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GB1070243A - S-triazolopyrimidones, their preparation and compositions containing them - Google Patents

S-triazolopyrimidones, their preparation and compositions containing them

Info

Publication number
GB1070243A
GB1070243A GB2915164A GB2915164A GB1070243A GB 1070243 A GB1070243 A GB 1070243A GB 2915164 A GB2915164 A GB 2915164A GB 2915164 A GB2915164 A GB 2915164A GB 1070243 A GB1070243 A GB 1070243A
Authority
GB
United Kingdom
Prior art keywords
group
substituted
halogen
formula
hydrogen
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB2915164A
Inventor
Robert Geoffrey Willi Spickett
Stanley Harold Biederbe Wright
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Smith Kline and French Laboratories Ltd
Original Assignee
Smith Kline and French Laboratories Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Smith Kline and French Laboratories Ltd filed Critical Smith Kline and French Laboratories Ltd
Priority to GB2915164A priority Critical patent/GB1070243A/en
Publication of GB1070243A publication Critical patent/GB1070243A/en
Expired legal-status Critical Current

Links

Classifications

    • CCHEMISTRY; METALLURGY
    • C07ORGANIC CHEMISTRY
    • C07DHETEROCYCLIC COMPOUNDS
    • C07D487/00Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00
    • C07D487/02Heterocyclic compounds containing nitrogen atoms as the only ring hetero atoms in the condensed system, not provided for by groups C07D451/00 - C07D477/00 in which the condensed system contains two hetero rings
    • C07D487/04Ortho-condensed systems

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Nitrogen Condensed Heterocyclic Rings (AREA)

Abstract

Novel 8-triazolo(1,5-a)pyrimid-5-ones of general formula <FORM:1070243/C2/1> <FORM:1070243/C2/2> wherein, in Formula I, R3 represents an alkyl group or an aralkyl group which may be substituted by halogen, R5 represents hydrogen, or an alkyl group and R6 represents a carbalkoxy group, or R3 represents an alkyl group or an aralkyl group which may be substituted by halogen, and R5 and R6 are halogen, or R3 represents an aralkyl group which may be substituted by halogen, R5 represents hydrogen or alkyl or aryl and R6 represents hydrogen provided that when R3 is an unsubstituted benzyl group, R5 is not hydrogen or methyl, in Formula II R2 represents an aryl group, R4 represents an optionally substituted aralkyl group (where the substituent is halogen), R5 represents hydrogen or an alkyl group and R6 is hydrogen or a carbalkoxy group, or R2 represents hydrogen, R4 represents alkyl or aralkyl which may be substituted by halogen and R5 and R6 represent hydrogen, and novel s-triazolo(1,5-a)-pyrimid-7-ones of formulae <FORM:1070243/C2/3> AND <FORM:1070243/C2/4> wherein in Formula III R3 represents an aralkyl group which may be substituted by halogen, R6 represents a carbalkoxy group and R7 represents hydrogen or an alkyl group, and in Formula IV R2 represents an aryl group, R4 represents an aralkyl group, which may be substituted by halogen, R6 represents a carbalkoxy group and R7 represents hydrogen or an alkyl group, are prepared by condensing in a suitable solvent, e.g. acetic acid, a 3-amino (or aralkylamino)-1,2,4-triazole-5-R2 substituted as defined above, with either a b -keto ester of formula R5-CO-CH-COOR1 wherein R5 and R6 are as defined above and R1 is an alkyl group, or with an alkylalkoxymethylene malonate of formula <FORM:1070243/C2/5> or <FORM:1070243/C2/6> The compounds may also be prepared by N-alkylation or N-aralkylation of a hydroxy-triazolo pyrimidine of formula <FORM:1070243/C2/7> AND <FORM:1070243/C2/8> wherein R2, R5, R6 and R7 are as defined above and 4 - Benzyl - 6 - carbethoxy - 2 - phenyl - s - triazolo(1,5-a)-pyrimid-5-one is prepared by adding a solution of lead tetra-acetate in methylene dichloride to 1-benzyl-2-benzylidenehydrazine-5 -carbethoxypyrimid-6-one in the same solvent. 5 - R2 - substituted 3 - amino (or aralkylamino)-thiazoles, wherein R2 is defined above, and the aralkyl radical may be chloro-substituted, are prepared by cyclization with formic acid of the corresponding substituted aminoguanidines. N - Benzyl - N1 - (benzylideneamino) - guanidine is prepared by refluxing N-amino-N1-benzylguanidine hydriodide and benzaldehyde in ethanol. Pharmaceutical compositions having analgesic and anti-inflammatory activity and which may be administered orally or parenterally and contain a compound of any of the first four general formula above, as the active ingredient.
GB2915164A 1964-07-15 1964-07-15 S-triazolopyrimidones, their preparation and compositions containing them Expired GB1070243A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
GB2915164A GB1070243A (en) 1964-07-15 1964-07-15 S-triazolopyrimidones, their preparation and compositions containing them

