GB1026329A - Preparation of pelletized solid materials - Google Patents
Preparation of pelletized solid materialsInfo
- Publication number
- GB1026329A GB1026329A GB3306064A GB3306064A GB1026329A GB 1026329 A GB1026329 A GB 1026329A GB 3306064 A GB3306064 A GB 3306064A GB 3306064 A GB3306064 A GB 3306064A GB 1026329 A GB1026329 A GB 1026329A
- Authority
- GB
- United Kingdom
- Prior art keywords
- pellets
- line
- bed
- particles
- reintroduced
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000011343 solid material Substances 0.000 title 1
- 239000008188 pellet Substances 0.000 abstract 10
- 239000002245 particle Substances 0.000 abstract 8
- 239000000463 material Substances 0.000 abstract 6
- 239000007864 aqueous solution Substances 0.000 abstract 4
- 229910052783 alkali metal Inorganic materials 0.000 abstract 2
- 230000008020 evaporation Effects 0.000 abstract 2
- 238000001704 evaporation Methods 0.000 abstract 2
- 229920006395 saturated elastomer Polymers 0.000 abstract 2
- 238000012216 screening Methods 0.000 abstract 2
- 239000007787 solid Substances 0.000 abstract 2
- 238000005507 spraying Methods 0.000 abstract 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract 2
- UXVMQQNJUSDDNG-UHFFFAOYSA-L Calcium chloride Chemical compound [Cl-].[Cl-].[Ca+2] UXVMQQNJUSDDNG-UHFFFAOYSA-L 0.000 abstract 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 abstract 1
- BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 abstract 1
- 239000003513 alkali Substances 0.000 abstract 1
- 229910001514 alkali metal chloride Inorganic materials 0.000 abstract 1
- -1 alkali metal sulfonates Chemical class 0.000 abstract 1
- 150000001340 alkali metals Chemical class 0.000 abstract 1
- 229910001617 alkaline earth metal chloride Inorganic materials 0.000 abstract 1
- 229910001628 calcium chloride Inorganic materials 0.000 abstract 1
- 239000001110 calcium chloride Substances 0.000 abstract 1
- USIUVYZYUHIAEV-UHFFFAOYSA-N diphenyl ether Chemical class C=1C=CC=CC=1OC1=CC=CC=C1 USIUVYZYUHIAEV-UHFFFAOYSA-N 0.000 abstract 1
- 150000004760 silicates Chemical class 0.000 abstract 1
- FAPWRFPIFSIZLT-UHFFFAOYSA-M sodium chloride Inorganic materials [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 abstract 1
- 239000011780 sodium chloride Substances 0.000 abstract 1
- HCJLVWUMMKIQIM-UHFFFAOYSA-M sodium;2,3,4,5,6-pentachlorophenolate Chemical compound [Na+].[O-]C1=C(Cl)C(Cl)=C(Cl)C(Cl)=C1Cl HCJLVWUMMKIQIM-UHFFFAOYSA-M 0.000 abstract 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/16—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic by suspending the powder material in a gas, e.g. in fluidised beds or as a falling curtain
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C39/00—Compounds having at least one hydroxy or O-metal group bound to a carbon atom of a six-membered aromatic ring
- C07C39/24—Halogenated derivatives
- C07C39/44—Metal derivatives of an hydroxy group bound to a carbon atom of a six-membered aromatic ring
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
Abstract
Pellets of alkali and alkaline earth metal chlorides or silicates, such as sodium or calcium chloride or silicate, are formed by spray coating particles of the material with an aqueous solution thereof in one or more dilute zones in a fluidized bed, said zones being formed by injecting steam into the bed transverse to the flow of circulatory air. As in Fig. 1, particles of the material are fluidized in a vessel 1 by a stream of heated air from heater 6, which passes upwards through screen 10. Steam under pressure, together with a saturated aqueous solution of the material, is injected into the fluidized bed through a bifluid nozzle 1 and forms a dilute zone, as shown, in which the particles are coated, a solid coat being formed by the subsequent evaporation of the water. The pellets thus produced are drawn off through line 18 and elevator 3 to a screening mechanism 4, whence the oversized pellets are crushed at 5 and reintroduced to the bed through line 24, the underized pellets reintroduced through lines 22 and 24, and