GB1338204A - Thermosetting acrylic powder coating compositions - Google Patents
Thermosetting acrylic powder coating compositionsInfo
- Publication number
- GB1338204A GB1338204A GB1355872A GB1355872A GB1338204A GB 1338204 A GB1338204 A GB 1338204A GB 1355872 A GB1355872 A GB 1355872A GB 1355872 A GB1355872 A GB 1355872A GB 1338204 A GB1338204 A GB 1338204A
- Authority
- GB
- United Kingdom
- Prior art keywords
- powder coating
- copolymer
- march
- methacrylate
- monomers
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000000843 powder Substances 0.000 title abstract 3
- 239000008199 coating composition Substances 0.000 title abstract 2
- 229920001187 thermosetting polymer Polymers 0.000 title abstract 2
- NIXOWILDQLNWCW-UHFFFAOYSA-N acrylic acid group Chemical group C(C=C)(=O)O NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 title 1
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 abstract 3
- 239000000178 monomer Substances 0.000 abstract 3
- OZAIFHULBGXAKX-UHFFFAOYSA-N 2-(2-cyanopropan-2-yldiazenyl)-2-methylpropanenitrile Chemical compound N#CC(C)(C)N=NC(C)(C)C#N OZAIFHULBGXAKX-UHFFFAOYSA-N 0.000 abstract 2
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 abstract 2
- CERQOIWHTDAKMF-UHFFFAOYSA-M Methacrylate Chemical compound CC(=C)C([O-])=O CERQOIWHTDAKMF-UHFFFAOYSA-M 0.000 abstract 2
- 229910000831 Steel Inorganic materials 0.000 abstract 2
- PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 abstract 2
- 239000002253 acid Substances 0.000 abstract 2
- 150000007513 acids Chemical class 0.000 abstract 2
- 229920006243 acrylic copolymer Polymers 0.000 abstract 2
- 125000001931 aliphatic group Chemical group 0.000 abstract 2
- 239000011248 coating agent Substances 0.000 abstract 2
- 238000000576 coating method Methods 0.000 abstract 2
- 229920001577 copolymer Polymers 0.000 abstract 2
- 239000010959 steel Substances 0.000 abstract 2
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 abstract 2
- 229920002554 vinyl polymer Polymers 0.000 abstract 2
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 abstract 1
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 abstract 1
- 239000004372 Polyvinyl alcohol Substances 0.000 abstract 1
- 235000021355 Stearic acid Nutrition 0.000 abstract 1
- 229910010413 TiO 2 Inorganic materials 0.000 abstract 1
- XTXRWKRVRITETP-UHFFFAOYSA-N Vinyl acetate Chemical compound CC(=O)OC=C XTXRWKRVRITETP-UHFFFAOYSA-N 0.000 abstract 1
- 125000000217 alkyl group Chemical group 0.000 abstract 1
- 150000008064 anhydrides Chemical class 0.000 abstract 1
- 239000006229 carbon black Substances 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- MOTZDAYCYVMXPC-UHFFFAOYSA-N dodecyl hydrogen sulfate Chemical compound CCCCCCCCCCCCOS(O)(=O)=O MOTZDAYCYVMXPC-UHFFFAOYSA-N 0.000 abstract 1
- 239000000945 filler Substances 0.000 abstract 1
- 230000009477 glass transition Effects 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- QIQXTHQIDYTFRH-UHFFFAOYSA-N octadecanoic acid Chemical compound CCCCCCCCCCCCCCCCCC(O)=O QIQXTHQIDYTFRH-UHFFFAOYSA-N 0.000 abstract 1
- OQCDKBAXFALNLD-UHFFFAOYSA-N octadecanoic acid Natural products CCCCCCCC(C)CCCCCCCCC(O)=O OQCDKBAXFALNLD-UHFFFAOYSA-N 0.000 abstract 1
- RPQRDASANLAFCM-UHFFFAOYSA-N oxiran-2-ylmethyl prop-2-enoate Chemical compound C=CC(=O)OCC1CO1 RPQRDASANLAFCM-UHFFFAOYSA-N 0.000 abstract 1
- 239000003973 paint Substances 0.000 abstract 1
- 239000000049 pigment Substances 0.000 abstract 1
- 229920002451 polyvinyl alcohol Polymers 0.000 abstract 1
- 229920006395 saturated elastomer Polymers 0.000 abstract 1
- 239000008117 stearic acid Substances 0.000 abstract 1
- 239000000126 substance Substances 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 1
- LRXTYHSAJDENHV-UHFFFAOYSA-H zinc phosphate Chemical compound [Zn+2].[Zn+2].[Zn+2].[O-]P([O-])([O-])=O.[O-]P([O-])([O-])=O LRXTYHSAJDENHV-UHFFFAOYSA-H 0.000 abstract 1
- 229940077935 zinc phosphate Drugs 0.000 abstract 1
