GB1468790A - Production of salts of chlorinated acetic acids - Google Patents
Production of salts of chlorinated acetic acidsInfo
- Publication number
- GB1468790A GB1468790A GB2613175A GB2613175A GB1468790A GB 1468790 A GB1468790 A GB 1468790A GB 2613175 A GB2613175 A GB 2613175A GB 2613175 A GB2613175 A GB 2613175A GB 1468790 A GB1468790 A GB 1468790A
- Authority
- GB
- United Kingdom
- Prior art keywords
- salts
- bed reactor
- salt
- fluidized bed
- inert gas
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000003839 salts Chemical class 0.000 title abstract 4
- 150000001243 acetic acids Chemical class 0.000 title abstract 2
- FOCAUTSVDIKZOP-UHFFFAOYSA-N chloroacetic acid Chemical class OC(=O)CCl FOCAUTSVDIKZOP-UHFFFAOYSA-N 0.000 abstract 3
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 abstract 2
- 229940106681 chloroacetic acid Drugs 0.000 abstract 2
- 239000011261 inert gas Substances 0.000 abstract 2
- 239000007788 liquid Substances 0.000 abstract 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-L Carbonate Chemical compound [O-]C([O-])=O BVKZGUZCCUSVTD-UHFFFAOYSA-L 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 abstract 1
- -1 alkaline earth metal salts Chemical class 0.000 abstract 1
- 229910021529 ammonia Inorganic materials 0.000 abstract 1
- UTPOUAZEFGTYAY-UHFFFAOYSA-N azanium;2-chloroacetate Chemical compound [NH4+].[O-]C(=O)CCl UTPOUAZEFGTYAY-UHFFFAOYSA-N 0.000 abstract 1
- 239000002585 base Substances 0.000 abstract 1
- 150000007514 bases Chemical class 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 230000009969 flowable effect Effects 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 1
- YNLZKJXZEZFHDO-UHFFFAOYSA-M potassium;2,2,2-trichloroacetate Chemical compound [K+].[O-]C(=O)C(Cl)(Cl)Cl YNLZKJXZEZFHDO-UHFFFAOYSA-M 0.000 abstract 1
- FDRCDNZGSXJAFP-UHFFFAOYSA-M sodium chloroacetate Chemical compound [Na+].[O-]C(=O)CCl FDRCDNZGSXJAFP-UHFFFAOYSA-M 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- 239000000725 suspension Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
- C07C51/41—Preparation of salts of carboxylic acids
- C07C51/412—Preparation of salts of carboxylic acids by conversion of the acids, their salts, esters or anhydrides with the same carboxylic acid part
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
1468790 Salts of chloroacetic acids HOECHST AG 19 June 1975 [6 July 1974] 26131/75 Heading C2C Alkali metal, ammonium or alkaline earth metal salts of chlorinated acetic acids are produced by reacting a chloroacetic acid with a suitable base and/or salt-forming derivative thereof at 20-150 C. by introducing them into a fluidized bed reactor, the bed being prepared from the resulting salt and being fluidized by means of an inert gas or liquid, and the resulting readily flowable salt is discharged from the fluidized bed reactor continuously or intermittently, at the same rate as it is being formed. Liquid or dissolved chloroacetic acid is preferably sprayed into the fluidized bed reactor or molten acid is introduced in vapour form by means of an inert gas. The basic compound may be added either in substance, solution or suspension and is preferably an oxide, hydroxide, carbonate or ammonia. In the examples sodium monochloroacetate, ammonium monochloroacetate and potassium trichloroacetate are prepared.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2432567A DE2432567C3 (en) | 1974-07-06 | 1974-07-06 | Process for the preparation of salts of chlorinated acetic acids |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1468790A true GB1468790A (en) | 1977-03-30 |
