ES8605220A1 - Procedimiento de preparacion de esteres del dietilenglicol - Google Patents
Procedimiento de preparacion de esteres del dietilenglicolInfo
- Publication number
- ES8605220A1 ES8605220A1 ES548226A ES548226A ES8605220A1 ES 8605220 A1 ES8605220 A1 ES 8605220A1 ES 548226 A ES548226 A ES 548226A ES 548226 A ES548226 A ES 548226A ES 8605220 A1 ES8605220 A1 ES 8605220A1
- Authority
- ES
- Spain
- Prior art keywords
- esters
- diethylene glycol
- socl2
- pref
- reaction
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 title abstract 4
- 150000002148 esters Chemical class 0.000 title abstract 2
- FYSNRJHAOHDILO-UHFFFAOYSA-N thionyl chloride Chemical compound ClS(Cl)=O FYSNRJHAOHDILO-UHFFFAOYSA-N 0.000 abstract 4
- 229910006124 SOCl2 Inorganic materials 0.000 abstract 2
- WLJVXDMOQOGPHL-UHFFFAOYSA-N phenylacetic acid Chemical compound OC(=O)CC1=CC=CC=C1 WLJVXDMOQOGPHL-UHFFFAOYSA-N 0.000 abstract 2
- -1 2-(2-Hydroxyethoxy)ethyl Chemical group 0.000 abstract 1
- IPBVNPXQWQGGJP-UHFFFAOYSA-N acetic acid phenyl ester Natural products CC(=O)OC1=CC=CC=C1 IPBVNPXQWQGGJP-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229940049953 phenylacetate Drugs 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K31/00—Medicinal preparations containing organic active ingredients
- A61K31/21—Esters, e.g. nitroglycerine, selenocyanates
- A61K31/215—Esters, e.g. nitroglycerine, selenocyanates of carboxylic acids
Landscapes
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Chemical & Material Sciences (AREA)
- Medicinal Chemistry (AREA)
- Pharmacology & Pharmacy (AREA)
- Epidemiology (AREA)
- Life Sciences & Earth Sciences (AREA)
- Animal Behavior & Ethology (AREA)
- General Health & Medical Sciences (AREA)
- Public Health (AREA)
- Veterinary Medicine (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
PROCEDIMIENTO PARA LA OBTENCION DE ESTERES DE DIETILENGLICOL. CONSISTE EN LA REACCION DIRECTA DEL DIETILENGLICOL CON UN ACIDO DE FORMULA (I), EN LA QUE R1 REPRESENTA HIDROGENO, CLORO O METILO, R2 ES HIDROGENO, METILO O TRIFLUOROMETILO, Y R3 ES HIDROGENO O CLORO Y N VALE 0 O 1, O CON SUS SALES SODICAS O POTASICAS. LA REACCION SE LLEVA A CABO EN PRESENCIA DE CLORURO DE TIONILO, A UNA TEMPERATURA COMPRENDIDA ENTRE LA TEMPERATURA AMBIENTE Y LA DEL BAÑO MARIA. EL PRODUCTO DE REACCION SE AISLA POR ADICION DE AGUA-ETER ETILICO Y SE PURIFICA MEDIANTE CROMATOGRAFIA A TRAVES DE UNA COLUMNA RELLENA DE SILICAGEL.
Priority Applications (9)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ES548226A ES8605220A1 (es) | 1985-10-25 | 1985-10-25 | Procedimiento de preparacion de esteres del dietilenglicol |
| PT81505A PT81505B (pt) | 1985-10-25 | 1985-11-15 | Processo de preparacao de esteres do dietileno-glicol |
| IT21774/86A IT1197255B (it) | 1985-10-25 | 1986-09-19 | Procedimento di preparazione di esteri di dietilenglicol |
| CH3810/86A CH676238A5 (es) | 1985-10-25 | 1986-10-22 | |
| DE19863636125 DE3636125A1 (de) | 1985-10-25 | 1986-10-23 | Verfahren zur herstellung von diethylenglykolestern |
| JP61252159A JPS62106064A (ja) | 1985-10-25 | 1986-10-24 | ジエチレングリコ−ルエステルの製造法 |
| GB8625481A GB2182041B (en) | 1985-10-25 | 1986-10-24 | Preparation of esters of diethylene glycol |
| BE0/217337A BE905666A (fr) | 1985-10-25 | 1986-10-27 | Procede de preparation d'esters de diethyleneglycol. |
| FR868614922A FR2589151B1 (fr) | 1985-10-25 | 1986-10-27 | Procede de preparation d'esters du diethyleneglycol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| ES548226A ES8605220A1 (es) | 1985-10-25 | 1985-10-25 | Procedimiento de preparacion de esteres del dietilenglicol |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES548226A0 ES548226A0 (es) | 1986-03-16 |
| ES8605220A1 true ES8605220A1 (es) | 1986-03-16 |
Family
ID=8490031