- 229910000165 zinc phosphate Inorganic materials 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/18—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing
- C08G59/20—Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups ; e.g. general methods of curing characterised by the epoxy compounds used
- C08G59/32—Epoxy compounds containing three or more epoxy groups
- C08G59/3209—Epoxy compounds containing three or more epoxy groups obtained by polymerisation of unsaturated mono-epoxy compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Paints Or Removers (AREA)
- Epoxy Resins (AREA)
Abstract
1338204 Acrylic copolymer composition KANSAI PAINT CO Ltd 23 March 1972 [26 March 1971] 13558/72 Heading C3B A thermosetting powder coating composition comprises (A) an acrylic copolymer and one or more of (B) aliphatic dibasic acids HOOC-RCOOH or anhydrides or substances yielding such acids under curing conditions, where R is a saturated or unsaturated C 4-11 aliphatic hydrocarbon group. (A) has glass transition temperature 40-70‹ C and is a copolymer of (1) 70-95% wt. of at least one acrylate or methacrylate CH 2 =CR<SP>1</SP>-COOR<SP>2</SP> (a) where R<SP>1</SP> is H or CH 3 and R<SP>2</SP> is C 1-17 alkyl, which may be mixed with up to 1À5 parts by wt., based on (a), of other vinyl monomers, and (2) 5-30% wt. of glycidyl acrylate and/or methacrylate. The vinyl monomer may be styrene, acrylonitrile, vinyl acetate or toluene. (A) and (B) may be melt blended and then cooled and pulverized to particle-size 20-150 Ám. Also present may be pigments, fillers, or levelling agents, e.g. TiO 2 , iron oxide, carbon black. Copolymer (A) may be made by heating the monomers with water, Na lauryl sulphate, Na 2 SO 4 , polyvinyl alcohol, azobisisobutyronitrile, stearic acid. Use.-Coating cars, steel furniture, and fences, e.g. by electrostatic powder coating of zincphosphate-treated steel, followed by baking at 150-220‹ C.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP1806271A JPS5312531B1 (en) | 1971-03-26 | 1971-03-26 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1338204A true GB1338204A (en) | 1973-11-21 |
Family
ID=11961186
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1355872A Expired GB1338204A (en) | 1971-03-26 | 1972-03-23 | Thermosetting acrylic powder coating compositions |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JPS5312531B1 (en) |
| DE (1) | DE2214650B2 (en) |
| FR (1) | FR2136051A5 (en) |
| GB (1) | GB1338204A (en) |
| NL (1) | NL7203950A (en) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5663240A (en) * | 1993-11-01 | 1997-09-02 | Ppg Industries, Inc. | Powder coating of epoxy-functional acrylic copolymer and polycarboxylic acid |
| US5965213A (en) * | 1996-04-04 | 1999-10-12 | Basf Coatings Ag | Aqueous dispersions of a transparent powder coating |
| US6159556A (en) * | 1995-05-19 | 2000-12-12 | Basf Coatings Ag | Process for preparing an aqueous powder coating dispersion and using the same |
| US6509096B1 (en) | 1999-05-03 | 2003-01-21 | Basf Coatings Ac | Low-yellowing aqueous clear powder coating dispersions, method of making the dispersions, and process for producing clearcoat finishes with the dispersions |
| US6630211B1 (en) | 1999-02-25 | 2003-10-07 | Basf Coatings Ag | Utilization of tricyclodecandimethanol for producing multilayer lacquers |
| US6747091B1 (en) | 1999-02-25 | 2004-06-08 | Basf Coatings Ag | Powder-slurry that can be hardened by actinic radiation or optionally by thermal means, method for producing said slurry and use of the same |
| US7122595B1 (en) | 1999-02-25 | 2006-10-17 | Basf Coatings Ag | Powder-slurry that can be hardened by actinic radiation or by thermal means, method for producing said slurry and use of the same |
| US7148295B2 (en) | 2003-06-26 | 2006-12-12 | Bayer Materialscience Ag | Carboxy-functional crosslinkers for epoxy-functional powder-lacquer binding agents |
