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EP1512469A1 - Method and device for lubricating rolling rolls - Google Patents

Method and device for lubricating rolling rolls Download PDF

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Publication number
EP1512469A1
EP1512469A1 EP04447085A EP04447085A EP1512469A1 EP 1512469 A1 EP1512469 A1 EP 1512469A1 EP 04447085 A EP04447085 A EP 04447085A EP 04447085 A EP04447085 A EP 04447085A EP 1512469 A1 EP1512469 A1 EP 1512469A1
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EP
European Patent Office
Prior art keywords
lubricant
installation according
box
diaphragm
strip
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
EP04447085A
Other languages
German (de)
French (fr)
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EP1512469B1 (en
Inventor
Guillaume Bourdon
Hugo Uijtdebroeks
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Centre de Recherches Metallurgiques CRM ASBL
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Centre de Recherches Metallurgiques CRM ASBL
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Publication of EP1512469A1 publication Critical patent/EP1512469A1/en
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Publication of EP1512469B1 publication Critical patent/EP1512469B1/en
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Classifications

    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B7/00Spraying apparatus for discharge of liquids or other fluent materials from two or more sources, e.g. of liquid and air, of powder and gas
    • B05B7/0012Apparatus for achieving spraying before discharge from the apparatus
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B7/00Spraying apparatus for discharge of liquids or other fluent materials from two or more sources, e.g. of liquid and air, of powder and gas
    • B05B7/02Spray pistols; Apparatus for discharge
    • B05B7/04Spray pistols; Apparatus for discharge with arrangements for mixing liquids or other fluent materials before discharge
    • B05B7/0416Spray pistols; Apparatus for discharge with arrangements for mixing liquids or other fluent materials before discharge with arrangements for mixing one gas and one liquid
    • B05B7/0441Spray pistols; Apparatus for discharge with arrangements for mixing liquids or other fluent materials before discharge with arrangements for mixing one gas and one liquid with one inner conduit of liquid surrounded by an external conduit of gas upstream the mixing chamber
    • B05B7/045Spray pistols; Apparatus for discharge with arrangements for mixing liquids or other fluent materials before discharge with arrangements for mixing one gas and one liquid with one inner conduit of liquid surrounded by an external conduit of gas upstream the mixing chamber the gas and liquid flows being parallel just upstream the mixing chamber
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B27/00Rolls, roll alloys or roll fabrication; Lubricating, cooling or heating rolls while in use
    • B21B27/06Lubricating, cooling or heating rolls
    • B21B27/10Lubricating, cooling or heating rolls externally
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B45/00Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
    • B21B45/02Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills for lubricating, cooling, or cleaning
    • B21B45/0203Cooling
    • B21B45/0209Cooling devices, e.g. using gaseous coolants
    • B21B45/0215Cooling devices, e.g. using gaseous coolants using liquid coolants, e.g. for sections, for tubes
    • B21B45/0233Spray nozzles, Nozzle headers; Spray systems
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B21MECHANICAL METAL-WORKING WITHOUT ESSENTIALLY REMOVING MATERIAL; PUNCHING METAL
    • B21BROLLING OF METAL
    • B21B45/00Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills
    • B21B45/02Devices for surface or other treatment of work, specially combined with or arranged in, or specially adapted for use in connection with, metal-rolling mills for lubricating, cooling, or cleaning
    • B21B45/0239Lubricating
    • B21B45/0245Lubricating devices
    • B21B45/0248Lubricating devices using liquid lubricants, e.g. for sections, for tubes
    • B21B45/0251Lubricating devices using liquid lubricants, e.g. for sections, for tubes for strips, sheets, or plates
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B05SPRAYING OR ATOMISING IN GENERAL; APPLYING FLUENT MATERIALS TO SURFACES, IN GENERAL
    • B05BSPRAYING APPARATUS; ATOMISING APPARATUS; NOZZLES
    • B05B7/00Spraying apparatus for discharge of liquids or other fluent materials from two or more sources, e.g. of liquid and air, of powder and gas
    • B05B7/02Spray pistols; Apparatus for discharge
    • B05B7/04Spray pistols; Apparatus for discharge with arrangements for mixing liquids or other fluent materials before discharge
    • B05B7/0416Spray pistols; Apparatus for discharge with arrangements for mixing liquids or other fluent materials before discharge with arrangements for mixing one gas and one liquid
    • B05B7/0441Spray pistols; Apparatus for discharge with arrangements for mixing liquids or other fluent materials before discharge with arrangements for mixing one gas and one liquid with one inner conduit of liquid surrounded by an external conduit of gas upstream the mixing chamber

