ES474615A1 - Procedimiento para la obtencion de un producto de condensa- cion de fenotizina y pnitrosofenol - Google Patents
Procedimiento para la obtencion de un producto de condensa- cion de fenotizina y pnitrosofenolInfo
- Publication number
- ES474615A1 ES474615A1 ES474615A ES474615A ES474615A1 ES 474615 A1 ES474615 A1 ES 474615A1 ES 474615 A ES474615 A ES 474615A ES 474615 A ES474615 A ES 474615A ES 474615 A1 ES474615 A1 ES 474615A1
- Authority
- ES
- Spain
- Prior art keywords
- condensation product
- producing
- sulfur dyes
- phenothiazine
- nitrosophenol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- WJFKNYWRSNBZNX-UHFFFAOYSA-N 10H-phenothiazine Chemical compound C1=CC=C2NC3=CC=CC=C3SC2=C1 WJFKNYWRSNBZNX-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 3
- 229950000688 phenothiazine Drugs 0.000 title abstract 3
- JSTCPNFNKICNNO-UHFFFAOYSA-N 4-nitrosophenol Chemical compound OC1=CC=C(N=O)C=C1 JSTCPNFNKICNNO-UHFFFAOYSA-N 0.000 title abstract 2
- 239000007859 condensation product Substances 0.000 title 3
- 239000000988 sulfur dye Substances 0.000 title 2
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 abstract 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 abstract 2
- 239000011593 sulfur Substances 0.000 abstract 2
- 229910052717 sulfur Inorganic materials 0.000 abstract 2
- 239000000975 dye Substances 0.000 abstract 1
- 239000007800 oxidant agent Substances 0.000 abstract 1
- 238000010992 reflux Methods 0.000 abstract 1
- 229910052979 sodium sulfide Inorganic materials 0.000 abstract 1
- GRVFOGOEDUUMBP-UHFFFAOYSA-N sodium sulfide (anhydrous) Chemical compound [Na+].[Na+].[S-2] GRVFOGOEDUUMBP-UHFFFAOYSA-N 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D279/00—Heterocyclic compounds containing six-membered rings having one nitrogen atom and one sulfur atom as the only ring hetero atoms
- C07D279/10—1,4-Thiazines; Hydrogenated 1,4-thiazines
- C07D279/14—1,4-Thiazines; Hydrogenated 1,4-thiazines condensed with carbocyclic rings or ring systems
- C07D279/18—[b, e]-condensed with two six-membered rings
- C07D279/34—[b, e]-condensed with two six-membered rings with hetero atoms directly attached to the ring sulfur atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D279/00—Heterocyclic compounds containing six-membered rings having one nitrogen atom and one sulfur atom as the only ring hetero atoms
- C07D279/10—1,4-Thiazines; Hydrogenated 1,4-thiazines
- C07D279/14—1,4-Thiazines; Hydrogenated 1,4-thiazines condensed with carbocyclic rings or ring systems
- C07D279/18—[b, e]-condensed with two six-membered rings
- C07D279/20—[b, e]-condensed with two six-membered rings with hydrogen atoms directly attached to the ring nitrogen atom
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B49/00—Sulfur dyes
- C09B49/10—Sulfur dyes from diphenylamines, indamines, or indophenols, e.g. p-aminophenols or leucoindophenols
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Coloring (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procedimiento para la obtención de un producto de condensación de fenotiazina y p-nitrosofenol, que contiene el indofenol-S-óxido de fórmula I **(Fórmula)** por reacción de fenotiazina con p-nitrosofenol en ácido sulfúrico, caracterizado porque la fenotiazina antes o durante la reacción se oxida con un agente de oxidación adicional.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2748744A DE2748744C3 (de) | 1977-10-29 | 1977-10-29 | Kondensationsprodukt aus Phenothiazin und p-Nitrosophenol, Verfahren zu seiner Herstellung und seine Verwendung zur Herstellung grüner Schwefelfarbstoffe |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES474615A1 true ES474615A1 (es) | 1979-03-16 |
Family
ID=6022689
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES474615A Expired ES474615A1 (es) | 1977-10-29 | 1978-10-27 | Procedimiento para la obtencion de un producto de condensa- cion de fenotizina y pnitrosofenol |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US4218219A (es) |
| EP (1) | EP0001801B1 (es) |
| JP (1) | JPS5471115A (es) |
| BR (1) | BR7807100A (es) |
| DE (2) | DE2748744C3 (es) |
| ES (1) | ES474615A1 (es) |
| IT (1) | IT1121504B (es) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2908486A1 (de) * | 1979-03-05 | 1980-09-11 | Cassella Ag | Verfahren zur herstellung eines kondensationsprodukts aus phenothiazin und p-nitrosophenol |
| US4917706B2 (en) * | 1988-02-01 | 1996-02-20 | Sandoz Ltd | Liquid compositions of prereduced sulfur dyes and production thereof |
| DE4136939A1 (de) * | 1990-11-22 | 1992-05-27 | Sandoz Ag | Verfahren zur reinigung von kupfer-enthaltenden industrieabwassern |
| US5631371A (en) * | 1995-11-22 | 1997-05-20 | Bayer Corporation | Method for the preparation of substituted 3-(phenylimino)-3H-phenothiazines and phenoxazines |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US966092A (en) * | 1910-03-04 | 1910-08-02 | Cassella Color Company | Indophenolic compound and process of making same. |
| US1128370A (en) * | 1913-04-24 | 1915-02-16 | Hoechst Ag | Indophenolsulfonic acids and process of making same. |
| US1867863A (en) * | 1927-02-14 | 1932-07-19 | Gen Aniline Works Inc | Indophenol azine compounds |
-
1977
- 1977-10-29 DE DE2748744A patent/DE2748744C3/de not_active Expired
-
1978
- 1978-10-24 EP EP78101212A patent/EP0001801B1/de not_active Expired
- 1978-10-24 DE DE7878101212T patent/DE2860346D1/de not_active Expired
- 1978-10-27 IT IT29209/78A patent/IT1121504B/it active
- 1978-10-27 JP JP13176378A patent/JPS5471115A/ja active Pending
- 1978-10-27 ES ES474615A patent/ES474615A1/es not_active Expired
- 1978-10-27 BR BR7807100A patent/BR7807100A/pt unknown
- 1978-10-30 US US05/955,643 patent/US4218219A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE2748744C3 (de) | 1981-10-01 |
| DE2748744A1 (de) | 1979-05-10 |
| DE2860346D1 (en) | 1981-02-12 |
| EP0001801A1 (de) | 1979-05-16 |
| DE2748744B2 (de) | 1980-09-25 |
| IT1121504B (it) | 1986-04-02 |
| JPS5471115A (en) | 1979-06-07 |
| EP0001801B1 (de) | 1980-11-26 |
| US4218219A (en) | 1980-08-19 |
| BR7807100A (pt) | 1979-05-15 |
| IT7829209A0 (it) | 1978-10-27 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FD1A | Patent lapsed |
Effective date: 19990405 |