| US7329717B2 (en) | 2003-06-26 | 2008-02-12 | Bayer Materialscience Ag | Polyisocyanate-modified polycarboxylic acids |
| US10829588B2 (en) | 2015-07-09 | 2020-11-10 | Basf Se | Curable compositions |
| US11807724B2 (en) | 2018-01-20 | 2023-11-07 | Gregor Luthe | Mechanochemical process for producing valuable products free from persistent organic pollutants and other organohalogen compounds from waste comprising plastics and plastic laminates |
Families Citing this family (28)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3857905A (en) * | 1973-02-02 | 1974-12-31 | Minnesota Mining & Mfg | Powdered coating composition of unsaturated aycidyl polymer containing a sulfur terminating group, dicarboxylic acid, polester and polyacrylate |
| DE2540921C2 (en) * | 1975-09-13 | 1981-11-26 | Hoechst Ag, 6000 Frankfurt | Thermosetting, powdery coating agent from a mixture of copolymers containing glycidyl groups and hardening agents. Process for its production and its use |
| JPS58150092A (en) * | 1982-03-02 | 1983-09-06 | Sanyo Electric Co Ltd | Enclosed type rotary compressor |
| DE58909320D1 (en) * | 1988-09-06 | 1995-08-03 | Lonza Ag | Process for the preparation of 5-alkyltetramic acids. |
| DE19652813A1 (en) | 1996-12-18 | 1998-06-25 | Basf Coatings Ag | Aqueous powder coating dispersion |
| DE19727892A1 (en) | 1997-07-01 | 1999-01-07 | Basf Coatings Ag | Aqueous powder coating dispersion, process for its preparation and use of the powder coating dispersion obtained |
| DE19735540C1 (en) | 1997-08-16 | 1999-04-01 | Basf Coatings Ag | Multilayered substrate and process for its manufacture |
| DE19744561A1 (en) * | 1997-09-20 | 1999-04-01 | Basf Coatings Ag | Powder-form paint for automobile body |
| DE19752759A1 (en) | 1997-11-28 | 1999-07-01 | Basf Coatings Ag | Triboelectrically chargeable powder coatings |
| EP1084199A2 (en) | 1998-04-01 | 2001-03-21 | BASF Coatings AG | Non-ionically stabilized transparent powder-coating dispersion |
| DE19835206A1 (en) | 1998-08-04 | 2000-02-17 | Basf Coatings Ag | Aqueous powder clearcoat dispersion |
| DE19846650A1 (en) | 1998-10-09 | 2000-04-13 | Basf Coatings Ag | Aqueous powder paint slurry, useful for the coating of motor vehicle bodies, comprises a hydroxyl group binding agent and a polyisocyanate crosslinking agent with stabilized surface isocyanate groups. |
| DE19850211C1 (en) | 1998-10-31 | 2000-11-23 | Basf Coatings Ag | Powder coatings and their use in the manufacture of low-noise powder coatings |
| DE10126651A1 (en) | 2001-06-01 | 2002-12-12 | Basf Coatings Ag | Use of copolymers with diphenylethylene units as emulsifiers for the production of powder slurry and coating powder for use in coating materials, adhesives and sealants, e.g. for painting cars |
| DE10353638A1 (en) | 2003-11-17 | 2005-06-23 | Basf Coatings Ag | Pseudoplastic, aqueous dispersions, process for their preparation and their use |
| DE102008016050A1 (en) | 2007-12-24 | 2009-06-25 | Voest-Alpine Stahl Gmbh | Primer useful for coating metal substrates comprises binder, additives, pigments, fillers and corrosion inhibitors, crosslinker and solvent |
| EP2582740B1 (en) | 2010-06-15 | 2015-03-25 | Basf Se | Use of cyclic carbonates in epoxy resin compositions |
| US8586653B2 (en) | 2011-09-19 | 2013-11-19 | Basf Se | Curing of epoxy resin compositions comprising cyclic carbonates using mixtures of amino hardeners |
| WO2013041398A1 (en) | 2011-09-19 | 2013-03-28 | Basf Se | Curing of epoxy resin compositions comprising cyclic carbonates using mixtures of amino hardeners |
| US8877837B2 (en) | 2011-09-21 | 2014-11-04 | Basf Se | Curing of epoxy resin compositions comprising cyclic carbonates using mixtures of amino hardeners and catalysts |
| WO2013041425A1 (en) | 2011-09-21 | 2013-03-28 | Basf Se | Curing of epoxy resin compositions comprising cyclic carbonates using mixtures of amino hardeners and catalysts |
| DK2764033T3 (en) | 2011-10-04 | 2015-09-14 | Basf Se | EPOXIDHARPIKSSAMMENSÆTNINGER CONTAINING A 2-OXO [1,3] dioxolane |
