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DE69108600D1 - Verfahren zur Herstellung von e-Caprolacton. - Google Patents

Verfahren zur Herstellung von e-Caprolacton.

Info

Publication number
DE69108600D1
DE69108600D1 DE69108600T DE69108600T DE69108600D1 DE 69108600 D1 DE69108600 D1 DE 69108600D1 DE 69108600 T DE69108600 T DE 69108600T DE 69108600 T DE69108600 T DE 69108600T DE 69108600 D1 DE69108600 D1 DE 69108600D1
Authority
DE
Germany
Prior art keywords
mole
caprolactone
cyclohexanone
hydrogen peroxide
less
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
DE69108600T
Other languages
English (en)
Other versions
DE69108600T2 (de
Inventor
Yukio Inaba
Yohsuke Ueno
Takafumi Hirakawa
Suzuo Takiguchi
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Arkema France SA
Ube Corp
Original Assignee
Elf Atochem SA
Ube Industries Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Elf Atochem SA, Ube Industries Ltd filed Critical Elf Atochem SA
Publication of DE69108600D1 publication Critical patent/DE69108600D1/de
Application granted granted Critical
Publication of DE69108600T2 publication Critical patent/DE69108600T2/de
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D315/00—Heterocyclic compounds containing rings having one oxygen atom as the only ring hetero atom according to more than one of groups C07D303/00 - C07D313/00
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C407/00—Preparation of peroxy compounds
    • C07C407/003—Separation; Purification; Stabilisation; Use of additives
    • C07C407/006—Stabilisation; Use of additives

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Pyrane Compounds (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
DE69108600T 1990-04-25 1991-04-22 Verfahren zur Herstellung von e-Caprolacton. Expired - Fee Related DE69108600T2 (de)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
JP2107674A JPH0798816B2 (ja) 1990-04-25 1990-04-25 ε―カプロラクトンの製造法

Publications (2)

Publication Number Publication Date
DE69108600D1 true DE69108600D1 (de) 1995-05-11
DE69108600T2 DE69108600T2 (de) 1996-01-11

Family

ID=14465118

Family Applications (1)

Application Number Title Priority Date Filing Date
DE69108600T Expired - Fee Related DE69108600T2 (de) 1990-04-25 1991-04-22 Verfahren zur Herstellung von e-Caprolacton.

Country Status (7)

Country Link
US (1) US5250707A (de)
EP (1) EP0454397B1 (de)
JP (1) JPH0798816B2 (de)
CN (1) CN1035379C (de)
AT (1) ATE120742T1 (de)
CA (1) CA2040270A1 (de)
DE (1) DE69108600T2 (de)

Families Citing this family (29)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO1999014190A1 (fr) * 1997-09-16 1999-03-25 Daicel Chemical Industries, Ltd. Procede de preparation de peroxyacide d'equilibre et procede de production de lactone
JP2004143047A (ja) * 2002-10-22 2004-05-20 Daicel Chem Ind Ltd ε−カプロラクトンの製造方法
JP2005139110A (ja) * 2003-11-06 2005-06-02 Ecology Maximum Co Ltd ε−カプロラクトンの製造方法、並びに、ε−カプロラクトンを用いたポリカプロラクトンの製造方法
JP4297152B2 (ja) 2006-10-06 2009-07-15 トヨタ自動車株式会社 車両前部構造
US8809392B2 (en) 2008-03-28 2014-08-19 Ecolab Usa Inc. Sulfoperoxycarboxylic acids, their preparation and methods of use as bleaching and antimicrobial agents
BRPI0907918B1 (pt) 2008-03-28 2018-07-24 Ecolab Inc. Ácidos sulfoperoxicarboxílicos, sua preparação e métodos de utilizção como agentes alvejantes e antimicrobianos
US8871807B2 (en) 2008-03-28 2014-10-28 Ecolab Usa Inc. Detergents capable of cleaning, bleaching, sanitizing and/or disinfecting textiles including sulfoperoxycarboxylic acids
US12203056B2 (en) 2008-03-28 2025-01-21 Ecolab Usa Inc. Sulfoperoxycarboxylic acids, their preparation and methods of use as bleaching and antimicrobial agents
CN102584776A (zh) * 2011-01-12 2012-07-18 中国石油化工集团公司 一种制备ε-己内酯的方法
CN102584775B (zh) * 2011-01-12 2015-04-22 中国石油化工集团公司 制备ε-己内酯的方法
CN102304117A (zh) * 2011-09-19 2012-01-04 武汉理工大学 一种合成ε-己内酯的方法
US9321664B2 (en) 2011-12-20 2016-04-26 Ecolab Usa Inc. Stable percarboxylic acid compositions and uses thereof
CA2867565C (en) 2012-03-30 2021-01-19 Victor KEASLER Use of peracetic acid/hydrogen peroxide and peroxide-reducing agents for treatment of drilling fluids, frac fluids, flowback water and disposal water
US20140256811A1 (en) 2013-03-05 2014-09-11 Ecolab Usa Inc. Efficient stabilizer in controlling self accelerated decomposition temperature of peroxycarboxylic acid compositions with mineral acids
US10165774B2 (en) 2013-03-05 2019-01-01 Ecolab Usa Inc. Defoamer useful in a peracid composition with anionic surfactants
CN104003972A (zh) * 2014-04-28 2014-08-27 安徽红太阳新材料有限公司 一种制备己内酯的方法
CN104130234A (zh) * 2014-07-25 2014-11-05 南京红太阳新材料有限公司 一种制备己内酯的方法
US10172351B2 (en) 2015-09-04 2019-01-08 Ecolab Usa Inc. Performic acid on-site generator and formulator
CN105315442A (zh) * 2015-12-01 2016-02-10 仇颖超 一种淀粉改性聚己内酯塑料材料的制备方法
GB2548137A (en) * 2016-03-09 2017-09-13 Perstorp Ab Production equipment (I) for production of a caprolactone
GB2548138A (en) * 2016-03-09 2017-09-13 Perstorp Ab Production equipment (II) for production of a caprolactone
CN107163018A (zh) * 2017-06-23 2017-09-15 中山大学惠州研究院 一种分离ε‑己内酯的精馏方法
EP3841059A1 (de) 2018-08-22 2021-06-30 Ecolab USA Inc. Wasserstoffperoxid- und persäurestabilisierung mit molekülen auf basis einer pyridincarbonsäure an c-3, -4 oder -5
US12096768B2 (en) 2019-08-07 2024-09-24 Ecolab Usa Inc. Polymeric and solid-supported chelators for stabilization of peracid-containing compositions
CN111763192B (zh) * 2020-07-14 2023-09-12 湖南瑞源石化股份有限公司 一种ε-己内酯的制备方法及其装置
CN115490623B (zh) * 2021-06-18 2024-08-30 中国石油化工股份有限公司 合成无水过氧有机酸的方法和合成ε-己内酯的方法
CN114835669A (zh) * 2022-03-23 2022-08-02 华东理工大学 高纯度ε-己内酯的微流控合成方法
CN115812713B (zh) * 2022-11-29 2024-03-29 湖南聚仁新材料股份公司 消毒剂和己内酯生产过程中联产过氧羧酸消毒剂的方法
CN119588424A (zh) * 2023-09-11 2025-03-11 中国石油化工股份有限公司 一种催化剂组合物以及制备过氧酸的方法