the pellets of the required size discharged into storage means through line 21. Any particles carried upwards, by the air, pass through line 16 to a cyclone 2 whence they are reintroduced into the bed through line 24.ALSO:Pellets of alkali metal pentachlorophenates such as sodium pentachlorophenate, or of alkali metal sulfonates of alkylated diphenyl oxide, are formed by spray coating particles of the material with an aqueous solution thereof in one or more dilute zones in a fluidized bed, said zones being formed by injecting steam into the bed transverse to the flow of circulatory air. As in Figure 1, particles of the material are fluidized in a vessel 1 by a stream of heated air from heater 6, which passes upwards through screen 10. Steam under pressure, together with a saturated aqueous solution of the material, is injected into the fluidized bed through a bifluid nozzle 1 and forms a dilute zone, as shown, in which the particles are coated, a solid coat being formed by the subsequent evaporation of the water. The pellets thus produced are drawn off through line 18 and elevator 3 to a screening mechanism 4, whence the oversized pellets are crushed at 5 and reintroduced to the bed through line 24, the undersized pellets reintroduced through lines 22 and 24, and the pellets of the required size discharged into storage means through line 21. Any particles carried upwards, by the air, pass through line 16 to a cyclone 2 whence they are reintroduced into the bed through line 24.
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3306064A GB1026329A (en) | 1964-08-13 | 1964-08-13 | Preparation of pelletized solid materials |
| DED45201A DE1265715B (en) | 1964-08-13 | 1964-08-17 | Continuous process for the granulation of water-soluble solids |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB3306064A GB1026329A (en) | 1964-08-13 | 1964-08-13 | Preparation of pelletized solid materials |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1026329A true GB1026329A (en) | 1966-04-20 |
Family
ID=10348017
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB3306064A Expired GB1026329A (en) | 1964-08-13 | 1964-08-13 | Preparation of pelletized solid materials |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB1026329A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2263968A1 (en) * | 1972-12-29 | 1974-07-11 | Basf Ag | PROCESS FOR MANUFACTURING NON-DUSTING OR PRACTICALLY NON-DUSTING COLORANT CORES |
| FR2519562A1 (en) * | 1982-01-09 | 1983-07-18 | Sandoz Sa | PROCESS AND APPARATUS FOR THE PREPARATION OF A DUST-FREE GRANULAR PRODUCT |
| US4804146A (en) * | 1985-05-30 | 1989-02-14 | Alpine Aktiengesellschaft | Method for the continuous production of granulates from a solid in a fluidized bed of material |
| WO1995013864A1 (en) * | 1993-11-17 | 1995-05-26 | Niro Holding A/S | A process and a spray drying apparatus for producing an agglomerated powder |
| EP1426332A1 (en) * | 2002-12-04 | 2004-06-09 | Degussa AG | Process for the preparation of anhydrous alkali metal sulfide |
-
1964
- 1964-08-13 GB GB3306064A patent/GB1026329A/en not_active Expired
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2263968A1 (en) * | 1972-12-29 | 1974-07-11 | Basf Ag | PROCESS FOR MANUFACTURING NON-DUSTING OR PRACTICALLY NON-DUSTING COLORANT CORES |
| FR2519562A1 (en) * | 1982-01-09 | 1983-07-18 | Sandoz Sa | PROCESS AND APPARATUS FOR THE PREPARATION OF A DUST-FREE GRANULAR PRODUCT |
| US4804146A (en) * | 1985-05-30 | 1989-02-14 | Alpine Aktiengesellschaft | Method for the continuous production of granulates from a solid in a fluidized bed of material |
| WO1995013864A1 (en) * | 1993-11-17 | 1995-05-26 | Niro Holding A/S | A process and a spray drying apparatus for producing an agglomerated powder |
| US5632100A (en) * | 1993-11-17 | 1997-05-27 | Niro Holding A/S | Process and a spray drying apparatus for producing an agglomerated powder |
| EP1426332A1 (en) * | 2002-12-04 | 2004-06-09 | Degussa AG | Process for the preparation of anhydrous alkali metal sulfide |
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