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GB1278974A - Improvements in or relating to the liquefication of natural gas - Google Patents

Improvements in or relating to the liquefication of natural gas

Info

Publication number
GB1278974A
GB1278974A GB52889/69A GB5288969A GB1278974A GB 1278974 A GB1278974 A GB 1278974A GB 52889/69 A GB52889/69 A GB 52889/69A GB 5288969 A GB5288969 A GB 5288969A GB 1278974 A GB1278974 A GB 1278974A
Authority
GB
United Kingdom
Prior art keywords
separator
gas
expanded
passed
liquid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB52889/69A
Inventor
Wolfgang Forg
Volker Etzbach
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Linde GmbH
Original Assignee
Linde GmbH
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from DE19681806879 external-priority patent/DE1806879C3/en
Application filed by Linde GmbH filed Critical Linde GmbH
Publication of GB1278974A publication Critical patent/GB1278974A/en
Expired legal-status Critical Current

Links

Classifications

    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/0002Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the fluid to be liquefied
    • F25J1/0022Hydrocarbons, e.g. natural gas
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/003Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production
    • F25J1/0032Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. "internal refrigeration"
    • F25J1/004Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. "internal refrigeration" by flash gas recovery
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/003Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production
    • F25J1/0032Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. "internal refrigeration"
    • F25J1/0045Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using the feed stream itself or separated fractions from it, i.e. "internal refrigeration" by vaporising a liquid return stream
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/003Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production
    • F25J1/0047Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using an "external" refrigerant stream in a closed vapor compression cycle
    • F25J1/0052Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using an "external" refrigerant stream in a closed vapor compression cycle by vaporising a liquid refrigerant stream
    • F25J1/0055Processes or apparatus for liquefying or solidifying gases or gaseous mixtures characterised by the kind of cold generation within the liquefaction unit for compensating heat leaks and liquid production using an "external" refrigerant stream in a closed vapor compression cycle by vaporising a liquid refrigerant stream originating from an incorporated cascade
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/02Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process
    • F25J1/0201Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process using only internal refrigeration means, i.e. without external refrigeration
    • F25J1/0202Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process using only internal refrigeration means, i.e. without external refrigeration in a quasi-closed internal refrigeration loop
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J1/00Processes or apparatus for liquefying or solidifying gases or gaseous mixtures
    • F25J1/02Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process
    • F25J1/0211Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process using a multi-component refrigerant [MCR] fluid in a closed vapor compression cycle
    • F25J1/0212Processes or apparatus for liquefying or solidifying gases or gaseous mixtures requiring the use of refrigeration, e.g. of helium or hydrogen ; Details and kind of the refrigeration system used; Integration with other units or processes; Controlling aspects of the process using a multi-component refrigerant [MCR] fluid in a closed vapor compression cycle as a single flow MCR cycle
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2220/00Processes or apparatus involving steps for the removal of impurities
    • F25J2220/60Separating impurities from natural gas, e.g. mercury, cyclic hydrocarbons
    • F25J2220/62Separating low boiling components, e.g. He, H2, N2, Air
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2220/00Processes or apparatus involving steps for the removal of impurities
    • F25J2220/60Separating impurities from natural gas, e.g. mercury, cyclic hydrocarbons
    • F25J2220/64Separating heavy hydrocarbons, e.g. NGL, LPG, C4+ hydrocarbons or heavy condensates in general
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2230/00Processes or apparatus involving steps for increasing the pressure of gaseous process streams
    • F25J2230/30Compression of the feed stream
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2245/00Processes or apparatus involving steps for recycling of process streams
    • F25J2245/90Processes or apparatus involving steps for recycling of process streams the recycled stream being boil-off gas from storage
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2290/00Other details not covered by groups F25J2200/00 - F25J2280/00
    • F25J2290/62Details of storing a fluid in a tank

Landscapes

  • Engineering & Computer Science (AREA)
  • Physics & Mathematics (AREA)
  • Mechanical Engineering (AREA)
  • Thermal Sciences (AREA)
  • General Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Separation By Low-Temperature Treatments (AREA)

