GB1024323A - Improvements in the manufacture of organic esters of dipropylene glycol - Google Patents
Improvements in the manufacture of organic esters of dipropylene glycolInfo
- Publication number
- GB1024323A GB1024323A GB185062A GB185062A GB1024323A GB 1024323 A GB1024323 A GB 1024323A GB 185062 A GB185062 A GB 185062A GB 185062 A GB185062 A GB 185062A GB 1024323 A GB1024323 A GB 1024323A
- Authority
- GB
- United Kingdom
- Prior art keywords
- tin
- dipropylene glycol
- manufacture
- organic esters
- triphosphide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 title abstract 2
- 238000004519 manufacturing process Methods 0.000 title abstract 2
- 150000002895 organic esters Chemical class 0.000 title 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 abstract 5
- 229910021626 Tin(II) chloride Inorganic materials 0.000 abstract 2
- 230000032050 esterification Effects 0.000 abstract 2
- 238000005886 esterification reaction Methods 0.000 abstract 2
- OQBLGYCUQGDOOR-UHFFFAOYSA-L 1,3,2$l^{2}-dioxastannolane-4,5-dione Chemical group O=C1O[Sn]OC1=O OQBLGYCUQGDOOR-UHFFFAOYSA-L 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 abstract 1
- 150000002148 esters Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 150000007524 organic acids Chemical class 0.000 abstract 1
- 235000005985 organic acids Nutrition 0.000 abstract 1
- PZTAGFCBNDBBFZ-UHFFFAOYSA-N tert-butyl 2-(hydroxymethyl)piperidine-1-carboxylate Chemical compound CC(C)(C)OC(=O)N1CCCCC1CO PZTAGFCBNDBBFZ-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C69/00—Esters of carboxylic acids; Esters of carbonic or haloformic acids
- C07C69/76—Esters of carboxylic acids having a carboxyl group bound to a carbon atom of a six-membered aromatic ring
- C07C69/78—Benzoic acid esters
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C67/00—Preparation of carboxylic acid esters
- C07C67/08—Preparation of carboxylic acid esters by reacting carboxylic acids or symmetrical anhydrides with the hydroxy or O-metal group of organic compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Esters of dipropylene glycol with organic acids are prepared by an esterification process in which a tin phosphide or a tin salt is used as an esterification catalyst. Specified tin phosphides are stannous phosphide, tin triphosphide and tetra-tin triphosphide, and a specified tin salt is stannous oxalate. Examples are given of the manufacture of dipropylene glycol dibenzoate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB185062A GB1024323A (en) | 1962-01-18 | 1962-01-18 | Improvements in the manufacture of organic esters of dipropylene glycol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB185062A GB1024323A (en) | 1962-01-18 | 1962-01-18 | Improvements in the manufacture of organic esters of dipropylene glycol |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1024323A true GB1024323A (en) | 1966-03-30 |
Family
ID=9729104
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB185062A Expired GB1024323A (en) | 1962-01-18 | 1962-01-18 | Improvements in the manufacture of organic esters of dipropylene glycol |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB1024323A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106565471A (en) * | 2016-10-29 | 2017-04-19 | 湖北绿色家园材料技术股份有限公司 | Synthetic method of dipropylene glycol dibenzoate |
-
1962
- 1962-01-18 GB GB185062A patent/GB1024323A/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106565471A (en) * | 2016-10-29 | 2017-04-19 | 湖北绿色家园材料技术股份有限公司 | Synthetic method of dipropylene glycol dibenzoate |
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