GB1075563A - Derivative of carnitinamide and process for preparing the same - Google Patents
Derivative of carnitinamide and process for preparing the sameInfo
- Publication number
- GB1075563A GB1075563A GB7589/66A GB758966A GB1075563A GB 1075563 A GB1075563 A GB 1075563A GB 7589/66 A GB7589/66 A GB 7589/66A GB 758966 A GB758966 A GB 758966A GB 1075563 A GB1075563 A GB 1075563A
- Authority
- GB
- United Kingdom
- Prior art keywords
- carnitinamide
- camphorate
- treating
- silver
- prepared
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- KWIXGIMKELMNGH-UHFFFAOYSA-O carnitinamide Chemical class C[N+](C)(C)CC(O)CC(N)=O KWIXGIMKELMNGH-UHFFFAOYSA-O 0.000 title 1
- 238000004519 manufacturing process Methods 0.000 title 1
- 230000001476 alcoholic effect Effects 0.000 abstract 3
- LSPHULWDVZXLIL-LDWIPMOCSA-N (?)-Camphoric acid Chemical compound CC1(C)[C@@H](C(O)=O)CC[C@@]1(C)C(O)=O LSPHULWDVZXLIL-LDWIPMOCSA-N 0.000 abstract 2
- KWIXGIMKELMNGH-ZCFIWIBFSA-O (R)-carnitinamide Chemical compound C[N+](C)(C)C[C@H](O)CC(N)=O KWIXGIMKELMNGH-ZCFIWIBFSA-O 0.000 abstract 2
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 abstract 2
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 abstract 2
- 229910052709 silver Inorganic materials 0.000 abstract 2
- 239000004332 silver Substances 0.000 abstract 2
- MVOVUKIZAZCBRK-FYZOBXCZSA-N (R)-carnitinamide chloride Chemical compound [Cl-].C[N+](C)(C)C[C@H](O)CC(N)=O MVOVUKIZAZCBRK-FYZOBXCZSA-N 0.000 abstract 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 abstract 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 1
- 239000000908 ammonium hydroxide Substances 0.000 abstract 1
- 150000001875 compounds Chemical class 0.000 abstract 1
- 238000001640 fractional crystallisation Methods 0.000 abstract 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 abstract 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 229920006395 saturated elastomer Polymers 0.000 abstract 1
- UKHWJBVVWVYFEY-UHFFFAOYSA-M silver;hydroxide Chemical compound [OH-].[Ag+] UKHWJBVVWVYFEY-UHFFFAOYSA-M 0.000 abstract 1
- GGCZERPQGJTIQP-UHFFFAOYSA-N sodium;9,10-dioxoanthracene-2-sulfonic acid Chemical compound [Na+].C1=CC=C2C(=O)C3=CC(S(=O)(=O)O)=CC=C3C(=O)C2=C1 GGCZERPQGJTIQP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/385—Saturated compounds containing a keto group being part of a ring
- C07C49/417—Saturated compounds containing a keto group being part of a ring polycyclic
- C07C49/423—Saturated compounds containing a keto group being part of a ring polycyclic a keto group being part of a condensed ring system
- C07C49/427—Saturated compounds containing a keto group being part of a ring polycyclic a keto group being part of a condensed ring system having two rings
- C07C49/433—Saturated compounds containing a keto group being part of a ring polycyclic a keto group being part of a condensed ring system having two rings the condensed ring system containing seven carbon atoms
- C07C49/437—Camphor; Fenchone
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B28—WORKING CEMENT, CLAY, OR STONE
- B28C—PREPARING CLAY; PRODUCING MIXTURES CONTAINING CLAY OR CEMENTITIOUS MATERIAL, e.g. PLASTER
- B28C7/00—Controlling the operation of apparatus for producing mixtures of clay or cement with other substances; Supplying or proportioning the ingredients for mixing clay or cement with other substances; Discharging the mixture
- B28C7/04—Supplying or proportioning the ingredients