Abstract

1278974 Liquefying gases LINDE AG 29 Oct 1969 [4 Nov 1968] 52889/69 Heading F4P In a process for liquefying natural gas circulating medium is compressed in a multi-stage compressor, cooled, partially condensed and separated between successive stages, the gas phase being passed to the next compression stage and the liquid phase passed in heat exchange with the gas to be liquefied, expanded and returned to the first compression stage. In a circuit having two compression stages the circulating medium is fed to a first compressor 2, partially liquefied in a cooler 3, and the liquid collected in a separator 4 passed through a heat exchanger 5, expanded through a valve 6, vaporized in the heat exchanger 5 and returned via a line 1 to the compressor 2. Gas from the separator 4 is mixed with gas to be liquefied in line 7, fed to a compressor 8, cooler. 9, and the partially liquefied gas passed into a separator 10. The liquid collected is sub-cooled in exchanger 5, expanded through valve 11 and recycled via line 1 as before; part of the sub-cooled liquid is expanded through a valve 13 into a line 27 to a gasometer. Gas from separator 10 is partly condensed in exchanger 5, and both resulting phases collected in separator 14 and passed through a heat exchanger 15. The sub-cooled liquid is expanded and recycled as before, and the gas is again partly condensed, collected in separator 16 and both phases passed through an exchanger 17. The sub-cooled liquid is recycled as before and the partially liquefied gas phase collected in a separator 18, both phases being cooled in heat exchanger 19. The liquid resulting in separator 20 is united with liquid from separator 18, passed through a heat exchanger 21, expanded and recycled. Vapour from separator 20 is liquefied in exchangers 21 and 23 and expanded through valve 24 into a storage tank 25; part of the flow is expanded through valve 26 into the line 27 which passes back through exchangers 23, 21, 19, 17, 15 and 5 to the gasometer. Vapour from tank 25 is fed via a line 28, a cold gas blower 29 into line 27. In another embodiment (Fig. 2, not shown) the gas to be liquefied is not added to the circulating medium, and is passed through the heat exchangers in a separate circuit.
GB52889/69A 1968-11-04 1969-10-29 Improvements in or relating to the liquefication of natural gas Expired GB1278974A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE19681806879 DE1806879C3 (en) 1968-11-04 Process for liquefying natural gas

Publications (1)

Publication Number Publication Date
GB1278974A true GB1278974A (en) 1972-06-21

Family

ID=5712332

Family Applications (1)

Application Number Title Priority Date Filing Date
GB52889/69A Expired GB1278974A (en) 1968-11-04 1969-10-29 Improvements in or relating to the liquefication of natural gas

Country Status (4)

Country Link
US (1) US3702063A (en)
JP (1) JPS5440512B1 (en)
FR (1) FR2022550B1 (en)
GB (1) GB1278974A (en)

