GB1277668A - Improved method of making glycidyl ethers - Google Patents
Improved method of making glycidyl ethersInfo
- Publication number
- GB1277668A GB1277668A GB6219969A GB6219969A GB1277668A GB 1277668 A GB1277668 A GB 1277668A GB 6219969 A GB6219969 A GB 6219969A GB 6219969 A GB6219969 A GB 6219969A GB 1277668 A GB1277668 A GB 1277668A
- Authority
- GB
- United Kingdom
- Prior art keywords
- water
- epichlorohydrin
- alkaline earth
- alkali metal
- earth metal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- GYZLOYUZLJXAJU-UHFFFAOYSA-N diglycidyl ether Chemical class C1OC1COCC1CO1 GYZLOYUZLJXAJU-UHFFFAOYSA-N 0.000 title abstract 8
- 238000004519 manufacturing process Methods 0.000 title 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 6
- BRLQWZUYTZBJKN-UHFFFAOYSA-N Epichlorohydrin Chemical compound ClCC1CO1 BRLQWZUYTZBJKN-UHFFFAOYSA-N 0.000 abstract 5
- 150000001340 alkali metals Chemical class 0.000 abstract 4
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 abstract 4
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical group [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 229910000272 alkali metal oxide Inorganic materials 0.000 abstract 3
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 abstract 3
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 abstract 2
- PXKLMJQFEQBVLD-UHFFFAOYSA-N bisphenol F Chemical compound C1=CC(O)=CC=C1CC1=CC=C(O)C=C1 PXKLMJQFEQBVLD-UHFFFAOYSA-N 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 2
- GHMLBKRAJCXXBS-UHFFFAOYSA-N resorcinol Chemical compound OC1=CC=CC(O)=C1 GHMLBKRAJCXXBS-UHFFFAOYSA-N 0.000 abstract 2
- DNIAPMSPPWPWGF-GSVOUGTGSA-N (R)-(-)-Propylene glycol Chemical compound C[C@@H](O)CO DNIAPMSPPWPWGF-GSVOUGTGSA-N 0.000 abstract 1
- 229910001514 alkali metal chloride Inorganic materials 0.000 abstract 1
- 229910001617 alkaline earth metal chloride Inorganic materials 0.000 abstract 1
- 239000003849 aromatic solvent Substances 0.000 abstract 1
- 238000010533 azeotropic distillation Methods 0.000 abstract 1
- 239000003795 chemical substances by application Substances 0.000 abstract 1
- 239000000470 constituent Substances 0.000 abstract 1
- MIHINWMALJZIBX-UHFFFAOYSA-N cyclohexa-2,4-dien-1-ol Chemical class OC1CC=CC=C1 MIHINWMALJZIBX-UHFFFAOYSA-N 0.000 abstract 1
- 238000004090 dissolution Methods 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 229920003986 novolac Polymers 0.000 abstract 1
- 238000002360 preparation method Methods 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
- 239000007787 solid Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
- C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
- C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
- C07D303/22—Ethers with hydroxy compounds containing no oxirane rings with monohydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
- C07D303/18—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by etherified hydroxyl radicals
- C07D303/20—Ethers with hydroxy compounds containing no oxirane rings
- C07D303/24—Ethers with hydroxy compounds containing no oxirane rings with polyhydroxy compounds
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G59/00—Polycondensates containing more than one epoxy group per molecule; Macromolecules obtained by polymerising compounds containing more than one epoxy group per molecule using curing agents or catalysts which react with the epoxy groups
- C08G59/02—Polycondensates containing more than one epoxy group per molecule
- C08G59/04—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof
- C08G59/06—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols
- C08G59/063—Polycondensates containing more than one epoxy group per molecule of polyhydroxy compounds with epihalohydrins or precursors thereof of polyhydric phenols with epihalohydrins
