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GB1322701A - Apparatus for converting liquid fatty nitriles to amines - Google Patents

Apparatus for converting liquid fatty nitriles to amines

Info

Publication number
GB1322701A
GB1322701A GB1322701DA GB1322701A GB 1322701 A GB1322701 A GB 1322701A GB 1322701D A GB1322701D A GB 1322701DA GB 1322701 A GB1322701 A GB 1322701A
Authority
GB
United Kingdom
Prior art keywords
coolant
valve
line
reactants
surge drum
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WADDLETON N
Original Assignee
WADDLETON N
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by WADDLETON N filed Critical WADDLETON N
Publication of GB1322701A publication Critical patent/GB1322701A/en
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
    • C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
    • B01J2219/00076—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements inside the reactor
    • B01J2219/00083—Coils

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

1322701 Temperature control of exothermic reactions N WADDLETON (ANDERSON LUEDEKA FITCH EVEN & TABIN) 29 June 1970 [1 April 1969] 16930/69 Heading B1X Exothermic reactions are controlled by means of indirect cooling fed from a constant level surge drum, wherein any coolant losses due to evaporation are replenished with fresh coolant. In the particular application of converting fatty nitriles to amines reactants are fed into a reactor 1 via an inlet 6, and stirrer 29 is started. The mixture is first heated by passing steam through coil 31 and any excessive condensate collecting in surge drum 32 is removed via lines 36, 50. Pressure control 66 opens valve 34 to atmosphere during this time. Pump 22 circulates the reactants via line 7, heater 2 and header 21 and when the reactants are at the required temperature the valve 34 is closed and the steam heating stopped by closing valve 55. Hydrogen is then introduced into the reactor via sparger 15 and NH 3 through line 16. Heat emitted is controlled by passing a coolant, e.g. H 2 O through the surge drum 32, line 36 and the coil 31. Any coolant vaporising is vented via pressure relief line 33 whereupon the level in drum 32 drops. The level controller 35 then causes valve 40 to open to admit make up coolant. Upon completion of the reaction valves 34, 51 are opened and valve 52 is closed so that the mixture may be further cooled.
GB1322701D 1969-04-01 1969-04-01 Apparatus for converting liquid fatty nitriles to amines Expired GB1322701A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB1693069 1969-04-01

Publications (1)

Publication Number Publication Date
GB1322701A true GB1322701A (en) 1973-07-11

Family

ID=10086226

Family Applications (1)

Application Number Title Priority Date Filing Date
GB1322701D Expired GB1322701A (en) 1969-04-01 1969-04-01 Apparatus for converting liquid fatty nitriles to amines

Country Status (1)

Country Link
GB (1) GB1322701A (en)

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0070797A3 (en) * 1981-07-16 1984-02-22 Buss Ag Installation using a loop-type reactor and process by which a liquid educt is subjected to a chemical reaction in a circulatory manner
FR2632718A1 (en) * 1988-06-08 1989-12-15 Chinoin Gyogyszer Es Vegyeszet DEVICE FOR IMPLEMENTING THERMAL METHODS
DE3826320A1 (en) * 1988-08-03 1990-02-08 Henkel Kgaa Method for guiding a reaction proceeding at elevated temperature and apparatus for producing thermally sensitive products at elevated temperatures
US5110508A (en) * 1988-04-22 1992-05-05 Henkel Kommanditgesellschaft Auf Aktien Process and apparatus for making a heat-sensitive material
CN108273452A (en) * 2018-01-30 2018-07-13 浙江工业大学 A kind of grease epoxidation reactor
WO2018177400A1 (en) * 2017-03-31 2018-10-04 北京中科诚毅科技发展有限公司 Temperature and pressure control method for hydrogenation process, design method therefor and use thereof
CN114917853A (en) * 2022-05-11 2022-08-19 顶峰油脂化工(泰兴)有限公司 Method for intermittent hydrogenation reaction

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0070797A3 (en) * 1981-07-16 1984-02-22 Buss Ag Installation using a loop-type reactor and process by which a liquid educt is subjected to a chemical reaction in a circulatory manner
US5110508A (en) * 1988-04-22 1992-05-05 Henkel Kommanditgesellschaft Auf Aktien Process and apparatus for making a heat-sensitive material
FR2632718A1 (en) * 1988-06-08 1989-12-15 Chinoin Gyogyszer Es Vegyeszet DEVICE FOR IMPLEMENTING THERMAL METHODS
DE3826320A1 (en) * 1988-08-03 1990-02-08 Henkel Kgaa Method for guiding a reaction proceeding at elevated temperature and apparatus for producing thermally sensitive products at elevated temperatures
WO2018177400A1 (en) * 2017-03-31 2018-10-04 北京中科诚毅科技发展有限公司 Temperature and pressure control method for hydrogenation process, design method therefor and use thereof
CN108273452A (en) * 2018-01-30 2018-07-13 浙江工业大学 A kind of grease epoxidation reactor
CN108273452B (en) * 2018-01-30 2023-09-26 浙江工业大学 A grease epoxidation reactor
CN114917853A (en) * 2022-05-11 2022-08-19 顶峰油脂化工(泰兴)有限公司 Method for intermittent hydrogenation reaction

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Legal Events

Date Code Title Description
PS Patent sealed
PLNP Patent lapsed through nonpayment of renewal fees