Definitions

  • the present invention relates to a new cylinder lubrication system of a rolling line, preferably a rolling line to hot.
  • the invention also relates to the method implemented on the installation.
  • thermomechanical path well determined (reduction, temperature) which is influenced by the friction between the work rolls and the band in the gap between the rollers. It is well known that this thermomechanical path has a major influence on the tape quality (surface appearance and properties Metallurgical).
  • Friction is mainly influenced by the evolution of the surface of the roll and by the film of scale formed on the surface of the rollers and the strip.
  • the coefficient of friction changes during a rolling campaign, a deterioration of the surface of the rolls (banding, peeling) accompanied by a increase in this coefficient of friction.
  • Friction is also influenced by the nature of the rolls, the new HSS rollers being characterized by higher coefficients of friction.
  • cylinder lubrication rolling mill is produced by spraying an emulsion, which is a suspension of oil droplets in the water, without mixing of oil and water, with a concentration in oil typically ranging between 0.3 and 2%. he can either a stable emulsion or an emulsion unstable prepared online.
  • the emulsion is applied directly on the work rolls by means of a spray device located after the squeegees in the purpose of applying the oil on a dry surface.
  • This mode application ensures a better distribution of the oil and therefore contributes to the reduction of the oil consumption.
  • lubrication leads to a improvement of the metallurgical properties of the product, especially when the finishing lamination takes place at low temperature in the ferritic field.
  • the level of required quality therefore requires very little lubrication performance.
  • the level of coefficient of friction that should be achieved to obtain optimization of the mechanical properties of the product should to be close to 0.10, which is well below current performance.
  • the coefficient of friction depends on many factors such that the application technology used, the quantity of oil, the nature of the oil, the speed of flow and the concentration of the oil emulsion, the temperature of the surface of the tape, the nature and condition of the rollers (roughness, degradation, scale, etc.), the speed of rolling, reduction, etc.
  • the effectiveness of lubrication can be very different from a train to the other and from one cage to another in the same train.
  • the lubrication efficiency is a function of the rolling temperature, the nature of the lubricant (mineral, ester-based, etc.) and the amount thereof. Satisfactory results are obtained by spraying oil in surface densities ("plate-out") of 0.1 to 1 g / m 2 , which is significantly more than is required simply to control the degradation of the rollers .
  • the system of spraying the oil emulsion is either a venturi, the aspiration of the oil being carried out by the depression created by moving water in the main tube, a static mixer ("static tube mixer") where one oil injection into a tube area where the shear (velocity gradient) is increased thanks to the presence of "obstacles".
  • the venturi or the "static tube mixer” is combined with a series of injectors whose number is selected based on the bandwidth at lubricate (3 to 7 injectors for a band up to 2 meters wide).
  • EP-A-1,193,004 discloses a method of lubrication system for cold rolling comprising steps of: supplying a rolling oil emulsion using a first device for supplying the oil in the form of an emulsion supplied to a cylinder and a steel strip according to a recirculation mode and a second device for supplying the emulsion only on the front and back surfaces of the steel strip.
  • the rolling oil is added to an emulsifier of the same type and concentration as those used for the first device, with a control of average size of particles so that they are more large than in the first device.
  • the emulsion produced by the second device not adhered to the band is recovered at the same time as the emulsion produced by the first device.
  • US-A-3,933,660 proposes an oil lubricating reducer for hot rolling of copper and its alloys comprising 1000 parts by weight of water, 6 to 200 parts by weight of anionic surface activator of type carboxylic acid, sulfate or phosphate and 0.8 to 200 parts by weight of at least one compound containing a hydroxyl group of alcohol type, alkylene glycol or ether glycol.
  • Rolling oil provides copper and its alloys a lubrication, an ability to remove a oxide film and an ability to prevent the formation of a oxide film by spraying between the cylinder of rolling and the hot rolling strip.
  • JP-A-55 151 093 describes a process lubrication in cold rolling of a covered strip by a polar organic compound which is sprayed with a emulsion of oil and a composition comprising a compound polar organic such as stearic acid.
  • the emulsion excess oil is removed by spinning after formation of an adsorbed oil layer on the surface of the bandaged.
  • the present invention aims to provide a solution that overcomes the disadvantages of the state of technique such as the inability to control and control the concentration and stability of the emulsion oil-water, clogging of the intake pipes of the emulsion by formation of solid organic residues, the influence of the specific flow rate, etc.
  • the object of the invention is in particular to propose a new process of lubricating the cylinders of rolling to maintain constant or in any case under control the friction on an industrial scale.
  • the invention also aims to increase the effectiveness of the attachment of the lubricating oil on the cylinders.
  • the invention also aims to increase the homogenisation of the distribution of the oil on the cylinders.
  • said lubricant possesses a purity of at least 95% and a boiling temperature greater than 130 ° C, and preferably a temperature boiling above 300 ° C and a flash point greater than 180 ° C. This requirement therefore excludes water as lubricant as well as oil emulsions in the water. At the limit, traces of water present in the lubricant, within its purity, may to be tolerated.
  • the installation of the invention is provided with means of controlling the temperature of the box, preferably comprising an electrical resistance or a water circuit. Temperature control provides a better controllability of the process in general and in particular reduces the problems related to the viscosity of the lubricant.
  • said temperature control means are associated to the use of a solid lubricant at temperature ambient and liquid at a working temperature of installation above room temperature.
  • said means of formation of a cloud of droplets comprises at least one nozzle or injector without air, preferably a jet of full cone type, or an internal mixing atomizer or external lubricant suspended in air or gas inert or an ultrasonic atomizer.
  • the installation comprises a plurality of nozzles or injectors or atomizers distributed the width of the rolling line, some of which can be made non-operational to adapt to the effective width of the band and / or quantity surface of lubricant to be deposited.
  • the installation comprises means for cutting said sprinklers, ie one out of two, either randomly.
  • the box is subdivided into at least two parts, each part comprising a diaphragm and an associated device for recovering lubricant.
  • the excess lubricant recovery device and / or the diaphragm (s) is (are) made of a material pierced with a plurality of holes or in a porous material.
  • the lubricant recovery device surplus includes a closed circuit for the circulation of lubricant with pumping equipment and possibly lubricant recycling.
  • An additional feature of the invention is that the spray angle, the opening the diaphragm (s) and their number on the face front of the box, as well as possibly the dimensions of the box, are chosen according to the width of the cylinders and / or the tape to be lubricated and the speed of the band.
  • the installation of the invention comprises means for increasing the opening of the diaphragm (s) with the scroll speed of the band, which is also equal to the tangential speed cylinders.
  • the internal walls of the box are made of a material allowing suction of the lubricant.
  • the band scrolls at a speed ranging from 0.5 to 20 m / s.
  • the opening of the diaphragm or diaphragms is adjusted to deposit on the target a surface amount ("plate-out") of lubricant of between 0.01 and 1 g / m 2 .
  • the injection parameters of lubricant are regulated in open or closed loop.
  • Figure 1 schematically represents a nozzle for atomizing oil in the air, mixing internal, according to the state of the art.
  • Figure 2 schematically represents a first preferred embodiment of this invention.
  • Figure 3 schematically represents a second preferred embodiment of this invention.
  • Figure 4 schematically represents a third preferred embodiment of this invention.
  • the idea behind the present invention is combined use in a lubrication device a means for spraying fine droplets of lubricant and a diaphragm equipped with a oil recovery.
  • the The present invention relates more specifically to a spray lubrication system comprising a sprayer (or vaporizer) 1 of pure lubricant or a mixture of lubricants such as lubricants-based carbon, silicone or even molybdenum disulfide.
  • a sprayer or vaporizer
  • This or these lubricants have a degree of impurities or usual additives for products of this type commercially available (eg maximum 5%).
  • the spraying is carried out in the presence air.
  • Lubricants will be chosen as part of the present invention so as to have a temperature boiling above 130 ° C.
  • the function of the spray box 1 is to confine the atmosphere created by the fog of spray.
  • spray means either a spray or a spray atomisation, ie the reduction of the lubricant, at starting in the liquid state, in fine droplets, respectively in the presence or absence of air under pressure, leading to a droplet size ranging from a few microns to several millimeters, for example 2 mm, depending on the particular technology employed.
  • FIG. 1 shows an atomizer oil / air with internal mixing known in the state of the and can advantageously serve as a means of Spray 10 according to the present invention.
  • the air 12 is injected according to a ring 12 'surrounding the flow of oil 11, which makes it possible to obtain a conical cloud 20 atomization.
  • the cloud of droplets is formed by the shock occurring between the oil from the oil nozzle 11 and the air (or a gas inert) injected 12, the oil being dispersed in the air just before the release of the oil from the atomizer.
  • the oil flow is adjustable by changing the pressure of oil, the air pressure can be adjusted separately.
  • Figure 2 shows a sprayer according to a first preferred embodiment of the invention, comprising a only diaphragm 3, while figure 3 shows a sprayer according to a second preferred mode of the invention, comprising two diaphragms 3,3 '.
  • the internal side walls of the box may be covered with a common material 5 or alternatively a material allowing the suction of the lubricant, as shown in Figure 4.
  • the excess oil or lubricant, located on the inner walls and on the diaphragm, is sucked outside, recycled and reintroduced into the lubrication device.

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  • Engineering & Computer Science (AREA)
  • Mechanical Engineering (AREA)
  • Metal Rolling (AREA)
  • Nozzles (AREA)

Abstract

An installation for the in-line lubrication of rolls for the hot rolling of steel strip by pulverization or atomization of a lubricant or mixture of lubricants on a target, comprises an essentially closed case (1) provided with: (a) a mechanism (10) for forming a cloud of lubricating droplets with a size of less than 2 mm, preferably less than 700 Microm and more preferably less than 200 Microm; (b) a diaphragm (3) with an adjustable opening placed on a leading surface of the case; and (c) a device for the recuperation of excess lubricant (4) on the part of the diaphragm inside the case and on the inner walls of the case. An independent claim is also included for lubricating rolling mill rolls using this installation.

Description

Objet de l'inventionObject of the invention

La présente invention se rapporte à une nouvelle installation de lubrification de cylindres d'une ligne de laminage, de préférence une ligne de laminage à chaud.The present invention relates to a new cylinder lubrication system of a rolling line, preferably a rolling line to hot.

L'invention se rapporte également au procédé mis en oeuvre sur l'installation.The invention also relates to the method implemented on the installation.

Arrière-plan technologique et état de la techniqueTechnological background and state of the art

Pendant le laminage à chaud de bandes d'acier, dans chaque cage du train finisseur, la bande d'acier est soumise à un chemin thermomécanique bien déterminé (réduction, température) qui est influencé par le frottement entre les rouleaux de travail et la bande dans l'interstice entre les rouleaux. Il est bien connu que ce chemin thermomécanique a une influence majeure sur la qualité de la bande (aspect de surface et propriétés métallurgiques).During hot rolling of strips of steel, in each cage of the finishing train, the band of steel is subject to a thermomechanical path well determined (reduction, temperature) which is influenced by the friction between the work rolls and the band in the gap between the rollers. It is well known that this thermomechanical path has a major influence on the tape quality (surface appearance and properties Metallurgical).

Il est donc primordial de pouvoir contrôler et maítriser le frottement dans l'interstice des rouleaux (ou cylindres). Un coefficient de frottement trop élevé conduit à une consommation d'énergie trop importante, une dégradation rapide des rouleaux ainsi que des défauts de surface sur la bande. A l'inverse, un coefficient de frottement trop faible provoque des problèmes de glissement et de guidage de la bande ainsi que des problèmes d'entrée de celle-ci dans la cage.It is therefore essential to be able to control and control the friction in the interstice of the rollers (or cylinders). A coefficient of friction too high leads to excessive energy consumption, rapid degradation of the rolls as well as defects in surface on the band. Conversely, a coefficient of low friction causes slip problems and guide the tape as well as entry problems of it in the cage.