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES548226A Expired ES8605220A1 (es) | 1985-10-25 | 1985-10-25 | Procedimiento de preparacion de esteres del dietilenglicol |
Country Status (9)
| Country | Link |
|---|---|
| JP (1) | JPS62106064A (es) |
| BE (1) | BE905666A (es) |
| CH (1) | CH676238A5 (es) |
| DE (1) | DE3636125A1 (es) |
| ES (1) | ES8605220A1 (es) |
| FR (1) | FR2589151B1 (es) |
| GB (1) | GB2182041B (es) |
| IT (1) | IT1197255B (es) |
| PT (1) | PT81505B (es) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3811118C1 (es) * | 1988-03-31 | 1989-10-12 | Merckle Gmbh, 7902 Blaubeuren, De | |
| US9217066B2 (en) | 2008-03-31 | 2015-12-22 | Ford Global Technologies, Llc | Structural polymer insert and method of making the same |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1939112C3 (de) * | 1969-08-01 | 1975-03-06 | Troponwerke Dinklage & Co, 5000 Koeln | Ester der N-(3-Trifluormethylphenyl) -anthranilsäure, Verfahren zu ihrer Herstellung und pharmakologisch wirksame Zubereitungen derselben |
| DE2735569A1 (de) * | 1977-08-06 | 1979-02-15 | Troponwerke Gmbh & Co Kg | Verfahren zur herstellung von n-(alpha,alpha,alpha-trifluor-m-tolyl) anthranilsaeure-2-(2-hydroxyaethoxy)aethylester |
| DE2834169C2 (de) * | 1978-08-04 | 1984-02-09 | Troponwerke GmbH & Co KG, 5000 Köln | Verfahren zur Herstellung von 2-(2-Hydroxyäthoxy)äthyl-N-( alpha , alpha , alpha -trifluor-m-tolyl)anthranilat |
| DE2834168C2 (de) * | 1978-08-04 | 1984-02-09 | Troponwerke GmbH & Co KG, 5000 Köln | Verfahren zur Herstellung von 2-(2-Hydroxyäthoxy)äthyl-N-(α,α,α-trifluor-m-tolyl)anthranilat |
| DE2834167C2 (de) * | 1978-08-04 | 1984-01-26 | Troponwerke GmbH & Co KG, 5000 Köln | Verfahren zur Herstellung von 2-(2-Hydroxyäthoxy)äthyl-N-(α,α,α-trifluor-m-tolyl)anthranilat |
| DE2926472A1 (de) * | 1979-06-30 | 1981-01-15 | Thomae Gmbh Dr K | Neue benzoylderivate, deren herstellung und deren verwendung als arzneimittel |
| IL67445A (en) * | 1982-12-09 | 1985-11-29 | Teva Pharma | Ethoxycarbonyloxy ethyl esters of non-steroidal anti-inflammatory carboxylic acids |
| DE3476550D1 (en) * | 1983-07-21 | 1989-03-09 | Troponwerke Gmbh & Co Kg | Thermoplastics containing antiphlogistics |
| US4694105A (en) * | 1983-12-20 | 1987-09-15 | Ciba-Geigy Corporation | Herbicidal alkoxyamino- and polyalkoxyaminodiphenyl ethers |
| DE3407507A1 (de) * | 1984-03-01 | 1985-09-05 | A. Nattermann & Cie GmbH, 5000 Köln | Neue o-(2,6-dichloranilino)-phenylessigsaeureester, verfahren zu ihrer herstellung und diese enthaltende pharmazeutische praeparate |
-
1985
- 1985-10-25 ES ES548226A patent/ES8605220A1/es not_active Expired
- 1985-11-15 PT PT81505A patent/PT81505B/pt not_active IP Right Cessation
-
1986
- 1986-09-19 IT IT21774/86A patent/IT1197255B/it active
- 1986-10-22 CH CH3810/86A patent/CH676238A5/de not_active IP Right Cessation
- 1986-10-23 DE DE19863636125 patent/DE3636125A1/de not_active Ceased
- 1986-10-24 JP JP61252159A patent/JPS62106064A/ja active Pending
- 1986-10-24 GB GB8625481A patent/GB2182041B/en not_active Expired
- 1986-10-27 BE BE0/217337A patent/BE905666A/fr not_active IP Right Cessation
- 1986-10-27 FR FR868614922A patent/FR2589151B1/fr not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| FR2589151B1 (fr) | 1990-05-18 |
| IT8621774A0 (it) | 1986-09-19 |
| ES548226A0 (es) | 1986-03-16 |
| FR2589151A1 (fr) | 1987-04-30 |
| GB8625481D0 (en) | 1986-11-26 |
| IT8621774A1 (it) | 1988-03-19 |
| PT81505A (en) | 1985-12-01 |
| BE905666A (fr) | 1987-02-16 |
| CH676238A5 (es) | 1990-12-28 |
| IT1197255B (it) | 1988-11-30 |
| JPS62106064A (ja) | 1987-05-16 |
| GB2182041A (en) | 1987-05-07 |
| GB2182041B (en) | 1989-09-20 |
| DE3636125A1 (de) | 1987-04-30 |
| PT81505B (pt) | 1987-11-11 |
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