ES458768A1 - Procedimiento para separar 4,4'-diaminodifenilmetano. - Google Patents
Procedimiento para separar 4,4'-diaminodifenilmetano.Info
- Publication number
- ES458768A1 ES458768A1 ES458768A ES458768A ES458768A1 ES 458768 A1 ES458768 A1 ES 458768A1 ES 458768 A ES458768 A ES 458768A ES 458768 A ES458768 A ES 458768A ES 458768 A1 ES458768 A1 ES 458768A1
- Authority
- ES
- Spain
- Prior art keywords
- isomer
- mixture
- diamines
- diaminodiphenylmethane
- dihydrochloride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- YBRVSVVVWCFQMG-UHFFFAOYSA-N 4,4'-diaminodiphenylmethane Chemical compound C1=CC(N)=CC=C1CC1=CC=C(N)C=C1 YBRVSVVVWCFQMG-UHFFFAOYSA-N 0.000 title abstract 3
- 238000000034 method Methods 0.000 title abstract 2
- 239000000203 mixture Substances 0.000 abstract 6
- 150000004985 diamines Chemical class 0.000 abstract 5
- 239000007795 chemical reaction product Substances 0.000 abstract 1
- 238000002955 isolation Methods 0.000 abstract 1
- SYSQUGFVNFXIIT-UHFFFAOYSA-N n-[4-(1,3-benzoxazol-2-yl)phenyl]-4-nitrobenzenesulfonamide Chemical class C1=CC([N+](=O)[O-])=CC=C1S(=O)(=O)NC1=CC=C(C=2OC3=CC=CC=C3N=2)C=C1 SYSQUGFVNFXIIT-UHFFFAOYSA-N 0.000 abstract 1
- 239000003960 organic solvent Substances 0.000 abstract 1
- 229920000768 polyamine Polymers 0.000 abstract 1
- -1 polymethylene Polymers 0.000 abstract 1
- 229920006389 polyphenyl polymer Polymers 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton
- C07C209/78—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton from carbonyl compounds, e.g. from formaldehyde, and amines having amino groups bound to carbon atoms of six-membered aromatic rings, with formation of methylene-diarylamines
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Procedimiento para separar 4,4¿-diaminodifenilmetano, en forma substancialmente pura de mezclas del mismo con el isómero 2,4¿ correspondiente, caracterizado porque consiste en: calentar en presencia de un solvente orgánico inerte una mezcla de (a) el diclorhidrato de dicha mezcla de isómeros
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US05/693,081 US4201722A (en) | 1976-06-04 | 1976-06-04 | Process for separating 4,4'-diaminodiphenylmethane |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| ES458768A1 true ES458768A1 (es) | 1978-03-16 |
Family
ID=24783232
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| ES458768A Expired ES458768A1 (es) | 1976-06-04 | 1977-05-13 | Procedimiento para separar 4,4'-diaminodifenilmetano. |
Country Status (13)
| Country | Link |
|---|---|
| US (1) | US4201722A (es) |
| JP (1) | JPS5948819B2 (es) |
| BE (1) | BE855402A (es) |
| BR (1) | BR7703390A (es) |
| DD (1) | DD130930A5 (es) |
| DE (1) | DE2719996C2 (es) |
| ES (1) | ES458768A1 (es) |
| FR (1) | FR2353518A1 (es) |
| GB (1) | GB1546349A (es) |
| IT (1) | IT1078289B (es) |
| MX (1) | MX145854A (es) |
| NL (1) | NL7705499A (es) |
| SU (1) | SU718006A3 (es) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0009094B1 (de) * | 1978-09-12 | 1982-04-14 | GebràDer Sulzer Aktiengesellschaft | Verfahren zur Herstellung von Methylenbrücken aufweisenden Polyarylaminen |
| EP1979306B1 (de) * | 2006-01-20 | 2013-04-17 | Basf Se | Verfahren zur simultanen herstellung von 4,4'-diphenylmethandiamin sowie diphenylmethandiisocyanat und polyphenylenpolymethylenpolyisocyanaten |
| US10759736B2 (en) | 2018-10-17 | 2020-09-01 | Covestro Deutschland Ag | Process for the preparation of di- and polyamines of the diphenylmethane series |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2149525A (en) * | 1934-10-18 | 1939-03-07 | Monsanto Chemicals | Separation of aminodiphenyls |
| GB808425A (en) * | 1954-08-21 | 1959-02-04 | Takashige Tojo | Improvements in or relating to the separation of aromatic amines |
| US2938054A (en) * | 1958-02-18 | 1960-05-24 | Allied Chem | Process for purification of 4, 4'-methylenedianiline |
| US3175007A (en) * | 1961-08-14 | 1965-03-23 | Dow Chemical Co | Purification of dianilines |
| US3410906A (en) * | 1965-10-15 | 1968-11-12 | Phillips Petroleum Co | Process of separating amines |
| US3542871A (en) * | 1968-07-29 | 1970-11-24 | Upjohn Co | Purification of 4,4'-methylene dianiline by crystallization |
| DE2238379C3 (de) * | 1972-08-04 | 1984-08-30 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von Polyaminen |
| CA1004234A (en) * | 1972-08-04 | 1977-01-25 | Bayer Aktiengesellschaft | Process for the production of polyamines |
| DE2238920C3 (de) * | 1972-08-08 | 1984-09-27 | Bayer Ag, 5090 Leverkusen | Verfahren zur Herstellung von Polyaminen |
| US4029705A (en) * | 1975-08-18 | 1977-06-14 | The Upjohn Company | Purification process for MDA |
-
1976
- 1976-06-04 US US05/693,081 patent/US4201722A/en not_active Expired - Lifetime
-
1977
- 1977-05-04 DE DE2719996A patent/DE2719996C2/de not_active Expired
- 1977-05-09 GB GB19353/77A patent/GB1546349A/en not_active Expired
- 1977-05-11 MX MX169100A patent/MX145854A/es unknown
- 1977-05-13 ES ES458768A patent/ES458768A1/es not_active Expired
- 1977-05-18 NL NL7705499A patent/NL7705499A/xx not_active Application Discontinuation
- 1977-05-19 IT IT49480/77A patent/IT1078289B/it active
- 1977-05-25 DD DD7700199122A patent/DD130930A5/xx unknown
- 1977-05-26 BR BR7703390A patent/BR7703390A/pt unknown
- 1977-06-03 FR FR7717038A patent/FR2353518A1/fr active Granted
- 1977-06-03 JP JP52064972A patent/JPS5948819B2/ja not_active Expired
- 1977-06-03 BE BE178208A patent/BE855402A/xx not_active IP Right Cessation
- 1977-06-03 SU SU772488999A patent/SU718006A3/ru active
Also Published As
| Publication number | Publication date |
|---|---|
| JPS5948819B2 (ja) | 1984-11-29 |
| BR7703390A (pt) | 1978-02-28 |
| DD130930A5 (de) | 1978-05-17 |
| NL7705499A (nl) | 1977-12-06 |
| DE2719996A1 (de) | 1977-12-15 |
| SU718006A3 (ru) | 1980-02-25 |
| MX145854A (es) | 1982-04-07 |
| US4201722A (en) | 1980-05-06 |
| FR2353518A1 (fr) | 1977-12-30 |
| IT1078289B (it) | 1985-05-08 |
| GB1546349A (en) | 1979-05-23 |
| BE855402A (fr) | 1977-12-05 |
| FR2353518B1 (es) | 1983-09-09 |
| JPS52148055A (en) | 1977-12-08 |
| DE2719996C2 (de) | 1986-06-26 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FD1A | Patent lapsed |
Effective date: 19991201 |