Le frottement est principalement influencé par l'évolution de la surface du rouleau et par le film de calamine formé sur la surface des rouleaux et de la bande. Ainsi, le coefficient de frottement évolue lors d'une campagne de laminage, une dégradation de la surface des rouleaux (banding, peeling) s'accompagnant d'une augmentation de ce coefficient de frottement. Le frottement est également influencé par la nature des rouleaux, les nouveaux rouleaux HSS étant caractérisés par des coefficients de frottement plus élevés.Friction is mainly influenced by the evolution of the surface of the roll and by the film of scale formed on the surface of the rollers and the strip. Thus, the coefficient of friction changes during a rolling campaign, a deterioration of the surface of the rolls (banding, peeling) accompanied by a increase in this coefficient of friction. Friction is also influenced by the nature of the rolls, the new HSS rollers being characterized by higher coefficients of friction.

Le contrôle du coefficient de frottement est assuré par le processus de lubrification.The control of the coefficient of friction is ensured by the lubrication process.

Actuellement la lubrification des cylindres de laminoir est réalisée par pulvérisation d'une émulsion, qui est une suspension de gouttelettes d'huile dans l'eau, sans mélange de l'huile et de l'eau, avec une concentration en huile variant typiquement entre 0,3 et 2 %. Il peut s'agir soit d'une émulsion stable, soit d'une émulsion instable préparée en ligne.Currently cylinder lubrication rolling mill is produced by spraying an emulsion, which is a suspension of oil droplets in the water, without mixing of oil and water, with a concentration in oil typically ranging between 0.3 and 2%. he can either a stable emulsion or an emulsion unstable prepared online.

Généralement, l'émulsion est appliquée directement sur les rouleaux de travail au moyen d'un dispositif de pulvérisation situé après les raclettes dans le but d'appliquer l'huile sur une surface sèche. Ce mode d'application assure une meilleure répartition de l'huile et par conséquent contribue à la réduction de la consommation en huile.Generally, the emulsion is applied directly on the work rolls by means of a spray device located after the squeegees in the purpose of applying the oil on a dry surface. This mode application ensures a better distribution of the oil and therefore contributes to the reduction of the oil consumption.

L'intérêt d'une bonne lubrification des rouleaux de travail n'est pas simplement limité au problème de performance des rouleaux (dégradation de surface) mais est également lié aux forces et couples de laminage à appliquer et partant à la consommation électrique nécessaire. La nécessité d'avoir une lubrification performante est encore accrue avec l'utilisation de rouleaux de type HSS caractérisés par un coefficient de frottement plus élevé que les rouleaux traditionnels.The interest of a good lubrication of work rolls is not just limited to the problem roll performance (surface degradation) but is also related to the forces and rolling torques to apply and hence to the power consumption necessary. The need for lubrication performance is further enhanced with the use of HSS type rollers characterized by a coefficient of higher friction than traditional rollers.

Dans des conditions normales de laminage, sans lubrification, les coefficients de frottement de Coulomb s'élèvent à 0,2 - 0,25, au moins dans les premières cages. Avec lubrification, on a calculé, à partir de la perte de charge de laminage observée, que les coefficients de frottement sont de l'ordre de 0,15 - 0,18.Under normal rolling conditions, without lubrication, the friction coefficients of Coulomb amount to 0.2 - 0.25, at least in the first cages. With lubrication, we calculated, from the observed rolling pressure loss, that the coefficients friction are of the order of 0.15 - 0.18.

Outre la minimisation de la dégradation des rouleaux de travail, la lubrification conduit à une amélioration des propriétés métallurgiques du produit, surtout lorsque le laminage de finition a lieu à basse température dans le domaine ferritique. Le niveau de qualité exigé requiert dès lors une lubrification très performante. En fait, le niveau de coefficient de frottement qui devrait être atteint pour obtenir l'optimisation des propriétés mécaniques du produit devrait se situer au voisinage de 0,10, ce qui est bien en deçà des performances actuelles.In addition to minimizing the degradation of work rolls, lubrication leads to a improvement of the metallurgical properties of the product, especially when the finishing lamination takes place at low temperature in the ferritic field. The level of required quality therefore requires very little lubrication performance. In fact, the level of coefficient of friction that should be achieved to obtain optimization of the mechanical properties of the product should to be close to 0.10, which is well below current performance.

Dans les conditions de lubrification, le coefficient de frottement dépend de nombreux facteurs tels que la technologie d'application utilisée, la quantité d'huile, la nature de l'huile, la vitesse de flux et la concentration de l'émulsion d'huile, la température de la surface de la bande, la nature et l'état des rouleaux (rugosité, dégradation, calamine, etc.), la vitesse de laminage, la réduction, etc. Ainsi, l'efficacité de lubrification peut être très différente d'un train à l'autre et d'une cage à l'autre dans le même train.In lubrication conditions, the coefficient of friction depends on many factors such that the application technology used, the quantity of oil, the nature of the oil, the speed of flow and the concentration of the oil emulsion, the temperature of the surface of the tape, the nature and condition of the rollers (roughness, degradation, scale, etc.), the speed of rolling, reduction, etc. Thus, the effectiveness of lubrication can be very different from a train to the other and from one cage to another in the same train.

En laboratoire, on a déterminé que l'efficacité de lubrification est fonction de la température de laminage, de la nature du lubrifiant (minéral, à base d'ester, etc.) et de la quantité de celui-ci mise en oeuvre. Des résultats satisfaisants sont obtenus en pulvérisant de l'huile dans des répartitions surfaciques ("plate-out") de 0,1 à 1 g/m2, ce qui est nettement plus que ce qui est requis simplement pour contrôler la dégradation des rouleaux.In the laboratory, it has been determined that the lubrication efficiency is a function of the rolling temperature, the nature of the lubricant (mineral, ester-based, etc.) and the amount thereof. Satisfactory results are obtained by spraying oil in surface densities ("plate-out") of 0.1 to 1 g / m 2 , which is significantly more than is required simply to control the degradation of the rollers .

Conventionnellement, le dispositif de pulvérisation de l'émulsion d'huile est soit un venturi, l'aspiration de l'huile étant réalisée par la dépression créée par de l'eau en mouvement dans le tube principal, soit un mélangeur statique ("static tube mixer") où l'on procède à une injection d'huile dans une zone de tube où le cisaillement (gradient de vitesse) est augmenté grâce à la présence d'"obstacles". Le venturi ou le "static tube mixer" est combiné à une série d'injecteurs dont le nombre est sélectionné en fonction de la largeur de bande à lubrifier (3 à 7 injecteurs pour une bande allant jusqu'à 2 mètres de large).Conventionally, the system of spraying the oil emulsion is either a venturi, the aspiration of the oil being carried out by the depression created by moving water in the main tube, a static mixer ("static tube mixer") where one oil injection into a tube area where the shear (velocity gradient) is increased thanks to the presence of "obstacles". The venturi or the "static tube mixer "is combined with a series of injectors whose number is selected based on the bandwidth at lubricate (3 to 7 injectors for a band up to 2 meters wide).

Le document EP-A-1 193 004 décrit un procédé de lubrification pour laminage à froid comprenant les étapes de : fourniture d'une émulsion d'huile de laminage utilisant un premier dispositif de fourniture de l'huile sous forme d'une émulsion fournie à un cylindre et une bande d'acier selon un mode de recirculation ainsi qu'un deuxième dispositif de fourniture de l'émulsion seulement sur les surfaces avant et arrière de la bande d'acier. Dans le deuxième dispositif, l'huile de laminage est ajoutée à un émulsifiant de même type et même concentration que ceux utilisés pour le premier dispositif, avec un contrôle de taille moyenne de particules pour que celles-ci soient plus grandes que dans le premier dispositif. L'émulsion produite par le second dispositif n'ayant pas adhéré à la bande est récupérée en même temps que l'émulsion produite par le premier dispositif. EP-A-1,193,004 discloses a method of lubrication system for cold rolling comprising steps of: supplying a rolling oil emulsion using a first device for supplying the oil in the form of an emulsion supplied to a cylinder and a steel strip according to a recirculation mode and a second device for supplying the emulsion only on the front and back surfaces of the steel strip. In the second device, the rolling oil is added to an emulsifier of the same type and concentration as those used for the first device, with a control of average size of particles so that they are more large than in the first device. The emulsion produced by the second device not adhered to the band is recovered at the same time as the emulsion produced by the first device.