| US20160208042A1 (en) | 2013-10-01 | 2016-07-21 | Basf Se | Multi-component epoxy resin composition |
| DE102014006519A1 (en) | 2014-05-03 | 2015-11-05 | Smart Material Printing B.V. | Use of magnetic and / or magnetizable, polymeric micro- and / or nanocomposites for the production of complex, magnetic and / or magnetizable molded parts using additive manufacturers |
| WO2016116259A1 (en) | 2015-01-21 | 2016-07-28 | Smartmaterialprinting B.V. | Biocidal treatment of objects and water-containing cleaning and body-care products with polyoxometalate microparticles and/or nanoparticles |
| DE102015000814A1 (en) | 2015-01-21 | 2016-07-21 | Smart Material Printing B.V. | Biocide equipment of articles with polyoxometalate micro and / or nanoparticles |
| WO2016169858A1 (en) | 2015-04-23 | 2016-10-27 | Basf Se | Cyclic carbonates |
| DE102018003906A1 (en) | 2018-05-07 | 2019-11-07 | Smart Material Printing | Use of polyoxometalates against the infestation of eukaryotic cultures, viral cultures and microorganism populations by mollicutes and mollicutene-inhibiting and killing polyoxometalate-containing substances and processes |
-
1971
- 1971-03-26 JP JP1806271A patent/JPS5312531B1/ja active Pending
-
1972
- 1972-03-23 GB GB1355872A patent/GB1338204A/en not_active Expired
- 1972-03-24 NL NL7203950A patent/NL7203950A/xx unknown
- 1972-03-24 FR FR7210333A patent/FR2136051A5/fr not_active Expired
- 1972-03-25 DE DE19722214650 patent/DE2214650B2/en not_active Withdrawn
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5663240A (en) * | 1993-11-01 | 1997-09-02 | Ppg Industries, Inc. | Powder coating of epoxy-functional acrylic copolymer and polycarboxylic acid |
| US6159556A (en) * | 1995-05-19 | 2000-12-12 | Basf Coatings Ag | Process for preparing an aqueous powder coating dispersion and using the same |
| US5965213A (en) * | 1996-04-04 | 1999-10-12 | Basf Coatings Ag | Aqueous dispersions of a transparent powder coating |
| US6630211B1 (en) | 1999-02-25 | 2003-10-07 | Basf Coatings Ag | Utilization of tricyclodecandimethanol for producing multilayer lacquers |
| US6747091B1 (en) | 1999-02-25 | 2004-06-08 | Basf Coatings Ag | Powder-slurry that can be hardened by actinic radiation or optionally by thermal means, method for producing said slurry and use of the same |
| US7122595B1 (en) | 1999-02-25 | 2006-10-17 | Basf Coatings Ag | Powder-slurry that can be hardened by actinic radiation or by thermal means, method for producing said slurry and use of the same |
| US6509096B1 (en) | 1999-05-03 | 2003-01-21 | Basf Coatings Ac | Low-yellowing aqueous clear powder coating dispersions, method of making the dispersions, and process for producing clearcoat finishes with the dispersions |
| US6770329B2 (en) | 1999-05-03 | 2004-08-03 | Basf Coatings Ag | Low-yellowing aqueous clear powder coating dispersions, method of making the dispersions, and process for producing clearcoat finishes with the dispersions |
| US7148295B2 (en) | 2003-06-26 | 2006-12-12 | Bayer Materialscience Ag | Carboxy-functional crosslinkers for epoxy-functional powder-lacquer binding agents |
| US7329717B2 (en) | 2003-06-26 | 2008-02-12 | Bayer Materialscience Ag | Polyisocyanate-modified polycarboxylic acids |
| US10829588B2 (en) | 2015-07-09 | 2020-11-10 | Basf Se | Curable compositions |
| US11807724B2 (en) | 2018-01-20 | 2023-11-07 | Gregor Luthe | Mechanochemical process for producing valuable products free from persistent organic pollutants and other organohalogen compounds from waste comprising plastics and plastic laminates |
Also Published As
| Publication number | Publication date |
|---|---|
| DE2214650B2 (en) | 1975-04-30 |
| NL7203950A (en) | 1972-09-28 |
| FR2136051A5 (en) | 1972-12-22 |
| DE2214650A1 (en) | 1972-10-12 |
| JPS5312531B1 (en) | 1978-05-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PCNP | Patent ceased through non-payment of renewal fee |