EP1663480A1 - Garnissage structure pour transfert de chaleur et de matiere - Google Patents
Garnissage structure pour transfert de chaleur et de matiereInfo
- Publication number
- EP1663480A1 EP1663480A1 EP04763486A EP04763486A EP1663480A1 EP 1663480 A1 EP1663480 A1 EP 1663480A1 EP 04763486 A EP04763486 A EP 04763486A EP 04763486 A EP04763486 A EP 04763486A EP 1663480 A1 EP1663480 A1 EP 1663480A1
- Authority
- EP
- European Patent Office
- Prior art keywords
- packing
- layers
- packing layers
- larger surface
- package according
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Ceased
Links
- 238000012856 packing Methods 0.000 title claims abstract description 49
- 238000012546 transfer Methods 0.000 title claims abstract description 6
- 239000007788 liquid Substances 0.000 claims description 20
- 238000009826 distribution Methods 0.000 claims description 4
- 238000004821 distillation Methods 0.000 claims description 3
- 239000002184 metal Substances 0.000 claims description 3
- 229910052751 metal Inorganic materials 0.000 claims description 3
- 239000000463 material Substances 0.000 claims description 2
- 238000010521 absorption reaction Methods 0.000 claims 1
- 238000000895 extractive distillation Methods 0.000 claims 1
- 238000000066 reactive distillation Methods 0.000 claims 1
- 238000005201 scrubbing Methods 0.000 claims 1
- 239000010410 layer Substances 0.000 description 23
- 230000000694 effects Effects 0.000 description 3
- 239000012530 fluid Substances 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 239000002344 surface layer Substances 0.000 description 2
- 230000002411 adverse Effects 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000007700 distillative separation Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000000265 homogenisation Methods 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 238000000034 method Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000013517 stratification Methods 0.000 description 1
- 238000009827 uniform distribution Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/32—Packing elements in the form of grids or built-up elements for forming a unit or module inside the apparatus for mass or heat transfer
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/322—Basic shape of the elements
- B01J2219/32203—Sheets
- B01J2219/3221—Corrugated sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/322—Basic shape of the elements
- B01J2219/32203—Sheets
- B01J2219/32213—Plurality of essentially parallel sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/322—Basic shape of the elements
- B01J2219/32203—Sheets
- B01J2219/32224—Sheets characterised by the orientation of the sheet
- B01J2219/32227—Vertical orientation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/322—Basic shape of the elements
- B01J2219/32203—Sheets
- B01J2219/32224—Sheets characterised by the orientation of the sheet
- B01J2219/32234—Inclined orientation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/322—Basic shape of the elements
- B01J2219/32203—Sheets
- B01J2219/32237—Sheets comprising apertures or perforations
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/322—Basic shape of the elements
- B01J2219/32203—Sheets
- B01J2219/32255—Other details of the sheets
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/322—Basic shape of the elements
- B01J2219/32203—Sheets
- B01J2219/32265—Sheets characterised by the orientation of blocks of sheets
- B01J2219/32268—Sheets characterised by the orientation of blocks of sheets relating to blocks in the same horizontal level
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/32—Details relating to packing elements in the form of grids or built-up elements for forming a unit of module inside the apparatus for mass or heat transfer
- B01J2219/324—Composition or microstructure of the elements
- B01J2219/32408—Metal
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S261/00—Gas and liquid contact apparatus
- Y10S261/72—Packing elements
Definitions
- the invention relates to an ordered packing for heat and / or mass transfer columns with at least one packing layer of several packing layers.
- the packing for distillation columns are prepared according to the prior art from sub-elements of the same geometry, such as zigzag-shaped bent sheets, expanded metals or wire mesh.
- the purpose of this uniform geometric design is that over the entire column cross-section as uniform as possible flows of gas and liquid occur. Deviations from this, especially marginalities of the liquid or stratification of the liquid, must be avoided, as this negatively affects the separation performance.
- To remedy such negative non-uniform liquid distributions it is necessary to use liquid collector and liquid distributor at intervals of a few meters. In addition to the equipment costs of these installations also their installation height of about 1, 5 to 2.5 m negative, since this increases the height of the columns.
