GB1318609A - Method of protecting metal parts - Google Patents
Method of protecting metal partsInfo
- Publication number
- GB1318609A GB1318609A GB4927070A GB4927070A GB1318609A GB 1318609 A GB1318609 A GB 1318609A GB 4927070 A GB4927070 A GB 4927070A GB 4927070 A GB4927070 A GB 4927070A GB 1318609 A GB1318609 A GB 1318609A
- Authority
- GB
- United Kingdom
- Prior art keywords
- seconds
- hours
- cathodically
- anodically
- coating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 229910052751 metal Inorganic materials 0.000 title abstract 5
- 239000002184 metal Substances 0.000 title abstract 5
- 238000000576 coating method Methods 0.000 abstract 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 239000011651 chromium Substances 0.000 abstract 3
- 239000011248 coating agent Substances 0.000 abstract 3
- 101100283604 Caenorhabditis elegans pigk-1 gene Proteins 0.000 abstract 2
- WPYMKLBDIGXBTP-UHFFFAOYSA-N benzoic acid Chemical compound OC(=O)C1=CC=CC=C1 WPYMKLBDIGXBTP-UHFFFAOYSA-N 0.000 abstract 2
- 229910052804 chromium Inorganic materials 0.000 abstract 2
- 239000005711 Benzoic acid Substances 0.000 abstract 1
- 229910021555 Chromium Chloride Inorganic materials 0.000 abstract 1
- XFXPMWWXUTWYJX-UHFFFAOYSA-N Cyanide Chemical compound N#[C-] XFXPMWWXUTWYJX-UHFFFAOYSA-N 0.000 abstract 1
- 229910000604 Ferrochrome Inorganic materials 0.000 abstract 1
- 229910017709 Ni Co Inorganic materials 0.000 abstract 1
- 229910003267 Ni-Co Inorganic materials 0.000 abstract 1
- 229910003262 Ni‐Co Inorganic materials 0.000 abstract 1
- 229910000831 Steel Inorganic materials 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 abstract 1
- 229910000148 ammonium phosphate Inorganic materials 0.000 abstract 1
- ZRIUUUJAJJNDSS-UHFFFAOYSA-N ammonium phosphates Chemical compound [NH4+].[NH4+].[NH4+].[O-]P([O-])([O-])=O ZRIUUUJAJJNDSS-UHFFFAOYSA-N 0.000 abstract 1
- 235000010233 benzoic acid Nutrition 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- QSWDMMVNRMROPK-UHFFFAOYSA-K chromium(3+) trichloride Chemical compound [Cl-].[Cl-].[Cl-].[Cr+3] QSWDMMVNRMROPK-UHFFFAOYSA-K 0.000 abstract 1
- BNIILDVGGAEEIG-UHFFFAOYSA-L disodium hydrogen phosphate Chemical compound [Na+].[Na+].OP([O-])([O-])=O BNIILDVGGAEEIG-UHFFFAOYSA-L 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 150000002739 metals Chemical class 0.000 abstract 1
- 230000001681 protective effect Effects 0.000 abstract 1
- 235000011121 sodium hydroxide Nutrition 0.000 abstract 1
- 239000010959 steel Substances 0.000 abstract 1
- 239000000758 substrate Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C10/00—Solid state diffusion of only metal elements or silicon into metallic material surfaces
- C23C10/28—Solid state diffusion of only metal elements or silicon into metallic material surfaces using solids, e.g. powders, pastes
- C23C10/34—Embedding in a powder mixture, i.e. pack cementation
- C23C10/52—Embedding in a powder mixture, i.e. pack cementation more than one element being diffused in one step
- C23C10/54—Diffusion of at least chromium
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C10/00—Solid state diffusion of only metal elements or silicon into metallic material surfaces
- C23C10/28—Solid state diffusion of only metal elements or silicon into metallic material surfaces using solids, e.g. powders, pastes
- C23C10/34—Embedding in a powder mixture, i.e. pack cementation
- C23C10/52—Embedding in a powder mixture, i.e. pack cementation more than one element being diffused in one step
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C10/00—Solid state diffusion of only metal elements or silicon into metallic material surfaces
- C23C10/28—Solid state diffusion of only metal elements or silicon into metallic material surfaces using solids, e.g. powders, pastes
- C23C10/34—Embedding in a powder mixture, i.e. pack cementation