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB2915164A GB1070243A (en) 1964-07-15 1964-07-15 S-triazolopyrimidones, their preparation and compositions containing them

Publications (1)

Publication Number Publication Date
GB1070243A true GB1070243A (en) 1967-06-01

Family

ID=10286952

Family Applications (1)

Application Number Title Priority Date Filing Date
GB2915164A Expired GB1070243A (en) 1964-07-15 1964-07-15 S-triazolopyrimidones, their preparation and compositions containing them

Country Status (1)

Country Link
GB (1) GB1070243A (en)

Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2018077A1 (en) * 1968-09-13 1970-05-29 Ici Ltd
FR2424924A1 (en) * 1978-05-05 1979-11-30 Bristol Myers Co NEW AZOLOPYRIMIDINONES, THEIR PRODUCTION PROCESS AND THE MEDICINAL PRODUCT CONTAINING THEM
WO1985002846A1 (en) * 1983-12-27 1985-07-04 Schering Corporation 4,7-DIMETHYL-2-(4-PYRIDINYL)-1,2,4-TRIAZOLO AD1,5-a BDPYRIMIDIN-5(4H)-ONE
GR900100149A (en) * 1989-03-03 1990-07-31 Egyt Gyogyszervegyeszeti Gyar Preparation method of new triazolo-pyrimidine derivatives
EP4161494A4 (en) * 2020-06-02 2024-07-17 KSQ Therapeutics, Inc. NITROGEN-CONTAINING CONDENSED BICYCLIC COMPOUNDS AND THEIR USE AS UBIQUITIN-SPECIFIC PROCESSING PROTEASE 1 (USP1) INHIBITORS

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR2018077A1 (en) * 1968-09-13 1970-05-29 Ici Ltd
FR2424924A1 (en) * 1978-05-05 1979-11-30 Bristol Myers Co NEW AZOLOPYRIMIDINONES, THEIR PRODUCTION PROCESS AND THE MEDICINAL PRODUCT CONTAINING THEM
WO1985002846A1 (en) * 1983-12-27 1985-07-04 Schering Corporation 4,7-DIMETHYL-2-(4-PYRIDINYL)-1,2,4-TRIAZOLO AD1,5-a BDPYRIMIDIN-5(4H)-ONE
EP0147774A3 (en) * 1983-12-27 1985-08-07 Schering Corporation 4,7-dimethyl-2-(4-pyridinyl)-1,2,4-triazolo(1,5-a)pyrimidine-5(4h)-one
US4614743A (en) * 1983-12-27 1986-09-30 Schering Corporation Methods of treating pain and inflammation with 4,7-dimethyl-2-(4-pyridinyl)-1,2,4,-triazolo[1,5-a]pyrimidin-5(4H)-one or the pharmaceutically acceptable salts or solvates thereof
GR900100149A (en) * 1989-03-03 1990-07-31 Egyt Gyogyszervegyeszeti Gyar Preparation method of new triazolo-pyrimidine derivatives
FR2643904A1 (en) * 1989-03-03 1990-09-07 Egyt Gyogyszervegyeszeti Gyar NOVEL TRIAZOLO-PYRIMIDINE DERIVATIVES AND PHARMACEUTICAL COMPOSITIONS CONTAINING SAME
EP4161494A4 (en) * 2020-06-02 2024-07-17 KSQ Therapeutics, Inc. NITROGEN-CONTAINING CONDENSED BICYCLIC COMPOUNDS AND THEIR USE AS UBIQUITIN-SPECIFIC PROCESSING PROTEASE 1 (USP1) INHIBITORS

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