GB1201311A - Improvements in or relating to liquid-liquid separation - Google Patents
Improvements in or relating to liquid-liquid separationInfo
- Publication number
- GB1201311A GB1201311A GB1732967A GB1732967A GB1201311A GB 1201311 A GB1201311 A GB 1201311A GB 1732967 A GB1732967 A GB 1732967A GB 1732967 A GB1732967 A GB 1732967A GB 1201311 A GB1201311 A GB 1201311A
- Authority
- GB
- United Kingdom
- Prior art keywords
- tube
- liquid
- probes
- added
- liquids
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000007788 liquid Substances 0.000 title abstract 8
- 238000000926 separation method Methods 0.000 title 1
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 abstract 4
- 229910052802 copper Inorganic materials 0.000 abstract 4
- 239000010949 copper Substances 0.000 abstract 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 abstract 3
- 239000000523 sample Substances 0.000 abstract 3
- 229910052790 beryllium Inorganic materials 0.000 abstract 2
- ATBAMAFKBVZNFJ-UHFFFAOYSA-N beryllium atom Chemical compound [Be] ATBAMAFKBVZNFJ-UHFFFAOYSA-N 0.000 abstract 2
- LMBWSYZSUOEYSN-UHFFFAOYSA-N diethyldithiocarbamic acid Chemical compound CCN(CC)C(S)=S LMBWSYZSUOEYSN-UHFFFAOYSA-N 0.000 abstract 2
- 229950004394 ditiocarb Drugs 0.000 abstract 2
- 239000012074 organic phase Substances 0.000 abstract 2
- 239000000243 solution Substances 0.000 abstract 2
- 239000007864 aqueous solution Substances 0.000 abstract 1
- 239000007853 buffer solution Substances 0.000 abstract 1
- 229910052804 chromium Inorganic materials 0.000 abstract 1
- 239000011521 glass Substances 0.000 abstract 1
- 229910052751 metal Inorganic materials 0.000 abstract 1
- 239000002184 metal Substances 0.000 abstract 1
- 239000000203 mixture Substances 0.000 abstract 1
- 229910052759 nickel Inorganic materials 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 238000002798 spectrophotometry method Methods 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D17/00—Separation of liquids, not provided for elsewhere, e.g. by thermal diffusion
- B01D17/02—Separation of non-miscible liquids
- B01D17/0208—Separation of non-miscible liquids by sedimentation
- B01D17/0214—Separation of non-miscible liquids by sedimentation with removal of one of the phases
Landscapes
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
Abstract
1,201,311. Separating liquids; analysing beryllium for copper traces; contacting liquids. UNITED KINGDOM ATOMIC ENERGY AUTHORITY. 8 April, 1968 ,[14 April, 1967], No. 17329/67. Headings BID, B1F and B1X. An aqueous liquid and an organic solvent, of different densities and electrical conductivities, are mixed together in glass container 1 and allowed to separate by settling, after which the heavier liquid is drained off through rubber tube 14 until the interface passes probes 12, whereupon the change in resistance between the probes causes a solenoid-operated pinch valve to close the tube. The control circuit (Fig. 2, not shown) can be set so that the valve closes in response to an increase or decrease in resistance. The valve is spring-loaded towards the closed position and the current through probes 2 is automatically cut off when the valve closes. The lighter liquid is drawn off through adjustable tube 6. In liquid contacting, an aqueous solution of Cu, Ni or Cr is admitted through tube 3 and an ion-extracting solution of chloroform containing sodium diethyldithiocarbamate is added through tube 4, and the liquids are mixed by stirrer 18 and allowed to settle out. In analysing beryllium for traces (5 p.p.m.) of copper, the metal is dissolved in HC1 to form a solution to which buffer solution is added to bring the pH to 4.5. The mixture is contacted with chloroform containing sodium diethyldithiocarbamate as described above, further volumes of the organic phase being added and the mixing and settling repeated after draining off the first quantity. The various volumes of organic phase are mixed together and their copper content is measured by spectrophotometry.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1732967A GB1201311A (en) | 1967-04-14 | 1967-04-14 | Improvements in or relating to liquid-liquid separation |
| FR1562446D FR1562446A (en) | 1967-04-14 | 1968-04-12 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB1732967A GB1201311A (en) | 1967-04-14 | 1967-04-14 | Improvements in or relating to liquid-liquid separation |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1201311A true GB1201311A (en) | 1970-08-05 |
Family
ID=10093268
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB1732967A Expired GB1201311A (en) | 1967-04-14 | 1967-04-14 | Improvements in or relating to liquid-liquid separation |
Country Status (2)
| Country | Link |
|---|---|
| FR (1) | FR1562446A (en) |
| GB (1) | GB1201311A (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2446386A1 (en) * | 1979-01-10 | 1980-08-08 | Nissan Motor | FUEL FILTER COMPRISING MEANS OF DETECTING THE WATER LEVEL FOR AN INTERNAL COMBUSTION ENGINE |
| EP1241129A1 (en) * | 2001-03-12 | 2002-09-18 | Salvatore Italiano | Draining device for fuel tank sumps |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2421147A1 (en) * | 1978-03-31 | 1979-10-26 | Rampignon Jack | APPARATUS FOR THE PURIFICATION OF SOLVENT-LOADED WATER |
-
1967
- 1967-04-14 GB GB1732967A patent/GB1201311A/en not_active Expired
-
1968
- 1968-04-12 FR FR1562446D patent/FR1562446A/fr not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2446386A1 (en) * | 1979-01-10 | 1980-08-08 | Nissan Motor | FUEL FILTER COMPRISING MEANS OF DETECTING THE WATER LEVEL FOR AN INTERNAL COMBUSTION ENGINE |
| EP1241129A1 (en) * | 2001-03-12 | 2002-09-18 | Salvatore Italiano | Draining device for fuel tank sumps |
Also Published As
| Publication number | Publication date |
|---|---|
| FR1562446A (en) | 1969-04-04 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PLNP | Patent lapsed through nonpayment of renewal fees |