- C23C10/52—Embedding in a powder mixture, i.e. pack cementation more than one element being diffused in one step
- C23C10/54—Diffusion of at least chromium
- C23C10/56—Diffusion of at least chromium and at least aluminium
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Solid-Phase Diffusion Into Metallic Material Surfaces (AREA)
- Other Surface Treatments For Metallic Materials (AREA)
- Electroplating Methods And Accessories (AREA)
Abstract
1318609 Coating with metals DEUTSCHE EDELSTAHLWERKE AG 16 Oct 1970 [3 Nov 1969] 49270/70 Headings C7B and C7F A metal part of e.g. steel, Ni, Co or Ni-Co is coated with Cr and/or Si and a Pt group metal The coatings are completely diffused e.g. by heating in a protective atmosphere or vacuum at 900 to 1250 C. The coating may also contain Al. Either the Cr or Si or the Pt group metal may be applied first or both may be applied simultaneously. In an example the surface is wet blasted and degreased in a cyanide bath cathodically for 5 seconds and anodically for 15 seconds, pickled in H 2 SO 4 at a current density of 2 amps/dm<SP>2</SP> for 3 seconds, anodically and then for 2 seconds cathodically, and then immersed in caustic soda for 5 seconds cathodically and 15 seconds anodically. Pt is then electrolytically deposited from a bath consisting of (g/l):- 13 of hexachloroplatinic acid, 45 of triammonium phosphate, 240 of disodium hydrogen phosphate. The coating is then heated for 2 hours at 260 C and 3 hours at 450 C. The surface is then chromised in a pack at 1100 C comprising 12À5% Cr, 12À5% ferrochrome, 75% alumina and 0À2% chromium chloride. In another example Pd is electro-plated from a bath comprising (g/1.) 5 of Pd Cl 2 , 55 of (NH 4 ) 2 HPO 4 , 240 of Na 2 HPO 4 and 3À5 of benzoic acid. The coated surface is then heated at 260C for 2 hours and 450 C for 3 hours. The Pd-surface is then chromized as in the previous example. The substrates may also be plated with RU 4 or Rh.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691955203 DE1955203B2 (en) | 1969-11-03 | 1969-11-03 | SURFACE PROTECTION PROCESS FOR METALLIC OBJECTS |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1318609A true GB1318609A (en) | 1973-05-31 |
Family
ID=5749992
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB4927070A Expired GB1318609A (en) | 1969-11-03 | 1970-10-16 | Method of protecting metal parts |
Country Status (12)
| Country | Link |
|---|---|
| JP (1) | JPS4834292B1 (en) |
| AU (1) | AU2180270A (en) |
| BE (1) | BE757636A (en) |
| CH (1) | CH552071A (en) |
| DE (1) | DE1955203B2 (en) |
| FR (1) | FR2071753A5 (en) |
| GB (1) | GB1318609A (en) |
| IL (1) | IL35551A0 (en) |
| NL (1) | NL7015945A (en) |
| NO (1) | NO126807B (en) |
| SE (1) | SE358419B (en) |
| ZA (1) | ZA707104B (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2129017A (en) * | 1982-11-01 | 1984-05-10 | Turbine Components Corp | Forming protective diffusion layer on nickel cobalt and iron base alloys |
| GB2130249A (en) * | 1982-11-19 | 1984-05-31 | Turbine Components Corp | Diffusion coating of metals |
| US5645893A (en) * | 1994-12-24 | 1997-07-08 | Rolls-Royce Plc | Thermal barrier coating for a superalloy article and method of application |
| US5652044A (en) * | 1992-03-05 | 1997-07-29 | Rolls Royce Plc | Coated article |
| US5667663A (en) * | 1994-12-24 | 1997-09-16 | Chromalloy United Kingdom Limited | Method of applying a thermal barrier coating to a superalloy article and a thermal barrier coating |
| WO1999042633A1 (en) * | 1998-02-23 | 1999-08-26 | MTU MOTOREN- UND TURBINEN-UNION MüNCHEN GMBH | Method for producing a slip layer which is resistant to corrosion and oxidation |
| EP1088907A1 (en) * | 1999-09-29 | 2001-04-04 | MTU Aero Engines GmbH | Method for producing a plating for a metal component |
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1350855A (en) * | 1971-07-06 | 1974-04-24 | Chromalloy American Corp | Rhodium containing superalloy coatings |
