 1991-10-15 | Olin Corporation | Process for producing a gel-free coagulated rubber with low ethylenic unsaturation |
| US5039737A (en) * | 1990-02-22 | 1991-08-13 | The Goodyear Tire & Rubber Company/Olin Corp. | Ozonolysis of hydrogenated latices |
| KR100345874B1 (en) * | 2000-01-07 | 2002-07-27 | 주식회사 제이앤드제이 캐미칼 | Method for synthesizing hydrazodicarbonamide |
| DE10035010A1 (en) * | 2000-07-19 | 2002-01-31 | Bayer Ag | Process for the preparation of hydrazodicarbonamide (HDC) via ketimines |
| KR100473333B1 (en) * | 2001-10-24 | 2005-03-07 | 주식회사 제이앤드제이 캐미칼 | Method and apparatus for preparing hydrazodicarbonamide using urea as starting material |
| CN105130849A (en) * | 2015-10-10 | 2015-12-09 | 杭州海虹精细化工有限公司 | Environment-friendly technology for unitedly preparing ADC foaming agent and ammonium chloride by using ketazine as raw material |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2692281A (en) * | 1953-06-05 | 1954-10-19 | Us Rubber Co | Preparation of hydrazodicarbonamide |
| US3153089A (en) * | 1961-08-16 | 1964-10-13 | Allied Chem | Production of acetophenone-azine |
| FR2142786B1 (en) * | 1971-06-25 | 1973-06-29 | Ugine Kuhlmann |
-
1974
- 1974-09-09 US US05/504,015 patent/US3969466A/en not_active Expired - Lifetime
- 1974-11-13 CA CA213,633A patent/CA1022566A/en not_active Expired
-
1975
- 1975-07-23 GB GB30807/75A patent/GB1499217A/en not_active Expired
- 1975-07-28 NL NL7508949A patent/NL7508949A/en not_active Application Discontinuation
- 1975-08-19 IT IT69106/75A patent/IT1041584B/en active
- 1975-09-01 BE BE159641A patent/BE832951A/en not_active IP Right Cessation
- 1975-09-04 FR FR7527180A patent/FR2283889A1/en active Granted
- 1975-09-08 JP JP10880375A patent/JPS5724340B2/ja not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| CA1022566A (en) | 1977-12-13 |
| NL7508949A (en) | 1976-03-11 |
| FR2283889A1 (en) | 1976-04-02 |
| US3969466A (en) | 1976-07-13 |
| DE2539222B2 (en) | 1977-06-23 |
| BE832951A (en) | 1976-03-01 |
| FR2283889B1 (en) | 1978-09-22 |
| IT1041584B (en) | 1980-01-10 |
| JPS5724340B2 (en) | 1982-05-24 |
| DE2539222A1 (en) | 1976-03-25 |
| JPS5152129A (en) | 1976-05-08 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| ES442382A1 (en) | Red pigment and process | |
| GB1262752A (en) | A process for n-methylating nitroanilines and compounds prepared thereby | |
| GB1499217A (en) | Preparation of hydrazodicarbonamide | |
| ES441385A1 (en) | Substituted imidazolidines and pharmaceutical uses thereo | |
| GB1373549A (en) | 3-halogenopyridazines and their preparation | |
| GB1513168A (en) | Bisazomethine metal complex colourants of hydroxy-coumarin derivatives or hydroxy-chromone derivatives and process for their manufacture | |
| GB1449387A (en) | Benzylpyrimidine derivatives | |
| GB1303949A (en) | ||
| GB1213439A (en) | Pesticides comprising thiosemicarbazides | |
| GB1507414A (en) | Hydantoin derivatives | |
| GB1503447A (en) | Dl-and 8r-9-fluoro-prostadienoic acid derivatives and process | |
| GB1465794A (en) | Thiourea derivatives | |
| BG33282A3 (en) | Method for obtaining of 4- amino- 5- chlorine- 1- phenylpyridazon- (6) | |
| GB1379328A (en) | Monoazo dyestuffs | |
| GB1419923A (en) | Agent for inhibiting vegetative plant growth | |
| GB1463582A (en) | Pyridine derivatives | |
| GB1380368A (en) | Preparation of penicillamine or its homologues | |
| GB1386930A (en) | Process for the manufacture of tris-trimethylsiloxy-phenylsilane | |
| GB1394563A (en) | Process for preparing benzamides | |
| GB1341153A (en) | Fluorophenyl ureas and their use in the regulation of plant growth | |
| GB1461806A (en) | Pyridine derivatives | |
| GB1415338A (en) | Amino acids and derivatives thereof | |
| GB1295838A (en) | ||
| GB1363691A (en) | Benzothiazole derivatives | |
| GB1535994A (en) | Deuterated prostaglandin analogues |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| 732 | Registration of transactions, instruments or events in the register (sect. 32/1977) | ||
| PCNP | Patent ceased through non-payment of renewal fee |