DE69725717D1 - Reinigung von glycidylestern durch dünnschichtverdampfung - Google Patents
Reinigung von glycidylestern durch dünnschichtverdampfungInfo
- Publication number
- DE69725717D1 DE69725717D1 DE69725717T DE69725717T DE69725717D1 DE 69725717 D1 DE69725717 D1 DE 69725717D1 DE 69725717 T DE69725717 T DE 69725717T DE 69725717 T DE69725717 T DE 69725717T DE 69725717 D1 DE69725717 D1 DE 69725717D1
- Authority
- DE
- Germany
- Prior art keywords
- thin film
- reaction product
- cleaning
- distillation
- glycidyl esters
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
- 239000010409 thin film Substances 0.000 title abstract 2
- 238000004140 cleaning Methods 0.000 title 1
- 230000008020 evaporation Effects 0.000 title 1
- 238000001704 evaporation Methods 0.000 title 1
- SGFJJNBUMXQSMU-PDBXOOCHSA-N oxiran-2-ylmethyl (9z,12z,15z)-octadeca-9,12,15-trienoate Chemical class CC\C=C/C\C=C/C\C=C/CCCCCCCC(=O)OCC1CO1 SGFJJNBUMXQSMU-PDBXOOCHSA-N 0.000 title 1
- 239000007795 chemical reaction product Substances 0.000 abstract 3
- 238000004821 distillation Methods 0.000 abstract 3
- 239000010408 film Substances 0.000 abstract 1
- -1 glycidyl ester Chemical class 0.000 abstract 1
- 238000000034 method Methods 0.000 abstract 1
- 150000002762 monocarboxylic acid derivatives Chemical class 0.000 abstract 1
- 239000000047 product Substances 0.000 abstract 1
- 150000003839 salts Chemical class 0.000 abstract 1
- 229920006395 saturated elastomer Polymers 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D303/00—Compounds containing three-membered rings having one oxygen atom as the only ring hetero atom
- C07D303/02—Compounds containing oxirane rings
- C07D303/12—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms
- C07D303/16—Compounds containing oxirane rings with hydrocarbon radicals, substituted by singly or doubly bound oxygen atoms by esterified hydroxyl radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D301/00—Preparation of oxiranes
- C07D301/32—Separation; Purification
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Epoxy Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Detergent Compositions (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US1807396P | 1996-05-21 | 1996-05-21 | |
| US18073P | 1996-05-21 | ||
| PCT/US1997/008927 WO1997044335A1 (en) | 1996-05-21 | 1997-05-20 | Purification of glycidyl esters by thin film evaporation |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE69725717D1 true DE69725717D1 (de) | 2003-11-27 |
| DE69725717T2 DE69725717T2 (de) | 2004-07-29 |
Family
ID=21786103
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE69725717T Expired - Lifetime DE69725717T2 (de) | 1996-05-21 | 1997-05-20 | Reinigung von glycidylestern durch dünnschichtverdampfung |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US5880297A (de) |
| EP (1) | EP0901481B1 (de) |
| JP (1) | JP2001501587A (de) |
| AT (1) | ATE252568T1 (de) |
| AU (1) | AU723333B2 (de) |
| DE (1) | DE69725717T2 (de) |
| WO (1) | WO1997044335A1 (de) |
Families Citing this family (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US6136991A (en) | 1996-05-21 | 2000-10-24 | Exxon Chemical Patents Inc. | Glycidyl ester adducts having increased glass transition temperatures |
| TW455584B (en) * | 1998-09-23 | 2001-09-21 | Shell Int Research | Process for the preparation of glycidylesters of branched carboxylic acids |
| FI990089A7 (fi) | 1999-01-18 | 2000-07-19 | Dynea Chemicals Oy | Maalikoostumukset |
| JP4907821B2 (ja) * | 1999-12-07 | 2012-04-04 | スリーエム イノベイティブ プロパティズ カンパニー | 加水分解性ハロゲン化物および他の高分子量材料を含有する材料をエピハロヒドリン誘導エポキシ樹脂から除去する方法 |
| US6544596B2 (en) * | 2000-11-29 | 2003-04-08 | Pacific Northwest Coatings | Method of coating a substrate using a thermosetting basecoat composition and a thermoplastic top coat composition |