Le brevet US-A-3 933 660 propose une huile réductrice de lubrification pour laminage à chaud du cuivre et de ses alliages comprenant 1000 parts en poids d'eau, 6 à 200 parts en poids d'activateur de surface anionique de type acide carboxylique, sulfate ou phosphate et 0,8 à 200 parts en poids d'au moins un composé contenant un groupement hydroxyle de type alcool, alkylène glycol ou éther glycol. L'huile de laminage procure au cuivre et à ses alliages une lubrification, une aptitude à enlever un film d'oxyde et une aptitude à prévenir la formation d'un film d'oxyde par une pulvérisation entre le cylindre de laminage et la bande à laminer à chaud.US-A-3,933,660 proposes an oil lubricating reducer for hot rolling of copper and its alloys comprising 1000 parts by weight of water, 6 to 200 parts by weight of anionic surface activator of type carboxylic acid, sulfate or phosphate and 0.8 to 200 parts by weight of at least one compound containing a hydroxyl group of alcohol type, alkylene glycol or ether glycol. Rolling oil provides copper and its alloys a lubrication, an ability to remove a oxide film and an ability to prevent the formation of a oxide film by spraying between the cylinder of rolling and the hot rolling strip.

Le document JP-A-55 151 093 décrit un procédé de lubrification en laminage à froid d'une bande recouverte par un composé organique polaire où l'on pulvérise une émulsion d'huile et d'une composition comprenant un composé organique polaire tel que l'acide stéarique. L'émulsion d'huile excédentaire est enlevée par essorage après formation d'une couche d'huile adsorbée à la surface de la bande.JP-A-55 151 093 describes a process lubrication in cold rolling of a covered strip by a polar organic compound which is sprayed with a emulsion of oil and a composition comprising a compound polar organic such as stearic acid. The emulsion excess oil is removed by spinning after formation of an adsorbed oil layer on the surface of the bandaged.

Les principaux inconvénients inhérents à ces dispositifs de pulvérisation d'une émulsion d'huile, utilisés à l'échelle industrielle, sont les suivants :

  • l'interaction huile-eau, qui est fonction du type d'huile et de la "qualité" de l'eau, détermine le temps d'adhésion de l'huile sur le cylindre, ainsi que la quantité adhérente. L'efficacité des dispositifs utilisés n'est donc pas aisément prévisible ;
  • les performances des émulsions instables utilisées sont hautement corrélées à la capacité de maintenir une bonne dispersion de l'huile dans l'eau, ou en d'autres termes à la valeur et à la stabilité au cours du temps du taux de cisaillement obtenu, lequel est corrélé au gradient de vitesse, qui est fonction à la fois de la longueur et du diamètre du tube utilisé ainsi que du débit de l'émulsion. Il est en fait difficile de maintenir cette stabilité entre le "static tube mixer" et les différents injecteurs ; en d'autres termes, il est difficile d'assurer la contrôlabilité du coefficient de frottement obtenu ;
  • la mise en contact de l'huile et de l'eau conduit généralement à des réactions formant une phase polymérique dure et collante, bouchant les tuyaux d'admission et les injecteurs.
The main disadvantages inherent to these spraying devices of an oil emulsion, used on an industrial scale, are the following:
  • the oil-water interaction, which is a function of the type of oil and the "quality" of the water, determines the time of adhesion of the oil to the cylinder, as well as the adhering amount. The effectiveness of the devices used is therefore not easily predictable;
  • the performance of the unstable emulsions used is highly correlated with the ability to maintain a good dispersion of the oil in the water, or in other words the value and stability over time of the shear rate obtained, which is correlated with the speed gradient, which is a function of both the length and the diameter of the tube used as well as the flow rate of the emulsion. It is actually difficult to maintain this stability between the "static tube mixer" and the different injectors; in other words, it is difficult to ensure the controllability of the coefficient of friction obtained;
  • the contacting of the oil with the water generally leads to reactions forming a hard and sticky polymeric phase, blocking the intake pipes and the injectors.

Buts de l'inventionGoals of the invention

La présente invention vise à fournir une solution qui s'affranchisse des inconvénients de l'état de la technique tels que l'impossibilité de contrôler et maítriser la concentration et la stabilité de l'émulsion huile-eau, le bouchage des tuyaux d'admission de l'émulsion par formation de résidus organiques solides, l'influence de la vitesse de flux spécifique, etc.The present invention aims to provide a solution that overcomes the disadvantages of the state of technique such as the inability to control and control the concentration and stability of the emulsion oil-water, clogging of the intake pipes of the emulsion by formation of solid organic residues, the influence of the specific flow rate, etc.

L'invention a notamment pour but de proposer un nouveau procédé de lubrification des cylindres de laminage permettant de maintenir constant ou en tout cas sous contrôle le frottement à l'échelle industrielle.The object of the invention is in particular to propose a new process of lubricating the cylinders of rolling to maintain constant or in any case under control the friction on an industrial scale.

L'invention a encore pour but d'augmenter l'efficacité de l'accrochage de l'huile de lubrification sur les cylindres.The invention also aims to increase the effectiveness of the attachment of the lubricating oil on the cylinders.

L'invention a encore pour but d'augmenter l'homogénéisation de la répartition de l'huile sur les cylindres.The invention also aims to increase the homogenisation of the distribution of the oil on the cylinders.

Principaux éléments caractéristiques de l'inventionMain characteristic elements of the invention

Un premier objet de la présente invention se rapporte à une installation de lubrification en ligne de cylindres de laminage, de préférence à chaud, d'une bande métallique, de préférence en acier, ladite lubrification étant essentiellement réalisée par pulvérisation ou atomisation d'un lubrifiant ou d'un mélange de lubrifiants sur une cible comprenant lesdits cylindres et/ou ladite bande, de préférence au voisinage de l'interstice des cylindres de travail, caractérisée en ce qu'elle comprend un caisson essentiellement fermé muni :

  • d'un moyen de formation d'un nuage de gouttelettes de lubrifiant de taille inférieure à 2 mm, de préférence inférieure à 700 µm, et de préférence encore inférieure à 200 µm ;
  • d'un diaphragme à ouverture réglable associé audit moyen et placé sur une face avant du caisson et
  • d'un dispositif de récupération de lubrifiant excédentaire sur la partie du diaphragme interne au caisson et sur les parois internes du caisson.
A first object of the present invention relates to an in-line lubrication plant for rolling rolls, preferably hot, of a metal strip, preferably steel, said lubrication being essentially carried out by spraying or atomizing a lubricant. or a mixture of lubricants on a target comprising said rolls and / or said strip, preferably in the vicinity of the gap of the working rolls, characterized in that it comprises a substantially closed box provided with:
  • means for forming a cloud of lubricant droplets smaller than 2 mm, preferably less than 700 μm, and more preferably less than 200 μm;
  • an adjustable aperture diaphragm associated with said means and placed on a front face of the housing and
  • an excess lubricant recovery device on the part of the diaphragm internal to the box and on the internal walls of the box.

Selon l'invention, ledit lubrifiant possède une pureté d'au moins 95% et une température d'ébullition supérieure à 130°C, et de préférence une température d'ébullition supérieure à 300°C et un point éclair supérieur à 180°C. Cette exigence exclut donc l'eau en tant que lubrifiant ainsi que les émulsions d'huile dans l'eau. A la limite, des traces d'eau présentes dans le lubrifiant, dans les limites de pureté de celui-ci, peuvent être tolérées.According to the invention, said lubricant possesses a purity of at least 95% and a boiling temperature greater than 130 ° C, and preferably a temperature boiling above 300 ° C and a flash point greater than 180 ° C. This requirement therefore excludes water as lubricant as well as oil emulsions in the water. At the limit, traces of water present in the lubricant, within its purity, may to be tolerated.

