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GB1398196A - Pyrazoline compounds having insecticidal activity - Google Patents

Pyrazoline compounds having insecticidal activity

Info

Publication number
GB1398196A
GB1398196A GB583273A GB583273A GB1398196A GB 1398196 A GB1398196 A GB 1398196A GB 583273 A GB583273 A GB 583273A GB 583273 A GB583273 A GB 583273A GB 1398196 A GB1398196 A GB 1398196A
Authority
GB
United Kingdom
Prior art keywords
alkyl
atom
formula
halogen
phenyl group
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB583273A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Koninklijke Philips NV
Original Assignee
Philips Gloeilampenfabrieken NV
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Philips Gloeilampenfabrieken NV filed Critical Philips Gloeilampenfabrieken NV
Publication of GB1398196A publication Critical patent/GB1398196A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D231/00Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/12Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with only hydrogen atoms, hydrocarbon or substituted hydrocarbon radicals, directly attached to ring carbon atoms
    • AHUMAN NECESSITIES
    • A01AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01NPRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N47/00Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid
    • A01N47/08Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom not being member of a ring and having no bond to a carbon or hydrogen atom, e.g. derivatives of carbonic acid the carbon atom having one or more single bonds to nitrogen atoms
    • A01N47/28Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N<
    • A01N47/38Ureas or thioureas containing the groups >N—CO—N< or >N—CS—N< containing the group >N—CO—N< where at least one nitrogen atom is part of a heterocyclic ring; Thio analogues thereof
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C45/00Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
    • C07C45/61Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
    • C07C45/67Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
    • C07C45/68Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
    • C07C45/72Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups
    • C07C45/74Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction of compounds containing >C = O groups with the same or other compounds containing >C = O groups combined with dehydration
    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07CACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C49/00Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
    • C07C49/76Ketones containing a keto group bound to a six-membered aromatic ring
    • C07C49/80Ketones containing a keto group bound to a six-membered aromatic ring containing halogen
    • C07C49/813Ketones containing a keto group bound to a six-membered aromatic ring containing halogen polycyclic

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

1398196 1-Carbamoyl-#<SP>2</SP>-pyrazoline derivatives PHILIPS GLOEILAMPENFABRIEKEN NV 6 Feb 1973 [9 Feb 1972] 5832/73 Heading C2C Novel compounds have the Formula I wherein A is a phenyl group optionally carrying 1 or 2 substituents selected from halogen, -CN, C 1-4 alkyl, C 1-4 haloalkyl, cycloalkyl, C 1-4 alkoxy, C 1-4 alkylthio, -NHR, -NRR (each R is individually C 1-4 alkyl) and heterocyclic radicals attached to the phenyl group by a N ring atom and optionally containing a second hetero atom selected from S, O and N, or A is a thienyl or pyridyl group optionally substituted by a halogen atom or a C 1-4 alkyl group; B is a hydrogen atom or a phenyl group optionally carrying 1 to 3 substituents selected from halogen, C 1-4 alkoxy, C 1-4 alkyl, C 1-4 haloalkyl, cycloalkyl, C 1-4 alkylthio, C 1-4 alkylsulphonyl, C 1-4 dioxyalkylene, -NHR, -NRR (each R is individually C 1-4 alkyl) and heterocyclic radicals attached to the phenyl group by a N ring atom and optionally containing a second hetero atom, or B is a furyl, pyrryl, thienyl or pyridyl group optionally substituted by a halogen atom or a C 1-4 alkyl group; R 1 is halogen, C 1-4 alkoxy, C 1-4 alkyl, C 1-4 haloalkyl, cycloalkyl, C 1-4 alkylthio, C 1-4 alkylsulphonyl, -CN, -NO 2 or an amino group substituted by 1 or 2 alkyl groups which together with the common nitrogen atom can form a ring optionally containing a second hetero atom; and n is 0, 1 or 2, with the proviso that when A represents a phenyl group containing 2 substituents these do not occupy the 2,6 positions on the benzene ring and also that (R 1 ) n is not a 2,6- disubstitution. The #<SP>2</SP>-pyrazolines of Formula I are prepared by reacting a compound of Formula II with a compound of Formula III preferably in the presence of a solvent (e.g. an ether) and a catalyst (e.g. an organic base). Specific examples relate to the preparation of (a) 1 - (3,4 - dichlorophenylcarbamoyl) - 3- phenyl - #<SP>2</SP> - pyrazoline and (2) 1 - (4 - chlorophenylcarbamoyl) - 3 - (4 - chlorophenyl) - 5- (4 - chlorophenyl) - #<SP>2</SP> - pyrazoline but many more pyrazolines are listed with their physical properties. The compounds of Formula I possess biocidal activity.
GB583273A 1972-02-09 1973-02-06 Pyrazoline compounds having insecticidal activity Expired GB1398196A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
NL7201674.A NL158177B (en) 1972-02-09 1972-02-09 METHOD FOR PREPARING INSECTICIDE PREPARATIONS BASED ON UNSATURATED PYRAZOLIDINE DERIVATIVES, SO PREPARED PREPARATIONS, AND METHOD FOR PREPARING UNSATURATED PYRAZOLIDIN DERIVATICIDE DERIVATICIDE.