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Epoxy Resins (AREA)
- Epoxy Compounds (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CH18969A CH508680A (de) | 1969-01-08 | 1969-01-08 | Verfahren zum Herstellung von Glycidyläthern |
| CH1602569A CH536334A (de) | 1969-01-08 | 1969-10-28 | Verfahren zum Herstellen von Glycidyläthern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1277668A true GB1277668A (en) | 1972-06-14 |
Family
ID=25683815
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB6219969A Expired GB1277668A (en) | 1969-01-08 | 1969-12-22 | Improved method of making glycidyl ethers |
Country Status (8)
| Country | Link |
|---|---|
| JP (1) | JPS5218180B1 (de) |
| AT (1) | AT298805B (de) |
| CH (1) | CH536334A (de) |
| DE (1) | DE1961888C3 (de) |
| FR (1) | FR2027896A1 (de) |
| GB (1) | GB1277668A (de) |
| NL (1) | NL7000133A (de) |
| SE (1) | SE370228B (de) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109553755A (zh) * | 2017-09-27 | 2019-04-02 | 中国石油化工股份有限公司 | 一种降低环氧氯丙烷消耗的双酚a型环氧树脂生产方法 |
| CN110144038A (zh) * | 2019-05-31 | 2019-08-20 | 江苏鑫露化工新材料有限公司 | 一种双酚a二缩水甘油醚型环氧树脂的合成工艺 |
Families Citing this family (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CH551406A (de) * | 1971-04-23 | 1974-07-15 | Reichhold Albert Chemie Ag | Verfahren zum herstellen von glycidylaethern. |
| US3983056A (en) * | 1973-09-27 | 1976-09-28 | Dai Nippon Toryo Co., Ltd. | Aqueous epoxy resin paint composition |
| JPS5558873U (de) * | 1978-10-16 | 1980-04-21 | ||
| JPS55155468U (de) * | 1979-04-24 | 1980-11-08 | ||
| JPS56147874U (de) * | 1980-04-07 | 1981-11-07 | ||
| CA1293837C (en) * | 1986-10-14 | 1991-12-31 | Ha Q. Pham | Preparation of epoxy resins |
| JP6166568B2 (ja) * | 2013-03-28 | 2017-07-19 | 四日市合成株式会社 | エポキシ樹脂組成物、その製造方法、及びエポキシ樹脂硬化物 |
-
1969
- 1969-10-28 CH CH1602569A patent/CH536334A/de unknown
- 1969-12-10 DE DE19691961888 patent/DE1961888C3/de not_active Expired
- 1969-12-15 FR FR6943270A patent/FR2027896A1/fr not_active Withdrawn
- 1969-12-22 GB GB6219969A patent/GB1277668A/en not_active Expired
-
1970
- 1970-01-05 SE SE7270A patent/SE370228B/xx unknown
- 1970-01-05 JP JP1370A patent/JPS5218180B1/ja active Pending
- 1970-01-07 AT AT12570A patent/AT298805B/de not_active IP Right Cessation
- 1970-01-07 NL NL7000133A patent/NL7000133A/xx unknown
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109553755A (zh) * | 2017-09-27 | 2019-04-02 | 中国石油化工股份有限公司 | 一种降低环氧氯丙烷消耗的双酚a型环氧树脂生产方法 |
| CN110144038A (zh) * | 2019-05-31 | 2019-08-20 | 江苏鑫露化工新材料有限公司 | 一种双酚a二缩水甘油醚型环氧树脂的合成工艺 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5218180B1 (de) | 1977-05-20 |
| DE1961888C3 (de) | 1979-03-29 |
| SE370228B (de) | 1974-10-07 |
| AT298805B (de) | 1972-05-25 |
| CH536334A (de) | 1973-04-30 |
| FR2027896A1 (de) | 1970-10-02 |
| DE1961888A1 (de) | 1970-07-09 |
| NL7000133A (de) | 1970-07-10 |
| DE1961888B2 (de) | 1978-08-03 |
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| DE69302768T2 (de) | Verfahren zur Herstellung von Biphenolskelett aufweisenden Epoxyharzen | |
| GB2128185A (en) | Preparation of glycidyl derivatives | |
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| GB1485345A (en) | Process for the manufacture of glycidyl ethers of monohydric or polyhydric phenols which have improved properties | |
| JPS62218411A (ja) | 脂肪族ハライド含量の低い高度化エポキシまたはフエノキシ樹脂の製造方法 | |
| GB1377246A (en) | Process for the manufacture of of glycidyl-ethers | |
| US3023225A (en) | Xchxch | |
| US3041356A (en) | Preparation of epoxy alcohols from epoxy alkanals | |
| US4110354A (en) | Water-soluble epoxy resins and process for their preparation | |
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| JPS57170922A (en) | Preparation of solid epoxy resin |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PS | Patent sealed | ||
| PLNP | Patent lapsed through nonpayment of renewal fees |