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DE827727C - Procedure for magnetic oxygen measurement - Google Patents

Procedure for magnetic oxygen measurement

Info

Publication number
DE827727C
DE827727C DEP595K DEP0000595K DE827727C DE 827727 C DE827727 C DE 827727C DE P595 K DEP595 K DE P595K DE P0000595 K DEP0000595 K DE P0000595K DE 827727 C DE827727 C DE 827727C
Authority
DE
Germany
Prior art keywords
procedure
gas
oxygen
oxygen measurement
measuring
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DEP595K
Other languages
German (de)
Other versions
DE826220C (en
Inventor
Dr Phil Alfred Naumann
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Siemens and Halske AG
Siemens Corp
Original Assignee
Siemens and Halske AG
Siemens Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Siemens and Halske AG, Siemens Corp filed Critical Siemens and Halske AG
Priority to DEP595K priority Critical patent/DE827727C/en
Application granted granted Critical
Publication of DE827727C publication Critical patent/DE827727C/en
Expired legal-status Critical Current

Links

Classifications

    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N27/00Investigating or analysing materials by the use of electric, electrochemical, or magnetic means
    • G01N27/72Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables
    • G01N27/74Investigating or analysing materials by the use of electric, electrochemical, or magnetic means by investigating magnetic variables of fluids

Landscapes

  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Electrochemistry (AREA)
  • Physics & Mathematics (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Investigating Or Analyzing Materials By The Use Of Magnetic Means (AREA)

Description

Verfahren für die magnetische Sauerstoffmessung Der Erfindung liegt die Aufgabe zugrunde, die i7mpfindl ichkeit der magnetischen Sauerstoffanalyse zu erhöhen. Das ist z. B. wichtig für die ltauchgasanalyse auf Sauerstoff, da man für gute Feuerungen immer möglichst kleinen Luftüberschuß anstreben wird, also kleine Meßbereiche wünscht. Ferner ist die Erhöhung der Empfindlichkeit dieser Geräte für Sonderfälle in der chemischen Industrie, z. B. für Katalysatorregenerierung bei der Bunaherstellung, sehr wichtig.Procedure for magnetic oxygen measurement The invention lies the underlying task is to increase the sensitivity of the magnetic oxygen analysis raise. This is e.g. B. important for the analysis of the immersion gas for oxygen, because one for good furnaces will always aim for the smallest possible excess of air, i.e. small ones Desires measuring ranges. It also increases the sensitivity of these devices for Special cases in the chemical industry, e.g. B. for catalyst regeneration the Buna production, very important.

Der Erfindung liegt die Erkenntnis zugrunde, daß die Empfindlichkeit des magnetischen Sauerstoffmessers etwa verdoppelt werden kann, wenn man nicht nur den magnetischen Wind als Meßgröße für den Sauerstoff verwendet, sondern auch die Wärmeleitfähigkeit des Sauerstoffs und beide Effekte sich addieren läßt. Diese Forderung wird dadurch erfüllt, daß die beiden Meßkammern mit Meßgas und die beiden Vergleichskammern mit einem konstanten Gas, z. B. Luft, belüftet werden. The invention is based on the knowledge that the sensitivity of the magnetic oxygen meter can be roughly doubled, if not only uses the magnetic wind as a measure of the oxygen, but also the Thermal conductivity of oxygen and both effects can be added. This requirement is fulfilled in that the two measuring chambers with measuring gas and the two comparison chambers with a constant gas, e.g. B. air, ventilated.

Bei den bekannten Sauerstoffmessern wurden alle vier Kammern mit dem Meßgas belüftet. Der Effekt der Wärmeleitänderung des Gases fiel also heraus, gemessen wurde nur die Abkühlung der Systeme infolge des magnetischen Windes. In the known oxygen meters, all four chambers were with vented to the measuring gas. The effect of the change in thermal conductivity of the gas fell out, only the cooling of the systems as a result of the magnetic wind was measured.

Belüftet man aber gemäß der Erfindung lediglich die Meßkammern mit dem Meßgas und die Vergleichskammern getrennt mit einem konstanten Gas, z. B. Luft, so mißt das Gerät auch den Effekt der Wärmeleitänderung des Meßgases, ähnlich wie der bekannte C O2-Messer. Da nun der magnetische Wind eine Abkühlung der Meßsysteme bei steigender O2-Konzentration herbeiführt und die erhöhte \Märmeleitfähigkeit des Sauerstoffs ebenfalls, so addieren sich die beiden Effekte und bewirken dadurch eine erhöhte Empfindlichkeit des Gerätes auf Sauerstoff. Anzuwenden ist die Erfindung bevorzugt bei der Rauchgasanalyse und bei der technischen 02-Analyse bei hohen Empfindlichkeitsforderungen. However, according to the invention, only the measuring chambers are ventilated the measurement gas and the comparison chambers separated with a constant gas, e.g. B. air, so the device also measures the effect of the change in thermal conductivity of the measuring gas, similar to the well-known C O2 meter. Since now the magnetic wind is cooling down the measuring systems with increasing O2 concentration and the increased \ Fair conductivity of the oxygen as well, then the two effects add up and cause an increased sensitivity of the device to oxygen. The invention is to be applied preferred for flue gas analysis and technical 02 analysis with high sensitivity requirements.

Claims (1)

PATENTANSPRUCH: Verfahren für die magnetische Sauerstoffmessung, dadurch gekennzeichnet, daß die beiden Meßkammern mit Meßgas und die beidenVergleichskammern mit einem konstanten Gas, z. B. Luft, belüftet werden. PATENT CLAIM: Method for magnetic oxygen measurement, characterized in that the two measuring chambers with measuring gas and the two comparison chambers with a constant gas, e.g. B. air, ventilated.
DEP595K 1948-11-26 1948-11-26 Procedure for magnetic oxygen measurement Expired DE827727C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
DEP595K DE827727C (en) 1948-11-26 1948-11-26 Procedure for magnetic oxygen measurement

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DEP595K DE827727C (en) 1948-11-26 1948-11-26 Procedure for magnetic oxygen measurement

Publications (1)

Publication Number Publication Date
DE827727C true DE827727C (en) 1952-01-14

Family

ID=7356718

Family Applications (1)

Application Number Title Priority Date Filing Date
DEP595K Expired DE827727C (en) 1948-11-26 1948-11-26 Procedure for magnetic oxygen measurement

Country Status (1)

Country Link
DE (1) DE827727C (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE959332C (en) * 1953-08-23 1957-03-07 Siemens Ag Arrangement for measuring the deviation of the concentration of gases with a magnetic or electrical dipole moment from a given target value
DE964353C (en) * 1952-07-11 1957-05-23 Hartmann & Braun Ag Process for suppressing the influence of gas properties other than susceptibility on the display of thermomagnetic gas analyzers

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE964353C (en) * 1952-07-11 1957-05-23 Hartmann & Braun Ag Process for suppressing the influence of gas properties other than susceptibility on the display of thermomagnetic gas analyzers
DE959332C (en) * 1953-08-23 1957-03-07 Siemens Ag Arrangement for measuring the deviation of the concentration of gases with a magnetic or electrical dipole moment from a given target value

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