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C237/00—Carboxylic acid amides, the carbon skeleton of the acid part being further substituted by amino groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C49/00—Ketones; Ketenes; Dimeric ketenes; Ketonic chelates
- C07C49/385—Saturated compounds containing a keto group being part of a ring
- C07C49/417—Saturated compounds containing a keto group being part of a ring polycyclic
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Pyridine Compounds (AREA)
Abstract
The novel d-camphorate salt of l-carnitinamide is prepared by fractional crystallization of an alcoholic solution of the d-camphorate of dl-carnitinamide, the desired compound being obtained as the first fraction to crystallize. The d-camphorate of dl-carnitinamide may be prepared by treating a dl-carnitinamide halide in an aqueous or alcoholic medium with silver d-camphorate, or by treating a dl-carnitinamide halide in an aqueous or alcoholic medium with silver hydroxide, and reacting the product with d-camphoric acid. Silver d-camphorate may be prepared by treating ammonium d-camphorate, obtained by reacting d-camphoric acid with ammonium hydroxide, with a water-soluble silver salt. l-Carnitinamide chloride is obtained by treating an ethanolic solution of the d-camphorate of l-carnitinamide with ether saturated with hydrogen chloride.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE9258 | 1965-02-22 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1075563A true GB1075563A (en) | 1967-07-12 |
Family
ID=3839811
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB7589/66A Expired GB1075563A (en) | 1965-02-22 | 1966-02-21 | Derivative of carnitinamide and process for preparing the same |
Country Status (7)
| Country | Link |
|---|---|
| BE (1) | BE660039A (en) |
| CH (1) | CH458320A (en) |
| DE (1) | DE1242222B (en) |
| ES (1) | ES323347A1 (en) |
| FR (1) | FR1466696A (en) |
| GB (1) | GB1075563A (en) |
| NL (1) | NL6601978A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5248601A (en) * | 1986-03-14 | 1993-09-28 | Franco Francalanci | Process for preparing L(-)-carnitine chloride |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IT1156852B (en) * | 1978-07-10 | 1987-02-04 | Sigma Tau Ind Farmaceuti | INDUSTRIAL PROCEDURE FOR THE PREPARATION OF THE L CARNITINAMIDE D'CANFORATE AND THE D CARNITINAMIDE D CANPHORATE AND ITS APPLICATIONS |
| CH658857A5 (en) * | 1984-04-04 | 1986-12-15 | Lonza Ag | OPTICALLY ACTIVE DI (3-CHLORINE-2-OXY-PROPYLTRIMETHYLAMONIUM) TARTRATE. |
| WO1999038505A1 (en) * | 1998-01-30 | 1999-08-05 | The Procter & Gamble Company | Compositions for prevention and treatment of cold and influenza-like symptoms associated with respiratory tract infections |
-
1965
- 1965-02-22 BE BE660039A patent/BE660039A/xx unknown
-
1966
- 1966-01-25 FR FR47094A patent/FR1466696A/en not_active Expired
- 1966-02-03 CH CH150766A patent/CH458320A/en unknown
- 1966-02-09 DE DES101908A patent/DE1242222B/en active Pending
- 1966-02-16 NL NL6601978A patent/NL6601978A/xx unknown
- 1966-02-21 GB GB7589/66A patent/GB1075563A/en not_active Expired
- 1966-02-21 ES ES0323347A patent/ES323347A1/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5248601A (en) * | 1986-03-14 | 1993-09-28 | Franco Francalanci | Process for preparing L(-)-carnitine chloride |
Also Published As
| Publication number | Publication date |
|---|---|
| BE660039A (en) | 1965-08-23 |
| ES323347A1 (en) | 1967-01-01 |
| CH458320A (en) | 1968-06-30 |
| NL6601978A (en) | 1966-08-23 |
| FR1466696A (en) | 1967-01-20 |
| DE1242222B (en) | 1967-06-15 |
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