- the object of the invention is to achieve a uniform liquid distribution over the column cross-section in a package of the type mentioned in a simple structure.
- the packing layer has packing layers which, compared to the other packing layers of the same packing layer, have a greater density and thus a larger surface area.
- FIG. 1 shows a first embodiment of a packing unit / packing layer in the cutout
- FIG. 2 shows a second embodiment of a packing unit / packing layer in the neck.
- packing beds In a column several packing beds are arranged horizontally one above the other at a distance.
- the beds have one or more packing layers 3, which consist of Packing layers 4a, 4b are composed, which may be arranged vertically or obliquely.
- Figures 1 and 2 show sections of packing layers 3 according to the invention, in which the packing layers have at least two different sized specific surfaces.
- two narrower denser packing layers 4b are installed adjacent to the higher specific surface. Between these layers 4b with the larger specific surface are 1 to about 10, preferably 3 to 6, adjacent layers 4a having a smaller specific surface area.
- the specific surface area of the smaller specific surface layers 4a corresponds to the geometries customary in the art with a specific surface area of about 150 to 750 m 2 / m 3 .
- the larger specific surface layers 4b have about a factor of 2 to 10 larger specific surface area.
- the reason for this very large specific surface area is the incorporation-deviating function used by the usual distillation techniques.
- the interspaces of the packing layers 4b with the larger specific surface are preferably only or predominantly with liquid flows through. In these fluid-filled gaps occurs a good homogenization of a portion of the liquid flow and a uniform distribution.
- Such packing layers therefore have a distributive effect. They make separate arrangements of liquid collectors and liquid distributors wholly or at least partially dispensable. In order to achieve a mass transfer between the gas phase and the liquid even in the case of the narrow liquid-filled packing layers 4b, these packing layers are preferably produced from materials which have perforations, for example expanded metal or wire mesh.
Landscapes
- Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10343649A DE10343649A1 (de) | 2003-09-20 | 2003-09-20 | Geordnete Packung für Wärme- und Stoffaustausch |
| PCT/EP2004/008329 WO2005037429A1 (fr) | 2003-09-20 | 2004-07-24 | Garnissage structure pour transfert de chaleur et de matiere |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| EP1663480A1 true EP1663480A1 (fr) | 2006-06-07 |
Family
ID=34305987
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| EP04763486A Ceased EP1663480A1 (fr) | 2003-09-20 | 2004-07-24 | Garnissage structure pour transfert de chaleur et de matiere |
Country Status (4)
| Country | Link |
|---|---|
| US (1) | US7559540B2 (fr) |
| EP (1) | EP1663480A1 (fr) |
| DE (1) | DE10343649A1 (fr) |
| WO (1) | WO2005037429A1 (fr) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20110206569A1 (en) * | 2008-10-31 | 2011-08-25 | Basf Se | Ion exchanger moulded body and method for producing same |
| DE102012011553A1 (de) | 2012-06-11 | 2013-12-12 | Rvt Process Equipment Gmbh | Niedriglastverteiler |
| FR3018201B1 (fr) | 2014-03-10 | 2016-02-26 | Ifp Energies Now | Contacteur pour colonne d'echange constitue d'un agencement de garnissages structures |
| FR3018200B1 (fr) | 2014-03-10 | 2017-12-01 | Ifp Energies Now | Contacteur pour colonne d'echange constitue de compartiments de garnissage vrac |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| NL292044A (fr) * | 1963-03-22 | |||
