GB1045271A - Improvements in the manufacture of dextrinated lead azide - Google Patents
Improvements in the manufacture of dextrinated lead azideInfo
- Publication number
- GB1045271A GB1045271A GB152862A GB152862A GB1045271A GB 1045271 A GB1045271 A GB 1045271A GB 152862 A GB152862 A GB 152862A GB 152862 A GB152862 A GB 152862A GB 1045271 A GB1045271 A GB 1045271A
- Authority
- GB
- United Kingdom
- Prior art keywords
- salt
- azide
- aqueous solution
- lead
- solution
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 150000001540 azides Chemical class 0.000 title abstract 3
- 238000004519 manufacturing process Methods 0.000 title 1
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 abstract 3
- 239000007864 aqueous solution Substances 0.000 abstract 3
- 229920001353 Dextrin Polymers 0.000 abstract 2
- 239000004375 Dextrin Substances 0.000 abstract 2
- -1 azide salt Chemical class 0.000 abstract 2
- 235000019425 dextrin Nutrition 0.000 abstract 2
- 239000004094 surface-active agent Substances 0.000 abstract 2
- ZMESHQOXZMOOQQ-UHFFFAOYSA-N 1-(naphthalen-1-ylmethyl)naphthalene Chemical compound C1=CC=C2C(CC=3C4=CC=CC=C4C=CC=3)=CC=CC2=C1 ZMESHQOXZMOOQQ-UHFFFAOYSA-N 0.000 abstract 1
- KXDHJXZQYSOELW-UHFFFAOYSA-N Carbamic acid Chemical compound NC(O)=O KXDHJXZQYSOELW-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910052783 alkali metal Inorganic materials 0.000 abstract 1
- 125000000129 anionic group Chemical group 0.000 abstract 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 abstract 1
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 abstract 1
- 239000012266 salt solution Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 159000000000 sodium salts Chemical class 0.000 abstract 1
- 239000000243 solution Substances 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/08—Hydrazoic acid; Azides; Halogen azides
-
- C—CHEMISTRY; METALLURGY
- C06—EXPLOSIVES; MATCHES
- C06B—EXPLOSIVES OR THERMIC COMPOSITIONS; MANUFACTURE THEREOF; USE OF SINGLE SUBSTANCES AS EXPLOSIVES
- C06B35/00—Compositions containing a metal azide
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Dextrinated lead azide in granular free-flowing form is prepared by reacting an aqueous solution of a lead salt with an aqueous solution of an azide salt in the presence of dextrin and an anionic surface active agent, for example a disulphonic acid of dinaphthyl methane or a sodium salt of a naphthalene sulphonic acid/ formaldehyde condensate. Also present may be sodium hydroxide and an alkali metal salt of a hydroxycarboxylic or aminocarboxylic acid. Preferably the lead salt solution and azide solution are added separately to a stirred aqueous solution of dextrin and the surface active agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB152862A GB1045271A (en) | 1962-01-16 | 1962-01-16 | Improvements in the manufacture of dextrinated lead azide |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB152862A GB1045271A (en) | 1962-01-16 | 1962-01-16 | Improvements in the manufacture of dextrinated lead azide |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| GB1045271A true GB1045271A (en) | 1966-10-12 |
Family
ID=9723552
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| GB152862A Expired GB1045271A (en) | 1962-01-16 | 1962-01-16 | Improvements in the manufacture of dextrinated lead azide |
Country Status (1)
| Country | Link |
|---|---|
| GB (1) | GB1045271A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4954329A (en) * | 1988-07-28 | 1990-09-04 | Schweizerische Eidgenossenschaft | Process and apparatus for preparation of finely grained lead azide |
-
1962
- 1962-01-16 GB GB152862A patent/GB1045271A/en not_active Expired
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4954329A (en) * | 1988-07-28 | 1990-09-04 | Schweizerische Eidgenossenschaft | Process and apparatus for preparation of finely grained lead azide |
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