L'installation de l'invention est munie de moyens de contrôle de la température du caisson, de préférence comprenant une résistance électrique ou un circuit d'eau. Le contrôle de la température procure une meilleure contrôlabilité du procédé en général et notamment permet de réduire les problèmes liés à la viscosité du lubrifiant. The installation of the invention is provided with means of controlling the temperature of the box, preferably comprising an electrical resistance or a water circuit. Temperature control provides a better controllability of the process in general and in particular reduces the problems related to the viscosity of the lubricant.

De manière particulièrement avantageuse, lesdits moyens de contrôle de la température sont associés à l'utilisation d'un lubrifiant solide à la température ambiante et liquide à une température de travail de l'installation supérieure à la température ambiante.In a particularly advantageous manner, said temperature control means are associated to the use of a solid lubricant at temperature ambient and liquid at a working temperature of installation above room temperature.

Toujours selon l'invention, ledit moyen de formation d'un nuage de gouttelettes comprend au moins un gicleur ou injecteur sans air, de préférence un gicleur de type à cône plein, ou un atomiseur à mélange interne ou externe de lubrifiant en suspension dans l'air ou un gaz inerte ou encore un atomiseur à ultrasons.Still according to the invention, said means of formation of a cloud of droplets comprises at least one nozzle or injector without air, preferably a jet of full cone type, or an internal mixing atomizer or external lubricant suspended in air or gas inert or an ultrasonic atomizer.

Avantageusement, l'installation comprend une pluralité de gicleurs ou injecteurs ou atomiseurs répartis sur la largeur de la ligne de laminage, dont certains peuvent être rendus non opérationnels pour s'adapter à la largeur effective de la bande et/ou à la quantité surfacique de lubrifiant à déposer.Advantageously, the installation comprises a plurality of nozzles or injectors or atomizers distributed the width of the rolling line, some of which can be made non-operational to adapt to the effective width of the band and / or quantity surface of lubricant to be deposited.

De préférence encore, l'installation comprend des moyens pour couper lesdits gicleurs, soit un sur deux, soit aléatoirement.More preferably, the installation comprises means for cutting said sprinklers, ie one out of two, either randomly.

Avantageusement, le caisson est subdivisé en au moins deux parties, chaque partie comprenant un diaphragme et un dispositif associé de récupération de lubrifiant.Advantageously, the box is subdivided into at least two parts, each part comprising a diaphragm and an associated device for recovering lubricant.

Selon une modalité d'exécution préférée, le dispositif de récupération de lubrifiant excédentaire et/ou le(s) diaphragme(s) est (sont) réalisé(s) dans un matériau percé d'une pluralité de trous ou dans un matériau poreux.According to a preferred embodiment, the excess lubricant recovery device and / or the diaphragm (s) is (are) made of a material pierced with a plurality of holes or in a porous material.

Selon une autre modalité d'exécution préférée, le dispositif de récupération de lubrifiant excédentaire comprend un circuit fermé de circulation de lubrifiant muni d'équipements de pompage et éventuellement de recyclage du lubrifiant. According to another execution modality preferred, the lubricant recovery device surplus includes a closed circuit for the circulation of lubricant with pumping equipment and possibly lubricant recycling.

Il résulte des caractéristiques de l'invention que l'atmosphère du caisson est confinée.It results from the characteristics of the invention that the atmosphere of the box is confined.

Une caractéristique additionnelle de l'invention est que l'angle de pulvérisation, l'ouverture du ou des diaphragmes, ainsi que leur nombre sur la face avant du caisson, de même qu'éventuellement les dimensions du caisson, sont choisis en fonction de la largeur des cylindres et/ou de la bande à lubrifier et de la vitesse de la bande.An additional feature of the invention is that the spray angle, the opening the diaphragm (s) and their number on the face front of the box, as well as possibly the dimensions of the box, are chosen according to the width of the cylinders and / or the tape to be lubricated and the speed of the band.

Avantageusement, l'installation de l'invention comprend des moyens pour augmenter l'ouverture du (des) diaphragme(s) avec la vitesse de défilement de la bande, qui est également égale à la vitesse tangentielle des cylindres.Advantageously, the installation of the invention comprises means for increasing the opening of the diaphragm (s) with the scroll speed of the band, which is also equal to the tangential speed cylinders.

Toujours avantageusement, les parois internes du caisson sont réalisées dans un matériau permettant l'aspiration du lubrifiant.Always advantageously, the internal walls of the box are made of a material allowing suction of the lubricant.

Dans le contexte de l'invention, la bande défile à une vitesse pouvant aller de 0,5 à 20 m/s.In the context of the invention, the band scrolls at a speed ranging from 0.5 to 20 m / s.

Un deuxième objet de la présente invention se rapporte à un procédé de lubrification en ligne de cylindres de laminage, de préférence à chaud, d'une bande métallique, de préférence en acier, ladite lubrification étant essentiellement réalisée par pulvérisation ou atomisation d'un lubrifiant ou d'un mélange de lubrifiants sur une cible comprenant lesdits cylindres et/ou ladite bande, de préférence au voisinage de l'interstice des cylindres de travail, mettant en oeuvre une installation selon l'une quelconque des revendications précédentes,
caractérisé par les étapes suivantes :

  • on règle les paramètres d'injection de lubrifiant, notamment la pression et la température, de manière à obtenir le débit de lubrifiant désiré ;
  • on règle l'ouverture du (ou des) diaphragme(s) en fonction de la quantité surfacique de lubrifiant à déposer et de la vitesse de la bande ;
  • on récupère par récolte et pompage le lubrifiant excédentaire et on renvoie celui-ci en circuit fermé dans le caisson, éventuellement après recyclage.
A second subject of the present invention relates to a process for the in-line lubrication of rolling rolls, preferably hot rolls, of a metal strip, preferably made of steel, said lubrication being essentially carried out by spraying or atomizing a lubricant. or a mixture of lubricants on a target comprising said rolls and / or said strip, preferably in the vicinity of the gap of the working rolls, implementing an installation according to any one of the preceding claims,
characterized by the following steps:
  • the lubricant injection parameters, in particular the pressure and the temperature, are adjusted so as to obtain the desired lubricant flow rate;
  • the opening of the diaphragm (s) is adjusted according to the surface quantity of lubricant to be deposited and the speed of the strip;
  • the excess lubricant is recovered by harvesting and pumping and the latter is returned in closed circuit to the box, possibly after recycling.

Il est essentiel selon l'invention que l'ouverture du ou des diaphragmes soit réglée pour déposer sur la cible une quantité surfacique ("plate-out") de lubrifiant comprise entre 0,01 et 1 g/m2.It is essential according to the invention that the opening of the diaphragm or diaphragms is adjusted to deposit on the target a surface amount ("plate-out") of lubricant of between 0.01 and 1 g / m 2 .

Avantageusement, les paramètres d'injection de lubrifiant sont régulés en boucle ouverte ou fermée.Advantageously, the injection parameters of lubricant are regulated in open or closed loop.

Brève description des figuresBrief description of the figures

La figure 1 représente schématiquement un gicleur pour atomisation d'huile dans l'air, à mélange interne, selon l'état de la technique.Figure 1 schematically represents a nozzle for atomizing oil in the air, mixing internal, according to the state of the art.

La figure 2 représente schématiquement une première forme d'exécution préférée de la présente invention.Figure 2 schematically represents a first preferred embodiment of this invention.

La figure 3 représente schématiquement une deuxième forme d'exécution préférée de la présente invention.Figure 3 schematically represents a second preferred embodiment of this invention.

La figure 4 représente schématiquement une troisième forme d'exécution préférée de la présente invention.Figure 4 schematically represents a third preferred embodiment of this invention.