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3064008A (en) * 1962-11-13 I i i i i i
US2914556A (en) * 1956-04-13 1959-11-24 Union Carbide Corp Preparation of lactone adducts
US3189619A (en) * 1962-09-25 1965-06-15 Exxon Research Engineering Co Synthesis of carpolactone
US3317563A (en) * 1963-12-26 1967-05-02 Celanese Corp Preparation of epsilon-caprolactone
FR1474098A (fr) * 1966-01-25 1967-03-24 Electro Chimie Soc D Procédé de préparation d'epsilon-caprolactone
FR1474903A (fr) * 1966-02-12 1967-03-31 Electrochimie Soc Procédé de préparation d'epsiloncaprolactone
GB1140184A (en) * 1967-06-13 1969-01-15 Chisso Corp Process for manufacturing e-caprolactone
US3624258A (en) * 1969-03-22 1971-11-30 Teijin Ltd Process for the preparation of {68 -caprolactone
DE2038455A1 (de) * 1970-08-01 1972-02-10 Bayer Ag Verfahren zur Herstellung von epsilon-Caprolacton
US3781350A (en) * 1971-07-09 1973-12-25 Teijin Ltd Process for preparation of omega-hydroxy saturated aliphatic monocarboxylic acids
US3825570A (en) * 1971-11-02 1974-07-23 Teijin Ltd Process for the preparation of epsilon-caprolactone
US4183863A (en) * 1978-04-18 1980-01-15 Union Carbide Corporation Conversion of cyclohexanol to ε-caprolactone
DE2920436A1 (de) * 1979-05-19 1980-12-04 Bayer Ag Verfahren zur herstellung von epsilon -caprolacton
DE2934659A1 (de) * 1979-08-28 1981-03-19 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von sehr reinem epsilon -caprolacton
FR2500453A1 (fr) * 1981-02-20 1982-08-27 Ugine Kuhlmann Procede d'obtention de l'epsilon-caprolactone
FR2519985A1 (fr) * 1982-01-15 1983-07-22 Ugine Kuhlmann Procede perfectionne de fabrication de l'e-caprolactone
JPH0237919B2 (ja) * 1983-05-04 1990-08-28 Mitsubishi Chem Ind Kapurorakutonnoseizohoho
JPS61200120A (ja) * 1985-03-01 1986-09-04 Nippon Shokubai Kagaku Kogyo Co Ltd ラクトン変性化合物の製造方法
DE3823213A1 (de) * 1988-07-08 1990-01-11 Basf Ag Verfahren zur herstellung von caprolacton

Also Published As

Publication number Publication date
EP0454397B1 (de) 1995-04-05
EP0454397A1 (de) 1991-10-30
CN1035379C (zh) 1997-07-09
JPH0798816B2 (ja) 1995-10-25
CA2040270A1 (en) 1991-10-26
CN1071923A (zh) 1993-05-12
DE69108600T2 (de) 1996-01-11
US5250707A (en) 1993-10-05
ATE120742T1 (de) 1995-04-15
JPH049378A (ja) 1992-01-14

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Legal Events

Date Code Title Description
8364 No opposition during term of opposition
8339 Ceased/non-payment of the annual fee