GB1019131A - Improvements in or relating to the manufacture of 1,2,3,4-tetrachlorobutane - Google Patents
Improvements in or relating to the manufacture of 1,2,3,4-tetrachlorobutaneInfo
- Publication number
- GB1019131A GB1019131A GB2875463A GB2875463A GB1019131A GB 1019131 A GB1019131 A GB 1019131A GB 2875463 A GB2875463 A GB 2875463A GB 2875463 A GB2875463 A GB 2875463A GB 1019131 A GB1019131 A GB 1019131A
- Authority
- GB
- United Kingdom
- Prior art keywords
- tetrachlorobutane
- isomer
- solid
- relating
- manufacture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- IXZVKECRTHXEEW-UHFFFAOYSA-N 1,2,3,4-tetrachlorobutane Chemical compound ClCC(Cl)C(Cl)CCl IXZVKECRTHXEEW-UHFFFAOYSA-N 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title 1
- 239000007787 solid Substances 0.000 abstract 3
- QPFMBZIOSGYJDE-UHFFFAOYSA-N 1,1,2,2-tetrachloroethane Chemical compound ClC(Cl)C(Cl)Cl QPFMBZIOSGYJDE-UHFFFAOYSA-N 0.000 abstract 2
- KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 abstract 2
- VZGDMQKNWNREIO-UHFFFAOYSA-N tetrachloromethane Chemical compound ClC(Cl)(Cl)Cl VZGDMQKNWNREIO-UHFFFAOYSA-N 0.000 abstract 2
- LIFLRQVHKGGNSG-UHFFFAOYSA-N 2,3-dichlorobuta-1,3-diene Chemical compound ClC(=C)C(Cl)=C LIFLRQVHKGGNSG-UHFFFAOYSA-N 0.000 abstract 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 abstract 1
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 229910052801 chlorine Inorganic materials 0.000 abstract 1
- 239000000460 chlorine Substances 0.000 abstract 1
- 238000001914 filtration Methods 0.000 abstract 1
- 239000012442 inert solvent Substances 0.000 abstract 1
- 239000007788 liquid Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 239000000376 reactant Substances 0.000 abstract 1
- 239000002904 solvent Substances 0.000 abstract 1
- XJDNKRIXUMDJCW-UHFFFAOYSA-J titanium tetrachloride Chemical compound Cl[Ti](Cl)(Cl)Cl XJDNKRIXUMDJCW-UHFFFAOYSA-J 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/013—Preparation of halogenated hydrocarbons by addition of halogens
- C07C17/02—Preparation of halogenated hydrocarbons by addition of halogens to unsaturated hydrocarbons
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
1,2,3,4-Tetrachlorobutane having a predominant proportion of the solid isomer is prepared by reacting butadiene with chlorine in a solution of between 0.1 and 20% by weight of titanium tetrachloride in an inert solvent. The solvent may be, for example, carbon tetrachloride or sym-tetrachloroethane but more conveniently is 1,2,3,4-tetrachlorobutane initially added to the reactants and supplemented by the liquid isomer and, if the reaction temperature is above 60 DEG C., the solid isomer product in the molten state. The solid isomer, which may be isolated from the reaction product by filtration, may be dehydrochlorinated to form 2,3-dichlorobutadiene.
Priority Applications (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2875463A GB1019131A (en) | 1963-07-19 | 1963-07-19 | Improvements in or relating to the manufacture of 1,2,3,4-tetrachlorobutane |
| FR982189A FR1401077A (en) | 1963-07-19 | 1964-07-18 | Improved process for preparing 1, 2, 3, 4-tetrachlorobutane |
| DE1964B0077753 DE1237997B (en) | 1963-07-19 | 1964-07-20 | Process for the production of 1, 2, 3, 4-tetrachlorobutane |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB2875463A GB1019131A (en) | 1963-07-19 | 1963-07-19 | Improvements in or relating to the manufacture of 1,2,3,4-tetrachlorobutane |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1019131A true GB1019131A (en) | 1966-02-02 |
Family
ID=30776547
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB2875463A Expired GB1019131A (en) | 1963-07-19 | 1963-07-19 | Improvements in or relating to the manufacture of 1,2,3,4-tetrachlorobutane |
Country Status (3)
| Country | Link |
|---|---|
| DE (1) | DE1237997B (en) |
| FR (1) | FR1401077A (en) |
| GB (1) | GB1019131A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3932544A (en) * | 1974-07-01 | 1976-01-13 | Petro-Tex Chemical Corporation | Process for production of meso-1,2,3,4-tetrachlorobutane |
-
1963
- 1963-07-19 GB GB2875463A patent/GB1019131A/en not_active Expired
-
1964
- 1964-07-18 FR FR982189A patent/FR1401077A/en not_active Expired
- 1964-07-20 DE DE1964B0077753 patent/DE1237997B/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3932544A (en) * | 1974-07-01 | 1976-01-13 | Petro-Tex Chemical Corporation | Process for production of meso-1,2,3,4-tetrachlorobutane |
Also Published As
| Publication number | Publication date |
|---|---|
| FR1401077A (en) | 1965-05-28 |
| DE1237997B (en) | 1967-04-06 |
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