Description d'une forme d'exécution préférée de l'inventionDescription of a preferred embodiment of the invention

L'idée à la base de la présente invention est l'utilisation combinée dans un dispositif de lubrification d'un moyen permettant de pulvériser de fines gouttelettes de lubrifiant et d'un diaphragme muni d'un système de récupération d'huile. The idea behind the present invention is combined use in a lubrication device a means for spraying fine droplets of lubricant and a diaphragm equipped with a oil recovery.

Comme représenté sur les figures 2 à 4, la présente invention concerne plus précisément une installation de lubrification à pulvérisation comprenant un pulvérisateur (ou vaporisateur) 1 de lubrifiant pur ou d'un mélange de lubrifiants tels que les lubrifiants à base carbone, silicone, voire le bisulfure de molybdène. Ce ou ces lubrifiants possèdent un degré d'impuretés ou d'additifs habituel pour les produits de ce type disponibles dans le commerce (ex. maximum 5%). De préférence, la pulvérisation est réalisée en présence d'air. Les lubrifiants seront choisis dans le cadre de la présente invention de sorte à avoir une température d'ébullition supérieure à 130 °C.As shown in FIGS. 2 to 4, the The present invention relates more specifically to a spray lubrication system comprising a sprayer (or vaporizer) 1 of pure lubricant or a mixture of lubricants such as lubricants-based carbon, silicone or even molybdenum disulfide. This or these lubricants have a degree of impurities or usual additives for products of this type commercially available (eg maximum 5%). Of preferably, the spraying is carried out in the presence air. Lubricants will be chosen as part of the present invention so as to have a temperature boiling above 130 ° C.

Ce système est basé sur l'utilisation combinée dans un caisson 1 de pulvérisation :

  • d'un moyen de pulvérisation 10 ;
  • d'un ou plusieurs diaphragmes 3,3' à ouverture réglable permettant d'ajuster la quantité de lubrifiant sortant du pulvérisateur ;
  • d'un système de récupération 4 de l'excédent de lubrifiant sur la partie interne du ou des diaphragmes et/ou sur la surface interne du caisson 1. Ce système de récupération peut être réalisé dans un matériau percé de multiples trous ou dans un matériau poreux. Le diaphragme peut lui-même être réalisé dans le même matériau.
This system is based on the combined use in a spray box 1:
  • a spraying means 10;
  • one or more diaphragms 3,3 'with adjustable opening to adjust the amount of lubricant coming out of the sprayer;
  • a recovery system 4 of excess lubricant on the inner part of the diaphragm or diaphragms and / or on the inner surface of the casing 1. This recovery system can be made of a material pierced with multiple holes or in a material porous. The diaphragm may itself be made of the same material.

La fonction du caisson de pulvérisation 1 est de confiner l'atmosphère réalisée par le brouillard de pulvérisation.The function of the spray box 1 is to confine the atmosphere created by the fog of spray.

Dans le cadre de la présente invention, on entend par "pulvérisation" soit une pulvérisation, soit une atomisation, c'est-à-dire la réduction du lubrifiant, au départ à l'état liquide, en fines gouttelettes, respectivement en présence ou non d'air sous pression, conduisant à une taille de gouttelettes allant de quelques microns à plusieurs millimètres, par exemple 2 mm, selon la technologie particulière employée.In the context of the present invention, "spray" means either a spray or a spray atomisation, ie the reduction of the lubricant, at starting in the liquid state, in fine droplets, respectively in the presence or absence of air under pressure, leading to a droplet size ranging from a few microns to several millimeters, for example 2 mm, depending on the particular technology employed.

Ainsi le moyen de pulvérisation précité 10, qui définit la taille des gouttelettes produites, peut être, selon des formes d'exécution préférées de l'invention :

  • soit un gicleur muni d'orifices de sortie de diamètre élevé, produisant des gouttelettes dont le diamètre est de l'ordre de 1 à 3 mm, plutôt adapté aux débits de pulvérisation importants ;
  • soit un injecteur (sans air), de préférence un gicleur de type à cône plein, présentant des orifices de sortie de diamètre allant de 100 à 150 microns typiquement ; les gouttelettes produites sont distribuées de manière gaussienne avec une taille maximale inférieure à 700 microns environ ;
  • soit un atomiseur à mélange interne ou externe (air) permettant d'obtenir une taille (diamètre) de gouttelettes inférieure à 200 microns environ ;
  • soit un atomiseur à ultrasons permettant de créer une pulvérisation très précise en débit et en géométrie.
Thus the aforementioned spraying means 10, which defines the size of the droplets produced, may be, according to preferred embodiments of the invention:
  • either a nozzle provided with high diameter outlet orifices, producing droplets whose diameter is of the order of 1 to 3 mm, rather adapted to large spray rates;
  • either an injector (without air), preferably a solid cone type nozzle, having outlet orifices of diameter typically ranging from 100 to 150 microns; the droplets produced are distributed in a Gaussian manner with a maximum size of less than about 700 microns;
  • an internal or external mixing atomizer (air) for obtaining a size (diameter) of droplets of less than about 200 microns;
  • an ultrasonic atomizer to create a very precise spray rate and geometry.

Ces types de dispositifs n'induisent aucune limitation en pression, ni en température, mais ils doivent être régulés.These types of devices do not induce any limitation in pressure or temperature, but they must to be regulated.

On a représenté à la figure 1 un atomiseur huile/air à mélange interne connu dans l'état de la technique et pouvant avantageusement servir de moyen de pulvérisation 10 selon la présente invention. L'air 12 est injecté selon une couronne 12' entourant le flux d'huile 11, ce qui permet l'obtention d'un nuage conique 20 d'atomisation. Selon le principe de l'atomisation, le nuage de gouttelettes est formé grâce au choc se produisant entre l'huile provenant du gicleur d'huile 11 et l'air (ou un gaz inerte) injecté 12, l'huile étant dispersée dans l'air juste avant la sortie de l'huile de l'atomiseur.FIG. 1 shows an atomizer oil / air with internal mixing known in the state of the and can advantageously serve as a means of Spray 10 according to the present invention. The air 12 is injected according to a ring 12 'surrounding the flow of oil 11, which makes it possible to obtain a conical cloud 20 atomization. According to the principle of atomization, the cloud of droplets is formed by the shock occurring between the oil from the oil nozzle 11 and the air (or a gas inert) injected 12, the oil being dispersed in the air just before the release of the oil from the atomizer.

Dans le cas des atomiseurs à mélange externe, le flux d'huile est ajustable en modifiant la pression d'huile, la pression d'air pouvant être ajustée séparément.In the case of external mixing atomizers, the oil flow is adjustable by changing the pressure of oil, the air pressure can be adjusted separately.

La figure 2 montre un pulvérisateur selon une première modalité préférée de l'invention, comportant un seul diaphragme 3, tandis que la figure 3 montre un pulvérisateur selon une deuxième modalité préférée de l'invention, comportant deux diaphragmes 3,3'.Figure 2 shows a sprayer according to a first preferred embodiment of the invention, comprising a only diaphragm 3, while figure 3 shows a sprayer according to a second preferred mode of the invention, comprising two diaphragms 3,3 '.

Les diaphragmes intermédiaires 3', comme installés à la figure 3, ont pour but de :

  • réduire la hauteur du caisson de pulvérisation ;
  • limiter la quantité de brouillard sortant du pulvérisateur.
The intermediate diaphragms 3 ', as installed in FIG. 3, aim to:
  • reduce the height of the spray box;
  • limit the amount of mist coming out of the sprayer.

Les parois latérales internes du caisson peuvent être recouvertes d'un matériau commun 5 ou alternativement d'un matériau 5 permettant l'aspiration du lubrifiant, comme représenté à la figure 4.The internal side walls of the box may be covered with a common material 5 or alternatively a material allowing the suction of the lubricant, as shown in Figure 4.

Selon une modalité particulière de réalisation de l'invention, l'excédent d'huile ou lubrifiant, se trouvant sur les parois internes et sur le diaphragme, est aspiré à l'extérieur, recyclé et réintroduit dans le dispositif de lubrification.According to a particular modality embodiment of the invention, the excess oil or lubricant, located on the inner walls and on the diaphragm, is sucked outside, recycled and reintroduced into the lubrication device.