| SE338333B (fr) * | 1970-03-26 | 1971-09-06 | C Munters Ab | |
| SE8400302L (sv) * | 1984-01-20 | 1985-08-18 | Munters Ab Carl | Kontaktkropp |
| US4842778A (en) * | 1985-12-23 | 1989-06-27 | Glitsch, Inc. | Apparatus for flow distribution in packed towers |
| FR2711545B1 (fr) * | 1993-10-29 | 1995-12-22 | Air Liquide | Distributeur de liquide pour dispositif d'échange de chaleur et de matière, colonne de distillation comprenant un tel distributeur, et utilisation d'une telle colonne pour la distillation de l'air. |
| DE59510174D1 (de) * | 1995-11-29 | 2002-05-23 | Sulzer Chemtech Ag Winterthur | Packung für eine Gegenstrom-Hochdruckkolonne |
| US5876638A (en) * | 1996-05-14 | 1999-03-02 | Air Products And Chemicals, Inc. | Structured packing element with bi-directional surface texture and a mass and heat transfer process using such packing element |
| US6089549A (en) * | 1997-09-25 | 2000-07-18 | Koch-Glitsch, Inc. | Exchange column structured packing bed having packing bricks |
| JPH11179102A (ja) | 1997-12-19 | 1999-07-06 | Kimura Chem Plants Co Ltd | 内部熱交換型蒸留塔及びそれに用いる充填物 |
| US5984282A (en) * | 1998-01-20 | 1999-11-16 | Air Products And Chemicals, Inc. | Packed liquid-vapor contact column having at least one band of packing sheets surrounding a central core of packing sheets |
| FR2777533B1 (fr) * | 1998-04-17 | 2000-05-19 | Air Liquide | Structure maritime flottante perfectionnee |
| US6425574B1 (en) * | 1998-12-18 | 2002-07-30 | Air Products And Chemicals, Inc. | Mixed-resistance structured packing |
| DE19936380A1 (de) * | 1999-08-03 | 2001-02-08 | Basf Ag | Geordnete Packung zum Wärme- und Stoffaustausch |
| DE10010810A1 (de) * | 2000-03-08 | 2001-09-13 | Montz Gmbh Julius | Flüssigkeitsverteiler und Verfahren zum Betreiben |
| US6751986B2 (en) | 2000-12-22 | 2004-06-22 | The Bog Group, Inc. | Structured packing |
| DE10203819C2 (de) * | 2002-01-31 | 2003-04-17 | Johann Stichlmair | Einbauten für Packungskolonnen |
| US6991222B2 (en) * | 2003-03-31 | 2006-01-31 | George Amir Meski | Structured packing with increased capacity |
-
2003
- 2003-09-20 DE DE10343649A patent/DE10343649A1/de not_active Ceased
-
2004
- 2004-07-24 WO PCT/EP2004/008329 patent/WO2005037429A1/fr not_active Ceased
- 2004-07-24 EP EP04763486A patent/EP1663480A1/fr not_active Ceased
- 2004-07-24 US US10/572,541 patent/US7559540B2/en not_active Expired - Lifetime
Non-Patent Citations (1)
| Title |
|---|
| See references of WO2005037429A1 * |
Also Published As
| Publication number | Publication date |
|---|---|
| WO2005037429A1 (fr) | 2005-04-28 |
| US20070035047A1 (en) | 2007-02-15 |
| DE10343649A1 (de) | 2005-04-14 |
| US7559540B2 (en) | 2009-07-14 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PUAI | Public reference made under article 153(3) epc to a published international application that has entered the european phase |
Free format text: ORIGINAL CODE: 0009012 |
|
| 17P | Request for examination filed |
Effective date: 20060223 |
|
| AK | Designated contracting states |
Kind code of ref document: A1 Designated state(s): AT BE BG CH CY CZ DE DK EE ES FI FR GB GR HU IE IT LI LU MC NL PL PT RO SE SI SK TR |
|
| DAX | Request for extension of the european patent (deleted) | ||
| RIN1 | Information on inventor provided before grant (corrected) |
Inventor name: ZICH, EGON Inventor name: RIETFORT, THOMAS Inventor name: JANSEN, HELMUT Inventor name: KAIBEL, BJOERN |
|
| 17Q | First examination report despatched |
Effective date: 20090803 |
|
| STAA | Information on the status of an ep patent application or granted ep patent |
Free format text: STATUS: THE APPLICATION HAS BEEN REFUSED |
|
| 18R | Application refused |
Effective date: 20100422 |