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GB1066492A - Determination of heats of reaction - Google Patents

Determination of heats of reaction

Info

Publication number
GB1066492A
GB1066492A GB23139/64A GB2313964A GB1066492A GB 1066492 A GB1066492 A GB 1066492A GB 23139/64 A GB23139/64 A GB 23139/64A GB 2313964 A GB2313964 A GB 2313964A GB 1066492 A GB1066492 A GB 1066492A
Authority
GB
United Kingdom
Prior art keywords
solid reactant
thermistors
measuring
reaction
test
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
GB23139/64A
Inventor
Aleksander Jerzy Groszek
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Microscal Ltd
Original Assignee
Microscal Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Microscal Ltd filed Critical Microscal Ltd
Priority to GB23139/64A priority Critical patent/GB1066492A/en
Priority to CH176865A priority patent/CH431129A/en
Priority to FR5426A priority patent/FR1424692A/en
Priority to DE19651573263 priority patent/DE1573263A1/en
Priority to US460315A priority patent/US3467501A/en
Publication of GB1066492A publication Critical patent/GB1066492A/en
Expired legal-status Critical Current

Links

Classifications

    • G—PHYSICS
    • G01—MEASURING; TESTING
    • G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N25/00—Investigating or analyzing materials by the use of thermal means
    • G01N25/20—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity
    • G01N25/48—Investigating or analyzing materials by the use of thermal means by investigating the development of heat, i.e. calorimetry, e.g. by measuring specific heat, by measuring thermal conductivity on solution, sorption, or a chemical reaction not involving combustion or catalytic oxidation

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Combustion & Propulsion (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analyzing Materials Using Thermal Means (AREA)

Abstract

1, 066, 492. Measuring heat of reaction electrically. MICROSCAL Ltd. June 2, 1965, [June 4, 1964], No. 23139/64. Addition to 822, 432. Heading G1N. Apparatus for determining the heat of reaction between a fluid and a solid reactant comprises a cell holding the solid reactant and thermistors for measuring the temperature change. As shown (Fig. 5) a granular solid reactant 20 is located in a calorimeter 5, and supported by a wire gauze 7. Suitable heat shielding 9 and insulation 18 is supplied externally. A stream of inert liquid acting as a solvent or carrier for the test fluid is introduced via the funnel 19 shown, and the test liquid via another funnel 19 not shown, or a test gas via inlet 25. The temperature of the solid reactant is measured by thermistors 1, 2 and compared with the ambient temperature measured by thermistors 3, 4, in a D. C. bridge circuit. The ambient temperature may be raised to a steady value by a heating coil 13. The apparatus is calibrated with a further heating coil (not shown) in the solid reactant 20, by measuring the power required to produce the same temperature change. The apparatus may be used for identifying the constituents of a fractionated liquid mixture.
GB23139/64A 1964-06-04 1964-06-04 Determination of heats of reaction Expired GB1066492A (en)

Priority Applications (5)

Application Number Priority Date Filing Date Title
GB23139/64A GB1066492A (en) 1964-06-04 1964-06-04 Determination of heats of reaction
CH176865A CH431129A (en) 1964-06-04 1965-02-10 Method and device for determining the heat of reaction between a fluid and a reagent in the solid phase
FR5426A FR1424692A (en) 1964-06-04 1965-02-12 Method and device for determining the heat of reaction
DE19651573263 DE1573263A1 (en) 1964-06-04 1965-03-16 Method and device for determining the heat of reaction
US460315A US3467501A (en) 1964-06-04 1965-06-01 Calorimeter for the determination of heats of reaction

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
GB23139/64A GB1066492A (en) 1964-06-04 1964-06-04 Determination of heats of reaction

Publications (1)

Publication Number Publication Date
GB1066492A true GB1066492A (en) 1967-04-26

Family

ID=10190783

Family Applications (1)

Application Number Title Priority Date Filing Date
GB23139/64A Expired GB1066492A (en) 1964-06-04 1964-06-04 Determination of heats of reaction

Country Status (4)

Country Link
US (1) US3467501A (en)
CH (1) CH431129A (en)
DE (1) DE1573263A1 (en)
GB (1) GB1066492A (en)

Families Citing this family (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CH543734A (en) * 1971-11-25 1973-10-31 Basf Ag Calorimeter vessel for isothermal calorimetry
US3967492A (en) * 1972-05-09 1976-07-06 Instrumentation Specialties Company Heat of interaction detector
US4021123A (en) * 1974-08-22 1977-05-03 The Perkin-Elmer Corporation Heat exchanger for analysis apparatus
SE381512B (en) * 1974-12-12 1975-12-08 Lkb Produkter Ab CALORIMETRIC METHOD
US4496249A (en) * 1982-09-23 1985-01-29 University Of Florida Method and apparatus for determining relative surface areas of a coated material on a substrate
US4551425A (en) * 1982-09-28 1985-11-05 Trustees Of The University Of Pennsylvania Pyroelectric gas sensor
DE69006016T2 (en) * 1989-02-15 1994-05-11 Microscal Ltd MICROCALORIMETER.
US5067820A (en) * 1990-06-19 1991-11-26 The United States Of America As Represented By The United States Department Of Energy Radionuclide calorimeter system
US7833800B2 (en) * 2002-04-01 2010-11-16 Palo Alto Research Center Incorporated Thermal sensing with bridge circuitry
US7578613B2 (en) * 2006-09-14 2009-08-25 Waters Investments Limited Modulated differential scanning calorimeter solvent loss calibration apparatus and method

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1594593A (en) * 1924-03-01 1926-08-03 Grasselli Chemical Co Apparatus for analyzing by heat of reaction

Also Published As

Publication number Publication date
DE1573263A1 (en) 1969-10-30
US3467501A (en) 1969-09-16
CH431129A (en) 1967-02-28

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