La présente invention présente les avantages suivants :

  • élimination de l'interaction eau-huile, d'où meilleure contrôlabilité et meilleure efficacité du procédé, avec, le cas échéant, élimination du problème de bouchage des tubes ;
  • possibilité d'utiliser des lubrifiants se trouvant à l'état solide à température ambiante, en les préchauffant initialement ;
  • possibilité d'utiliser des lubrifiants purs ou des émulsions très concentrées en lubrifiant ;
  • homogénéisation de la distribution d'huile sur la surface des cylindres ;
  • optimisation de l'efficacité d'accrochage de l'huile sur le cylindre. En effet, la meilleure condition de pulvérisation est choisie puis l'ouverture du diaphragme est réglée pour laisser passer la quantité désirée d'huile. L'ouverture du diaphragme peut suivre l'augmentation de la vitesse des cylindres. Le seul paramètre libre du système est donc l'ouverture du (des) diaphragme(s). Les mesures effectuées ont permis de constater que l'efficacité de l'atomisation reste dans une large mesure constante en fonction de l'importance du dépôt surfacique d'huile, au contraire de la pulvérisation d'émulsions stables qui subissent un phénomène de ruissellement aux dépôts surfaciques élevés.
The present invention has the following advantages:
  • elimination of the water-oil interaction, hence better controllability and better efficiency of the process, with, where appropriate, eliminating the problem of clogging of the tubes;
  • possibility of using lubricants in the solid state at room temperature, initially preheating them;
  • possibility of using pure lubricants or emulsions with a high concentration of lubricant;
  • homogenization of the oil distribution on the surface of the rolls;
  • optimization of the efficiency of attachment of the oil on the cylinder. Indeed, the best spraying condition is chosen and the aperture of the diaphragm is adjusted to let the desired amount of oil. The opening of the diaphragm can follow the increase in the speed of the cylinders. The only free parameter of the system is thus the opening of the diaphragm (s). The measurements carried out have made it possible to observe that the efficiency of the atomization remains to a large extent constant as a function of the importance of the surface deposition of oil, unlike the spraying of stable emulsions which undergo a runoff phenomenon at the same time. high surface deposits.

Claims (18)

Installation de lubrification en ligne de cylindres de laminage, de préférence à chaud, d'une bande métallique, de préférence en acier, ladite lubrification étant essentiellement réalisée par pulvérisation ou atomisation d'un lubrifiant ou d'un mélange de lubrifiants sur une cible comprenant lesdits cylindres et/ou ladite bande, de préférence au voisinage de l'interstice des cylindres de travail, caractérisée en ce qu'elle comprend un caisson (1) essentiellement fermé muni : d'un moyen (10) de formation d'un nuage de gouttelettes de lubrifiant de taille inférieure à 2 mm, de préférence inférieure à 700 µm, et de préférence encore inférieure à 200 µm ; d'un diaphragme (3,3') à ouverture réglable associé audit moyen (10) et placé sur une face avant du caisson et d'un dispositif de récupération de lubrifiant excédentaire (4) sur la partie du diaphragme interne au caisson et sur les parois internes du caisson. In-line lubrication system for rolling rolls, preferably hot-rolled, of a metal strip, preferably of steel, said lubrication being essentially carried out by spraying or atomizing a lubricant or a mixture of lubricants on a target comprising said cylinders and / or said band, preferably in the vicinity of the interstice of the working rolls, characterized in that it comprises a substantially closed box (1) provided with: means (10) for forming a cloud of lubricant droplets less than 2 mm in size, preferably less than 700 μm, and more preferably less than 200 μm; a diaphragm (3,3 ') with adjustable opening associated with said means (10) and placed on a front face of the box and an excess lubricant recovery device (4) on the portion of the diaphragm internal to the box and on the inner walls of the box. Installation selon la revendication 1, caractérisé en ce que ledit lubrifiant possède une pureté d'au moins 95% et une température d'ébullition supérieure à 130 °C, et de préférence une température d'ébullition supérieure à 300 °C et un point éclair supérieur à 180 °C.Plant according to claim 1, characterized in that said lubricant has a purity of at least 95% and a boiling point above 130 ° C, and preferably a boiling point above 300 ° C and a flash point greater than 180 ° C. Installation selon la revendication 1 ou 2, caractérisée en ce qu'elle est munie de moyens de contrôle de la température du caisson (1), de préférence comprenant une résistance électrique ou un circuit d'eau.Installation according to claim 1 or 2, characterized in that it is provided with means for controlling the temperature of the box (1), preferably comprising an electrical resistance or a water circuit. Installation selon la revendication 3, caractérisée en ce que lesdits moyens de contrôle de la température sont associés à l'utilisation d'un lubrifiant solide à la température ambiante et liquide à une température de travail supérieure à la température ambiante.Installation according to claim 3, characterized in that said temperature control means are associated with the use of a solid lubricant at ambient and liquid temperature at a working temperature higher than the ambient temperature. Installation selon l'une quelconque des revendications précédentes, caractérisée en ce que ledit moyen (10) de formation d'un nuage de gouttelettes comprend au moins un gicleur ou injecteur sans air, de préférence un gicleur de type à cône plein, ou un atomiseur à mélange interne ou externe de lubrifiant en suspension dans l'air ou dans un gaz inerte ou encore un atomiseur à ultrasons.Installation according to any one of the preceding claims, characterized in that said means (10) for forming a cloud of droplets comprises at least one nozzle or injector without air, preferably a full cone-type nozzle, or an atomizer with internal or external mixing of lubricant suspended in air or in an inert gas or an ultrasonic atomizer. Installation selon la revendication 5, caractérisée en ce qu'elle comprend une pluralité de gicleurs ou injecteurs ou atomiseurs répartis sur la largeur de la ligne de laminage, dont certains peuvent être rendus non opérationnels pour s'adapter à la largeur effective de la bande et/ou à la quantité surfacique de lubrifiant à déposer.Installation according to claim 5, characterized in that it comprises a plurality of nozzles or injectors or atomizers distributed over the width of the rolling line, some of which may be rendered non-operational in order to adapt to the effective width of the strip and or the surface quantity of lubricant to be deposited. Installation selon la revendication 6, caractérisée en ce qu'elle comprend des moyens pour couper lesdits gicleurs, soit un sur deux, soit aléatoirement.Installation according to claim 6, characterized in that it comprises means for cutting said nozzles, either one out of two, or randomly. Installation selon l'une quelconque des revendications 1 à 7, caractérisé en ce que le caisson (1) est subdivisé en au moins deux parties, chaque partie comprenant un diaphragme (3,3') et un dispositif associé de récupération de lubrifiant (4).Installation according to any one of claims 1 to 7, characterized in that the box (1) is subdivided into at least two parts, each part comprising a diaphragm (3,3 ') and an associated lubricant recovery device (4). ). Installation selon l'une quelconque des revendications précédentes, caractérisé en ce que le dispositif de récupération de lubrifiant excédentaire (4) et/ou le(s) diaphragme(s) (3,3') est (sont) réalisé(s) dans un matériau percé d'une pluralité de trous ou dans un matériau poreux.Installation according to one of the preceding claims, characterized in that the excess lubricant recovery device (4) and / or the diaphragm (s) (3,3 ') is (are) embodied in a material pierced with a plurality of holes or in a porous material. Installation selon l'une quelconque des revendications précédentes caractérisé en ce que le dispositif de récupération de lubrifiant excédentaire (4) comprend un circuit fermé de circulation de lubrifiant muni d'équipements de pompage et éventuellement de recyclage du lubrifiant.Installation according to any one of the preceding claims, characterized in that the excess lubricant recovery device (4) comprises a closed lubricant circulation circuit provided with pumping equipment and optionally recycling of the lubricant. Installation selon l'une quelconque des revendications précédentes, caractérisé en ce que l'atmosphère du caisson est confinée.Installation according to any one of the preceding claims, characterized in that the atmosphere of the box is confined. Installation selon l'une quelconque des revendications précédentes, caractérisé en ce que l'angle de pulvérisation, l'ouverture du ou des diaphragmes, ainsi que leur nombre sur la face avant du caisson, de même qu'éventuellement les dimensions du caisson, sont choisis en fonction de la largeur des cylindres et/ou de la bande à lubrifier et de la vitesse de la bande.Installation according to any one of the preceding claims, characterized in that the spray angle, the opening of the diaphragm or diaphragms and their number on the front face of the box, as well as possibly the dimensions of the box, are chosen according to the width of the rolls and / or the strip to be lubricated and the speed of the strip. Installation selon la revendication 12, caractérisé en ce qu'elle comprend des moyens pour augmenter l'ouverture du (des) diaphragme(s) avec la vitesse de défilement de la bande, qui est également égale à la vitesse tangentielle des cylindres.Installation according to claim 12, characterized in that it comprises means for increasing the opening of the diaphragm (s) with the running speed of the strip, which is also equal to the tangential speed of the rolls. Installation selon l'une quelconque des revendications précédentes, caractérisé en ce que les parois internes du caisson sont réalisées dans un matériau (5) permettant l'aspiration du lubrifiant.Installation according to any one of the preceding claims, characterized in that the internal walls of the box are made of a material (5) allowing the suction of the lubricant. Installation selon l'une quelconque des revendications précédentes, caractérisé en ce que la bande défile à une vitesse allant de 0,5 à 20 m/s.Installation according to any one of the preceding claims, characterized in that the strip travels at a speed ranging from 0.5 to 20 m / s. Procédé de lubrification en ligne de cylindres de laminage, de préférence à chaud, d'une bande métallique, de préférence en acier, ladite lubrification étant essentiellement réalisée par pulvérisation ou atomisation d'un lubrifiant ou d'un mélange de lubrifiants sur une cible comprenant lesdits cylindres et/ou ladite bande, de préférence au voisinage de l'interstice des cylindres de travail, mettant en oeuvre une installation selon l'une quelconque des revendications précédentes, caractérisé par les étapes suivantes : on règle les paramètres d'injection de lubrifiant, notamment la pression et la température, de manière à obtenir le débit de lubrifiant désiré ; on règle l'ouverture du (ou des) diaphragme(s) en fonction de la quantité surfacique de lubrifiant à déposer et de la vitesse de la bande ; on récupère par récolte et pompage le lubrifiant excédentaire et on renvoie celui-ci en circuit fermé dans le caisson, éventuellement après recyclage. A method of in-line lubrication of rolling rolls, preferably hot rolling, of a metal strip, preferably steel, said lubrication being essentially carried out by spraying or atomizing a lubricant or a mixture of lubricants on a target comprising said cylinders and / or said band, preferably in the vicinity of the interstice of the working rolls, implementing an installation according to any one of the preceding claims, characterized by the following steps: the lubricant injection parameters, in particular the pressure and the temperature, are adjusted so as to obtain the desired lubricant flow rate; the opening of the diaphragm (s) is adjusted according to the surface quantity of lubricant to be deposited and the speed of the strip; the excess lubricant is recovered by harvesting and pumping and the latter is returned in closed circuit to the box, possibly after recycling. Procédé selon la revendication 16, caractérisé en ce que l'ouverture du ou des diaphragmes est réglée pour déposer sur la cible une quantité surfacique ("plate-out") de lubrifiant comprise entre 0,01 et 1 g/m2.Method according to claim 16, characterized in that the opening of the diaphragm or diaphragms is adjusted to deposit on the target a surface amount ("plate-out") of lubricant of between 0.01 and 1 g / m 2 . Procédé selon la revendication 16 ou 17, caractérisé en ce que les paramètres d'injection de lubrifiant sont régulés en boucle ouverte ou fermée.Method according to Claim 16 or 17, characterized in that the lubricant injection parameters are regulated in open or closed loop.
EP04447085A 2003-09-08 2004-04-02 Method and device for lubricating rolling rolls Expired - Lifetime EP1512469B1 (en)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
BE200300480 2003-09-08
BE2003/0480A BE1015673A3 (en) 2003-09-08 2003-09-08 Method and system for rolling cylinder lubrication.