Publications (1)

Publication Number Publication Date
GB1398196A true GB1398196A (en) 1975-06-18

Family

ID=19815330

Family Applications (1)

Application Number Title Priority Date Filing Date
GB583273A Expired GB1398196A (en) 1972-02-09 1973-02-06 Pyrazoline compounds having insecticidal activity

Country Status (21)

Country Link
JP (1) JPS5419445B2 (en)
AR (1) AR195824A1 (en)
AT (1) AT330791B (en)
BE (1) BE795264A (en)
CA (1) CA974991A (en)
CH (1) CH590846A5 (en)
CS (1) CS193020B2 (en)
DE (1) DE2304584C2 (en)
DK (1) DK136841B (en)
EG (1) EG11009A (en)
ES (1) ES411380A1 (en)
FR (1) FR2171218B1 (en)
GB (1) GB1398196A (en)
IE (1) IE37346B1 (en)
IL (1) IL41472A (en)
IT (1) IT978847B (en)
NL (1) NL158177B (en)
PL (2) PL93536B1 (en)
SE (1) SE410187B (en)
SU (1) SU479295A3 (en)
ZA (1) ZA73576B (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0058424A3 (en) * 1981-02-17 1983-01-19 Nissan Chemical Industries Ltd. Pyrazoline derivatives
GB2166137A (en) * 1984-10-25 1986-04-30 Fmc Corp Pyrazoline insecticides

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
NL158178B (en) * 1974-07-12 1978-10-16 Philips Nv METHOD OF PREPARING INSECTICIDE PREPARATIONS CONTAINING A PYRAZOLINE DERIVATIVE, SO PREPARED PREPARATIONS, AND METHOD OF PREPARING PYRAZOLINE DERIVATIVES WITH INSECTICIDE ACTION.
US4156007A (en) * 1974-07-12 1979-05-22 U.S. Philips Corporation Pyrazoline compounds
NL183400C (en) * 1976-01-09 1988-10-17 Duphar Int Res METHOD FOR PREPARING AN INSECTICIDE PREPARATION CONTAINING A PYRAZOLINE COMPOUND AND METHOD FOR PREPARING A PYRAZOLINE COMPOUND WITH INSECTICIDE ACTION
US4174393A (en) * 1975-07-09 1979-11-13 Duphar International Research B.V. 1,3,4-Substituted pyrazoline derivatives
US4214090A (en) * 1976-01-14 1980-07-22 Commonwealth Scientific And Industrial Research Organization Fungicidal carboxamidopyrazoles
US4134987A (en) * 1976-01-14 1979-01-16 Huppatz John L Compounds and compositions
JPS57209275A (en) * 1981-06-19 1982-12-22 Nissan Chem Ind Ltd Novel pyrazoline derivative, its preparation, and vermin-controlling agent containing said derivative as active component
US4663341A (en) 1984-02-16 1987-05-05 Rohm And Haas Company Insecticidal n-aryl-3-aryl-4,5-dihydro-1h-pyrazole-1-carboxamides
EP0513046B1 (en) * 1990-01-31 1997-07-09 E.I. Du Pont De Nemours And Company Arthropodicidal pyrazolines, pyrazolidines and hydrazines
DE4117076A1 (en) * 1991-05-25 1992-11-26 Bayer Ag SUBSTITUTED 4-HETARYL PYRAZOLINE
JPH05112555A (en) * 1991-10-18 1993-05-07 Nippon Bayeragrochem Kk Selective insecticidal pyrazolines
JPH05112556A (en) * 1991-10-18 1993-05-07 Nippon Bayeragrochem Kk Insecticidal pyrazolines

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP0058424A3 (en) * 1981-02-17 1983-01-19 Nissan Chemical Industries Ltd. Pyrazoline derivatives
GB2166137A (en) * 1984-10-25 1986-04-30 Fmc Corp Pyrazoline insecticides

Also Published As

Publication number Publication date
IE37346L (en) 1973-08-09
CS193020B2 (en) 1979-09-17
PL98035B1 (en) 1978-04-29
PL93536B1 (en) 1977-06-30
AT330791B (en) 1976-07-26
DE2304584A1 (en) 1973-08-16
DK136841C (en) 1978-05-16
DE2304584C2 (en) 1983-08-11
FR2171218A1 (en) 1973-09-21
SE410187B (en) 1979-10-01
JPS5419445B2 (en) 1979-07-16
AR195824A1 (en) 1973-11-09
BE795264A (en) 1973-08-09
ATA103673A (en) 1975-10-15
SU479295A3 (en) 1975-07-30
CH590846A5 (en) 1977-08-31
IL41472A0 (en) 1973-04-30
NL7201674A (en) 1973-08-13
CA974991A (en) 1975-09-23
JPS4887028A (en) 1973-11-16
IL41472A (en) 1976-08-31
IT978847B (en) 1974-09-20
AU5179773A (en) 1974-08-08
ES411380A1 (en) 1976-07-16
EG11009A (en) 1976-10-31
IE37346B1 (en) 1977-07-06
ZA73576B (en) 1974-08-28
FR2171218B1 (en) 1978-09-08
NL158177B (en) 1978-10-16
DK136841B (en) 1977-12-05

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
732 Registration of transactions, instruments or events in the register (sect. 32/1977)
PCNP Patent ceased through non-payment of renewal fee