ES8300100A1 - Procedimiento para la obtencion de 1,2,4-triazol - Google Patents
Procedimiento para la obtencion de 1,2,4-triazolInfo
- Publication number
- ES8300100A1 ES8300100A1 ES503700A ES503700A ES8300100A1 ES 8300100 A1 ES8300100 A1 ES 8300100A1 ES 503700 A ES503700 A ES 503700A ES 503700 A ES503700 A ES 503700A ES 8300100 A1 ES8300100 A1 ES 8300100A1
- Authority
- ES
- Spain
- Prior art keywords
- triazole
- preparation
- hydrazine
- formamide
- metered
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- NSPMIYGKQJPBQR-UHFFFAOYSA-N 4H-1,2,4-triazole Chemical compound C=1N=CNN=1 NSPMIYGKQJPBQR-UHFFFAOYSA-N 0.000 title abstract 2
- ZHNUHDYFZUAESO-UHFFFAOYSA-N Formamide Chemical compound NC=O ZHNUHDYFZUAESO-UHFFFAOYSA-N 0.000 abstract 4
- OAKJQQAXSVQMHS-UHFFFAOYSA-N Hydrazine Chemical compound NN OAKJQQAXSVQMHS-UHFFFAOYSA-N 0.000 abstract 4
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
- C07D249/02—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms not condensed with other rings
- C07D249/08—1,2,4-Triazoles; Hydrogenated 1,2,4-triazoles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
PROCEDIMIENTO PARA 1 OBTENCION DE 1,2,4-TRIAZOL. CONSISTE EN HACER REACCIONAR LA HIDRAZINA Y LA FORMAMIDA A TEMPERATURA ELEVADA Y EN UNA PROPORCION MOLAR DE FORMAMIDA-HIDRAZINA DE AL MENOS 2:1. LA HIDRAZINA SE DOSIFICA COMO TAL O EN FORMA DE SU HIDRATO; DICHA HIDRAZINA SE CALIENTA PREVIAMENTE A UNA TEMPERATURA COMPRENDIDA ENTRE 160 Y 200GC, DURANTE LA DOSIFICACION, LA TEMPERATURA SE MANTIENE EN DICHO MARGEN, COMPLETANDOSE LA REACCION A 160-240GC. LA HIDRAZINA SE DOSIFICA EN LAS PROXIMIDADES DEL FONDO DE LA FORMAMIDA CALENTADA A TEMPERATURA DE REACCION QUE SE ENCUENTRA EN EL RECIPIENTE DE REACCION BAJO UNA SOBREPRESION SUFICIENTE PARA VENCER LA PRESION HIDROESTATICA EXISTENTE SOBRE LA ZONA DE ENTRADA DE LA HIDRAZINA. S
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| AT0353380A AT369736B (de) | 1980-07-07 | 1980-07-07 | Verfahren zur herstellung von 1,2,4-triazol |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| ES8300100A1 true ES8300100A1 (es) | 1982-10-01 |
| ES503700A0 ES503700A0 (es) | 1982-10-01 |
Family
ID=3551830
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES503700A Granted ES503700A0 (es) | 1980-07-07 | 1981-07-06 | Procedimiento para la obtencion de 1,2,4-triazol |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US4390704A (es) |
| EP (1) | EP0044438B2 (es) |
| JP (1) | JPS5781473A (es) |
| AT (1) | AT369736B (es) |
| CA (1) | CA1156662A (es) |
| DE (1) | DE3161422D1 (es) |
| DK (1) | DK157365C (es) |
| ES (1) | ES503700A0 (es) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR2521558A1 (fr) * | 1982-02-18 | 1983-08-19 | Nehezvegyipari Kutato Intezet | Procede pour la preparation de 1, 2, 4-triazole |
| US4490539A (en) * | 1982-06-22 | 1984-12-25 | Nehezvegyipari Kutato Intezet | Process for the preparation of 1,2,4-triazole |
| HU195790B (en) * | 1983-12-21 | 1988-07-28 | Alkaloida Vegyeszeti Gyar | Process for producing 1,2,4-triazol |
| EP0963979B1 (en) * | 1998-05-12 | 2006-12-27 | Mitsubishi Gas Chemical Company, Inc. | Method of producing 1,2,4-triazole starting from ketazin |
| KR100327818B1 (ko) * | 1999-04-16 | 2002-03-09 | 윤재승 | 플루코나졸의 제조방법 |
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| AT3500B (es) * | 1900-06-14 | 1901-02-25 | Gustav Goebel | |
| LU61617A1 (es) * | 1969-09-03 | 1970-12-01 | ||
| DE2802491B2 (de) * | 1978-01-20 | 1980-10-30 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von 1,2,4-Triazol |
| US4267347A (en) * | 1979-11-07 | 1981-05-12 | Ciba-Geigy Corporation | Method for direct preparation for 1,2,4-triazole from hydrazine and formamide |
-
1980
- 1980-07-07 AT AT0353380A patent/AT369736B/de not_active IP Right Cessation
-
1981
- 1981-06-26 DE DE8181104977T patent/DE3161422D1/de not_active Expired
- 1981-06-26 EP EP81104977A patent/EP0044438B2/de not_active Expired
- 1981-06-30 CA CA000380879A patent/CA1156662A/en not_active Expired
- 1981-07-03 DK DK294981A patent/DK157365C/da not_active IP Right Cessation
- 1981-07-06 ES ES503700A patent/ES503700A0/es active Granted
- 1981-07-07 JP JP56105166A patent/JPS5781473A/ja active Pending
- 1981-07-07 US US06/281,042 patent/US4390704A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0044438B1 (de) | 1983-11-16 |
| US4390704A (en) | 1983-06-28 |
| ATA353380A (de) | 1982-06-15 |
| EP0044438B2 (de) | 1987-01-21 |
| DK157365B (da) | 1989-12-27 |
| CA1156662A (en) | 1983-11-08 |
| ES503700A0 (es) | 1982-10-01 |
| AT369736B (de) | 1983-01-25 |
| DK294981A (da) | 1982-01-08 |
| JPS5781473A (en) | 1982-05-21 |
| EP0044438A3 (en) | 1982-02-10 |
| DK157365C (da) | 1990-05-21 |
| DE3161422D1 (en) | 1983-12-22 |
| EP0044438A2 (de) | 1982-01-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FD1A | Patent lapsed |
Effective date: 19970519 |