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GB1108292A - Process for the defined increase in the molecular weight of finished unsaturated polymerised hydrocarbons - Google Patents

Process for the defined increase in the molecular weight of finished unsaturated polymerised hydrocarbons

Info

Publication number
GB1108292A
GB1108292A GB32404/65A GB3240465A GB1108292A GB 1108292 A GB1108292 A GB 1108292A GB 32404/65 A GB32404/65 A GB 32404/65A GB 3240465 A GB3240465 A GB 3240465A GB 1108292 A GB1108292 A GB 1108292A
Authority
GB
United Kingdom
Prior art keywords
molecular weight
unsaturated
compound
finished
valency
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB32404/65A
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Huels AG
Original Assignee
Chemische Werke Huels AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Chemische Werke Huels AG filed Critical Chemische Werke Huels AG
Publication of GB1108292A publication Critical patent/GB1108292A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08CTREATMENT OR CHEMICAL MODIFICATION OF RUBBERS
    • C08C19/00Chemical modification of rubber

Landscapes

  • Chemical & Material Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Addition Polymer Or Copolymer, Post-Treatments, Or Chemical Modifications (AREA)

Abstract

The molecular weight of finished unsaturated polymerized hydrocarbons is increased by treating an unsaturated anhydrous polymerized hydrocarbon of molecular weight 1000 to 1,000,000 in solution with the catalyst system:- (a) a compound of formula RnMeXy-n where Me is boron, aluminium, gallium, beryllium, magnesium, calcium, zinc, silicon, tin arsenic, antimony, titanium, zirconium, phosphorus, molybdenum, tungsten, bismuth, iron, mercury, cadmium, vanadium, uranium or vanadyl, X is fluorine, chlorine, bromine or iodine, R is hydrogen, alkyl, cycloalkyl, aryl, aralkyl, alkoxy or sulphoxy or a carboxylate anion, y is the valency of Me and n is from 0 to the valency of Me, and (b) a compound of formula RX in which R is halogen, alkyl, alkenyl, cycloalkyl, aryl, aralkyl, acyl, thionyl, sulphuryl, chromyl, vanadinyl, phosphoroxy, thiophosphoric, sulphonic acid, sulphuric acid, arsenoxy, anti-monoxy, titanyl or imide radical or phosphorus, arsenic, sulphur, selenium, vanadium, titanium tin or silicon and X is halogen, the compound (a) and (b) being different and the catalyst component (a) being added in concentrations of 0.01 to 10% with reference to the polymer used, (b) being added in amounts of 0.002 to 2 moles per mole of the catalyst component (a). The polymerized hydrocarbon may be polybutadiene, polyisoprene, copolymers of butadiene or isoprene with mono-olefines, e.g. styrene, butyl rubber, ethylene-propylene copolymers and ethylene-propylene-dicyclopentadiene terpolymers.
GB32404/65A 1964-07-30 1965-07-29 Process for the defined increase in the molecular weight of finished unsaturated polymerised hydrocarbons Expired GB1108292A (en)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEC0033531 1964-07-30

Publications (1)

Publication Number Publication Date
GB1108292A true GB1108292A (en) 1968-04-03

Family

ID=7020875

Family Applications (1)

Application Number Title Priority Date Filing Date
GB32404/65A Expired GB1108292A (en) 1964-07-30 1965-07-29 Process for the defined increase in the molecular weight of finished unsaturated polymerised hydrocarbons

Country Status (5)

Country Link
BE (1) BE667734A (en)
DE (1) DE1495372A1 (en)
FR (1) FR1455243A (en)
GB (1) GB1108292A (en)
NL (1) NL6509916A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101805426A (en) * 2010-04-23 2010-08-18 华东理工大学 Modified butyl rubber

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
IT1030698B (en) * 1974-10-09 1979-04-10 Snam Progetti PROCEDURE FOR IMPROVING THE CHARACTERISTICS OF POLYIDIENIC ELASTOMERS AND MODULATED ELASTOMERS THUS OBTAINED
US4485833A (en) * 1983-06-03 1984-12-04 Phillips Petroleum Company Rubbery conjugated diene polymers terminated with hydrocarbyl phosphites
US4537932A (en) * 1983-06-03 1985-08-27 Phillips Petroleum Company Rubbery conjugated diene polymers terminated with hydrocarbyl phosphites

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101805426A (en) * 2010-04-23 2010-08-18 华东理工大学 Modified butyl rubber
CN101805426B (en) * 2010-04-23 2011-09-28 华东理工大学 Modified butyl rubber

Also Published As

Publication number Publication date
DE1495372A1 (en) 1969-04-10
NL6509916A (en) 1966-01-31
BE667734A (en) 1965-11-16
FR1455243A (en) 1966-04-01

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