Families Citing this family (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3884044A (en) * 1970-02-09 1975-05-20 Exxon Research Engineering Co Mixed refrigerant cycle
US3884045A (en) * 1970-02-09 1975-05-20 Exxon Research Engineering Co Mixed refrigerant cycle
US3914949A (en) * 1971-02-19 1975-10-28 Chicago Bridge & Iron Co Method and apparatus for liquefying gases
DE2163096B2 (en) * 1971-12-18 1974-02-14 Gutehoffnungshuette Sterkrade Ag, 4200 Oberhausen Process for reheating a compressed gas stream above the dew point
US3874184A (en) * 1973-05-24 1975-04-01 Phillips Petroleum Co Removing nitrogen from and subsequently liquefying natural gas stream
FR2237147B1 (en) * 1973-07-03 1976-04-30 Teal Procedes Air Liquide Tech
DE2628007A1 (en) * 1976-06-23 1978-01-05 Heinrich Krieger PROCESS AND SYSTEM FOR GENERATING COLD WITH AT LEAST ONE INCORPORATED CASCADE CIRCUIT
US4325231A (en) * 1976-06-23 1982-04-20 Heinrich Krieger Cascade cooling arrangement
US4707170A (en) * 1986-07-23 1987-11-17 Air Products And Chemicals, Inc. Staged multicomponent refrigerant cycle for a process for recovery of C+ hydrocarbons
MY122625A (en) * 1999-12-17 2006-04-29 Exxonmobil Upstream Res Co Process for making pressurized liquefied natural gas from pressured natural gas using expansion cooling
NO312736B1 (en) * 2000-02-10 2002-06-24 Sinvent As Method and plant for cooling and possibly liquefying a product gas
EP2021712A2 (en) * 2006-05-15 2009-02-11 Shell Internationale Research Maatschappij B.V. Method and apparatus for liquefying a hydrocarbon stream
US20070283718A1 (en) * 2006-06-08 2007-12-13 Hulsey Kevin H Lng system with optimized heat exchanger configuration
US10539363B2 (en) 2008-02-14 2020-01-21 Shell Oil Company Method and apparatus for cooling a hydrocarbon stream
FR2944096B1 (en) * 2009-04-07 2012-04-27 Ass Pour La Rech Et Le Dev De Methodes Et Processus Indutriels Armines METHOD AND REFRIGERATING SYSTEM FOR RECOVERING METHANE COLOR WITH REFRIGERATED FLUIDS
GB2470062A (en) * 2009-05-08 2010-11-10 Corac Group Plc Production and Distribution of Natural Gas
DE102011013345A1 (en) * 2011-03-08 2012-09-13 Linde Aktiengesellschaft refrigeration plant
CN102564057A (en) * 2011-12-19 2012-07-11 中国海洋石油总公司 Propane pre-cooling mixed refrigerant liquefaction system applied to base-load type natural gas liquefaction factory
CN102654346A (en) * 2012-05-22 2012-09-05 中国海洋石油总公司 Propane pre-cooling double-mixing refrigerant parallel-connection liquefaction system
FR3039080B1 (en) 2015-07-23 2019-05-17 L'air Liquide, Societe Anonyme Pour L'etude Et L'exploitation Des Procedes Georges Claude METHOD OF PURIFYING HYDROCARBON-RICH GAS
EP3162870A1 (en) 2015-10-27 2017-05-03 Linde Aktiengesellschaft Low-temperature mixed-refrigerant for hydrogen precooling in large scale
FR3052241A1 (en) * 2016-06-02 2017-12-08 L'air Liquide Sa Pour L'etude Et L'exploitation Des Procedes Georges Claude PROCESS FOR PURIFYING NATURAL GAS AND LIQUEFACTING CARBON DIOXIDE
EP4450909A1 (en) * 2023-04-21 2024-10-23 Cryocollect Method for liquefying a gas

Family Cites Families (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
GB895094A (en) * 1959-10-21 1962-05-02 Shell Int Research Improvements in or relating to process and apparatus for liquefying natural gas
FR86485E (en) * 1961-06-01 1966-02-18 Air Liquide Process for cooling a gas mixture at low temperature
US3364685A (en) * 1965-03-31 1968-01-23 Cie Francaise D Etudes Et De C Method and apparatus for the cooling and low temperature liquefaction of gaseous mixtures
FR1516728A (en) * 1965-03-31 1968-02-05 Cie Francaise D Etudes Et De C Method and apparatus for cooling and low temperature liquefaction of gas mixtures
GB1135871A (en) * 1965-06-29 1968-12-04 Air Prod & Chem Liquefaction of natural gas
US3548606A (en) * 1968-07-08 1970-12-22 Phillips Petroleum Co Serial incremental refrigerant expansion for gas liquefaction

Also Published As

Publication number Publication date
FR2022550B1 (en) 1973-12-07
US3702063A (en) 1972-11-07
DE1806879A1 (en) 1970-05-27
JPS5440512B1 (en) 1979-12-04
FR2022550A1 (en) 1970-07-31
DE1806879B2 (en) 1975-10-30

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Legal Events

Date Code Title Description
PS Patent sealed [section 19, patents act 1949]
PCNP Patent ceased through non-payment of renewal fee