| ATE222899T1 (de) | 2000-12-28 | 2002-09-15 | Lundbeck & Co As H | Verfahren zur herstellung von reinem citalopram |
| WO2003024914A1 (en) * | 2001-09-14 | 2003-03-27 | Resolution Research Nederland B.V. | Manufacture of allyl esters of tertiary alkane carboxylic acids |
| DE10211295C1 (de) * | 2002-03-14 | 2003-06-18 | Thioplast Chemicals Gmbh & Co | Verfahren zur Herstellung von epoxidierten Polysulfiden |
| DE10223283C1 (de) * | 2002-05-24 | 2003-07-24 | Thioplast Chemicals Gmbh & Co | Verfahren zur Herstellung von epoxidierten Polysulfiden |
| DE10320543B4 (de) * | 2003-05-07 | 2006-02-02 | Thioplast Chemicals Gmbh & Co.Kg | Verfahren zur Herstellung von Präpolymeren auf der Basis von Polysulfiden und Polyepoxiden |
| EP1538146A1 (de) * | 2003-12-05 | 2005-06-08 | Resolution Research Belgium S.A. | Verfahren zur Modifizierung von nicht glycidylfunktionellen Verunreinungen in zur weiteren radikalischen Polymerisation bestimmten Glycidylester |
| WO2005090325A1 (ja) * | 2004-03-18 | 2005-09-29 | Daicel Chemical Industries, Ltd. | 高純度脂環式 エポキシ化合物、その製造方法、硬化性エポキシ樹脂組成物、その硬化物、および用途 |
| EP2103605A1 (de) | 2008-03-18 | 2009-09-23 | Hexion Specialty Chemicals Research Belgium S.A. | Zusammensetzung für niedrige Farbe von ungesättigten Glycidylesterderivaten und Verwendung dafür |
| WO2013075806A2 (en) * | 2011-11-25 | 2013-05-30 | Momentive Specialty Chemicals Research Beigium Sa | Epoxy compositions |
| CN103183652B (zh) * | 2011-12-28 | 2016-04-06 | 河北四友卓越科技有限公司 | 叔碳酸缩水甘油酯的制备方法 |
| CN103539763B (zh) * | 2013-10-08 | 2016-05-04 | 常州大学 | 一种由二氯丙醇连续制备环氧氯丙烷的反应分离耦合工艺 |
| DK3068854T4 (da) | 2013-11-14 | 2023-08-21 | Cargill Inc | Fjernelse af uønskede propanolbestanddele |
| CN104761517B (zh) * | 2015-04-15 | 2017-04-26 | 西南化工研究设计院有限公司 | 一种叔碳酸缩水甘油酯的连续精制方法 |
| KR20170112515A (ko) | 2016-03-31 | 2017-10-12 | 코오롱인더스트리 주식회사 | 글리시딜에스테르 화합물의 제조방법 |
| CN106957284B (zh) * | 2017-04-14 | 2019-02-19 | 西南化工研究设计院有限公司 | 一种叔碳酸缩水甘油酯粗产品的分离提纯精制工艺 |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3075999A (en) * | 1963-01-29 | Glycidyl esteks | ||
| US3178454A (en) * | 1959-05-19 | 1965-04-13 | Shell Oil Co | Epoxy esters of alpha, alpha-dialkyl monocarboxylic acids |
| US3142686A (en) * | 1960-05-16 | 1964-07-28 | Shell Oil Co | Process for preparing epoxy esters of alpha, alpha-dialkyl monocarboxylic acids |
| US4922002A (en) * | 1984-12-21 | 1990-05-01 | King Industries, Inc. | Linear, low-molecular-weight polyester-based polyol |
| US5486542A (en) * | 1994-01-28 | 1996-01-23 | Shell Oil Company | Process for the distillation of Fisher-Tropsch products |
-
1997
- 1997-05-20 JP JP09542831A patent/JP2001501587A/ja active Pending
- 1997-05-20 DE DE69725717T patent/DE69725717T2/de not_active Expired - Lifetime
- 1997-05-20 EP EP97926739A patent/EP0901481B1/de not_active Expired - Lifetime
- 1997-05-20 AT AT97926739T patent/ATE252568T1/de not_active IP Right Cessation
- 1997-05-20 AU AU31435/97A patent/AU723333B2/en not_active Ceased
- 1997-05-20 WO PCT/US1997/008927 patent/WO1997044335A1/en not_active Ceased
- 1997-05-21 US US08/861,408 patent/US5880297A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| EP0901481A1 (de) | 1999-03-17 |
| US5880297A (en) | 1999-03-09 |
| AU3143597A (en) | 1997-12-09 |
| EP0901481B1 (de) | 2003-10-22 |
| JP2001501587A (ja) | 2001-02-06 |
| AU723333B2 (en) | 2000-08-24 |
| WO1997044335A1 (en) | 1997-11-27 |
| DE69725717T2 (de) | 2004-07-29 |
| ATE252568T1 (de) | 2003-11-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8364 | No opposition during term of opposition | ||
| 8327 | Change in the person/name/address of the patent owner |
Owner name: RESOLUTION SPECIALTY MATERIALS LLC (N.D.GES.D. STA |