| US3999956A (en) * | 1975-02-21 | 1976-12-28 | Chromalloy American Corporation | Platinum-rhodium-containing high temperature alloy coating |
| AU604462B2 (en) * | 1986-07-28 | 1990-12-20 | Furukawa Electric Co. Ltd., The | Fin of heat exchanger and method of making it |
| FR2638174B1 (en) * | 1988-10-26 | 1991-01-18 | Onera (Off Nat Aerospatiale) | METHOD FOR PROTECTING THE SURFACE OF METAL WORKPIECES AGAINST CORROSION AT HIGH TEMPERATURE, AND WORKPIECE TREATED BY THIS PROCESS |
| EP0567755B1 (en) * | 1992-04-29 | 1996-09-04 | WALBAR INC. (a Delaware Corporation) | Improved diffusion coating process and products |
| FR2757181B1 (en) * | 1996-12-12 | 1999-02-12 | Snecma | PROCESS FOR PRODUCING A HIGH EFFICIENCY PROTECTIVE COATING AGAINST HIGH TEMPERATURE CORROSION FOR SUPERALLOYS, PROTECTIVE COATING OBTAINED BY THIS PROCESS AND PARTS PROTECTED BY THIS COATING |
-
0
- BE BE757636D patent/BE757636A/en unknown
-
1969
- 1969-11-03 DE DE19691955203 patent/DE1955203B2/en active Pending
-
1970
- 1970-08-11 CH CH1206470A patent/CH552071A/en not_active IP Right Cessation
- 1970-10-09 FR FR7036518A patent/FR2071753A5/fr not_active Expired
- 1970-10-16 GB GB4927070A patent/GB1318609A/en not_active Expired
- 1970-10-19 ZA ZA707104A patent/ZA707104B/en unknown
- 1970-10-28 IL IL35551A patent/IL35551A0/en unknown
- 1970-10-30 NL NL7015945A patent/NL7015945A/xx unknown
- 1970-11-02 NO NO04160/70*[A patent/NO126807B/no unknown
- 1970-11-02 SE SE14735/70A patent/SE358419B/xx unknown
- 1970-11-03 AU AU21802/70A patent/AU2180270A/en not_active Expired
- 1970-11-04 JP JP45097091A patent/JPS4834292B1/ja active Pending
Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB2129017A (en) * | 1982-11-01 | 1984-05-10 | Turbine Components Corp | Forming protective diffusion layer on nickel cobalt and iron base alloys |
| GB2130249A (en) * | 1982-11-19 | 1984-05-31 | Turbine Components Corp | Diffusion coating of metals |
| AT381508B (en) * | 1982-11-19 | 1986-10-27 | Turbine Components Corp | METHOD FOR PRODUCING A PROTECTIVE DIFFUSION LAYER ON NICKEL, COBALT AND IRON ALLOYS |
| US5652044A (en) * | 1992-03-05 | 1997-07-29 | Rolls Royce Plc | Coated article |
| US5846605A (en) * | 1992-03-05 | 1998-12-08 | Rolls-Royce Plc | Coated Article |
| US5645893A (en) * | 1994-12-24 | 1997-07-08 | Rolls-Royce Plc | Thermal barrier coating for a superalloy article and method of application |
| US5667663A (en) * | 1994-12-24 | 1997-09-16 | Chromalloy United Kingdom Limited | Method of applying a thermal barrier coating to a superalloy article and a thermal barrier coating |
| US5763107A (en) * | 1994-12-24 | 1998-06-09 | Rolls-Royce Plc | Thermal barrier coating for a superalloy article |
| US5981091A (en) * | 1994-12-24 | 1999-11-09 | Rolls-Royce Plc | Article including thermal barrier coated superalloy substrate |
| WO1999042633A1 (en) * | 1998-02-23 | 1999-08-26 | MTU MOTOREN- UND TURBINEN-UNION MüNCHEN GMBH | Method for producing a slip layer which is resistant to corrosion and oxidation |
| US6440499B1 (en) | 1998-02-23 | 2002-08-27 | Mtu Aero Engines Gmbh | Method for producing a slip layer which is resistant to corrosion and oxidation |
| EP1088907A1 (en) * | 1999-09-29 | 2001-04-04 | MTU Aero Engines GmbH | Method for producing a plating for a metal component |
Also Published As
| Publication number | Publication date |
|---|---|
| DE1955203B2 (en) | 1971-11-25 |
| DE1955203A1 (en) | 1971-05-13 |
| FR2071753A5 (en) | 1971-09-17 |
| JPS4834292B1 (en) | 1973-10-20 |
| BE757636A (en) | 1971-04-01 |
| SE358419B (en) | 1973-07-30 |
| AU2180270A (en) | 1972-05-04 |
| IL35551A0 (en) | 1970-12-24 |
| CH552071A (en) | 1974-07-31 |
| NO126807B (en) | 1973-03-26 |
| NL7015945A (en) | 1971-05-05 |
| ZA707104B (en) | 1971-08-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed [section 19, patents act 1949] | ||
| PE20 | Patent expired after termination of 20 years |