Family
ID=5919898
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2613175A Expired GB1468790A (en) | 1974-07-06 | 1975-06-19 | Production of salts of chlorinated acetic acids |
Country Status (15)
| Country | Link |
|---|---|
| JP (1) | JPS5136418A (en) |
| BE (1) | BE831002A (en) |
| CA (1) | CA1041117A (en) |
| CH (1) | CH598177A5 (en) |
| CS (1) | CS192547B2 (en) |
| DD (1) | DD120011A5 (en) |
| DE (1) | DE2432567C3 (en) |
| DK (1) | DK304575A (en) |
| FR (1) | FR2277070A1 (en) |
| GB (1) | GB1468790A (en) |
| HU (1) | HU172246B (en) |
| IT (1) | IT1040824B (en) |
| NL (1) | NL7508023A (en) |
| NO (1) | NO144525C (en) |
| SE (1) | SE425731B (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2001040160A1 (en) * | 1999-12-01 | 2001-06-07 | Akzo Nobel N.V. | Monochloric acetic acid granules |
| EP1285690A3 (en) * | 2001-08-08 | 2003-11-26 | Glatt Ingenieurtechnik GmbH | Process for producing solids in granular form |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS62179200U (en) * | 1986-04-28 | 1987-11-13 | ||
| JPS63159339A (en) * | 1986-12-24 | 1988-07-02 | Daicel Chem Ind Ltd | Production of sodium monochloroacetate |
| FR2722782B1 (en) | 1994-07-21 | 1996-09-06 | Atochem Elf Sa | SODIUM MONOCHLORACETATE HAVING IMPROVED IMPLEMENTING PROPERTIES |
-
1974
- 1974-07-06 DE DE2432567A patent/DE2432567C3/en not_active Expired
-
1975
- 1975-06-12 CH CH762975A patent/CH598177A5/xx not_active IP Right Cessation
- 1975-06-19 GB GB2613175A patent/GB1468790A/en not_active Expired
- 1975-06-24 JP JP50078467A patent/JPS5136418A/en active Pending
- 1975-06-26 CA CA230,243A patent/CA1041117A/en not_active Expired
- 1975-07-03 SE SE7507662A patent/SE425731B/en unknown
- 1975-07-04 NO NO752433A patent/NO144525C/en unknown
- 1975-07-04 IT IT50359/75A patent/IT1040824B/en active
- 1975-07-04 DD DD187106A patent/DD120011A5/xx unknown
- 1975-07-04 HU HU75HO00001814A patent/HU172246B/en unknown
- 1975-07-04 BE BE157982A patent/BE831002A/en unknown
- 1975-07-04 NL NL7508023A patent/NL7508023A/en not_active Application Discontinuation
- 1975-07-04 DK DK304575A patent/DK304575A/en not_active Application Discontinuation
- 1975-07-04 FR FR7521155A patent/FR2277070A1/en active Granted
- 1975-07-07 CS CS754808A patent/CS192547B2/en unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2001040160A1 (en) * | 1999-12-01 | 2001-06-07 | Akzo Nobel N.V. | Monochloric acetic acid granules |
| EP1285690A3 (en) * | 2001-08-08 | 2003-11-26 | Glatt Ingenieurtechnik GmbH | Process for producing solids in granular form |
Also Published As
| Publication number | Publication date |
|---|---|
| DD120011A5 (en) | 1976-05-20 |
| DE2432567C3 (en) | 1978-09-14 |
| NO144525B (en) | 1981-06-09 |
| CA1041117A (en) | 1978-10-24 |
| BE831002A (en) | 1976-01-05 |
| FR2277070B1 (en) | 1980-08-22 |
| JPS5136418A (en) | 1976-03-27 |
| DK304575A (en) | 1976-01-07 |
| HU172246B (en) | 1978-07-28 |
| NO752433L (en) | 1976-01-07 |
| IT1040824B (en) | 1979-12-20 |
| SE425731B (en) | 1982-11-01 |
| DE2432567A1 (en) | 1976-01-22 |
| CH598177A5 (en) | 1978-04-28 |
| CS192547B2 (en) | 1979-08-31 |
| DE2432567B2 (en) | 1978-01-12 |
| SE7507662L (en) | 1976-01-07 |
| NL7508023A (en) | 1976-01-08 |
| FR2277070A1 (en) | 1976-01-30 |
| NO144525C (en) | 1981-09-16 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PCNP | Patent ceased through non-payment of renewal fee |