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EP1512469A1 true EP1512469A1 (en) 2005-03-09
EP1512469B1 EP1512469B1 (en) 2008-04-02

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AT (1) ATE390963T1 (en)
BE (1) BE1015673A3 (en)
DE (1) DE602004012810T2 (en)
ES (1) ES2301960T3 (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009046505A1 (en) * 2007-10-08 2009-04-16 Centre De Recherches Metallurgiques Asbl - Centrum Voor Research In De Metallurgie Vzw Spray lubrication unit and method for rolling cylinders

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102018117405A1 (en) 2018-07-18 2020-01-23 Kme Mansfeld Gmbh Process for descaling a copper raw material for manufacturing a copper product and copper product

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2019689A1 (en) * 1970-04-23 1971-11-11 Schmid Rudolf Josef Oil spray application device for rolls in rolling mills
DE2063878A1 (en) * 1970-12-24 1972-08-31 Schmid, Rudolf Josef, 2800 Bremen Roll stand sprayer - using several nozzle units mounted on a common support to spray steam-heated air/oil mixture
EP0060374A2 (en) * 1981-03-13 1982-09-22 VOEST-ALPINE Aktiengesellschaft Apparatus for lubricating strip or web sheet metal
JPS60223603A (en) * 1984-04-19 1985-11-08 Sumitomo Metal Ind Ltd Cold rolling method of thin steel strip
WO1988009230A1 (en) * 1987-05-28 1988-12-01 Edwards William J Coolant flow control
EP0369007A1 (en) * 1987-03-10 1990-05-23 Nippon Kokan Kabushiki Kaisha Lubricating method for hot rolling of high-silicon steel
EP1193004A1 (en) * 2000-03-09 2002-04-03 Nkk Corporation Rolling oil supplying method for cold rolling

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE2019689A1 (en) * 1970-04-23 1971-11-11 Schmid Rudolf Josef Oil spray application device for rolls in rolling mills
DE2063878A1 (en) * 1970-12-24 1972-08-31 Schmid, Rudolf Josef, 2800 Bremen Roll stand sprayer - using several nozzle units mounted on a common support to spray steam-heated air/oil mixture
EP0060374A2 (en) * 1981-03-13 1982-09-22 VOEST-ALPINE Aktiengesellschaft Apparatus for lubricating strip or web sheet metal
JPS60223603A (en) * 1984-04-19 1985-11-08 Sumitomo Metal Ind Ltd Cold rolling method of thin steel strip
EP0369007A1 (en) * 1987-03-10 1990-05-23 Nippon Kokan Kabushiki Kaisha Lubricating method for hot rolling of high-silicon steel
WO1988009230A1 (en) * 1987-05-28 1988-12-01 Edwards William J Coolant flow control
EP1193004A1 (en) * 2000-03-09 2002-04-03 Nkk Corporation Rolling oil supplying method for cold rolling

Non-Patent Citations (1)

* Cited by examiner, † Cited by third party
Title
PATENT ABSTRACTS OF JAPAN vol. 010, no. 083 (M - 466) 2 April 1986 (1986-04-02) *

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2009046505A1 (en) * 2007-10-08 2009-04-16 Centre De Recherches Metallurgiques Asbl - Centrum Voor Research In De Metallurgie Vzw Spray lubrication unit and method for rolling cylinders
BE1017806A3 (en) * 2007-10-08 2009-07-07 Ct Rech Metallurgiques Asbl ATOMIZATION LUBRICATION SYSTEM AND METHOD FOR ROLLING CYLINDERS.
US8544608B2 (en) 2007-10-08 2013-10-01 Centre De Recherches Metallurgiques Asbl Spray lubrication unit and method for rolling cylinders

Also Published As

Publication number Publication date
BE1015673A3 (en) 2005-07-05
ATE390963T1 (en) 2008-04-15
ES2301960T3 (en) 2008-07-01
DE602004012810D1 (en) 2008-05-15
EP1512469B1 (en) 2008-04-02
DE602004012810T2 (en) 2009-04-09

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