[go: up one dir, main page]

DE60013970D1 - Verfahren mit verbesserter Kapazität zur Herstellung und Reinigung von Acrylsäure aus Propylen - Google Patents

Verfahren mit verbesserter Kapazität zur Herstellung und Reinigung von Acrylsäure aus Propylen

Info

Publication number
DE60013970D1
DE60013970D1 DE60013970T DE60013970T DE60013970D1 DE 60013970 D1 DE60013970 D1 DE 60013970D1 DE 60013970 T DE60013970 T DE 60013970T DE 60013970 T DE60013970 T DE 60013970T DE 60013970 D1 DE60013970 D1 DE 60013970D1
Authority
DE
Germany
Prior art keywords
propylene
purification
production
acrylic acid
improved capacity
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Revoked
Application number
DE60013970T
Other languages
English (en)
Other versions
DE60013970T2 (de
Inventor
James Edward Elder
Charles Michael Lonzetta
Peter David Klugherz
Donald Alan Ebert
Elaine Lashae Williams
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Rohm and Haas Co
Original Assignee
Rohm and Haas Co
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=22512500&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=DE60013970(D1) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Rohm and Haas Co filed Critical Rohm and Haas Co
Publication of DE60013970D1 publication Critical patent/DE60013970D1/de
Application granted granted Critical
Publication of DE60013970T2 publication Critical patent/DE60013970T2/de
Anticipated expiration legal-status Critical
Revoked legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/16—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation
    • C07C51/21—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen
    • C07C51/25—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring
    • C07C51/252—Preparation of carboxylic acids or their salts, halides or anhydrides by oxidation with molecular oxygen of unsaturated compounds containing no six-membered aromatic ring of propene, butenes, acrolein or methacrolein
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
DE60013970T 1999-07-23 2000-07-20 Verfahren mit verbesserter Kapazität zur Herstellung und Reinigung von Acrylsäure aus Propylen Revoked DE60013970T2 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US14530899P 1999-07-23 1999-07-23
US145308P 1999-07-23

Publications (2)

Publication Number Publication Date
DE60013970D1 true DE60013970D1 (de) 2004-10-28
DE60013970T2 DE60013970T2 (de) 2005-03-31

Family

ID=22512500

Family Applications (1)

Application Number Title Priority Date Filing Date
DE60013970T Revoked DE60013970T2 (de) 1999-07-23 2000-07-20 Verfahren mit verbesserter Kapazität zur Herstellung und Reinigung von Acrylsäure aus Propylen

Country Status (9)

Country Link
US (1) US6639106B1 (de)
EP (1) EP1070700B1 (de)
JP (1) JP2001064227A (de)
KR (1) KR100735873B1 (de)
CN (1) CN1269787C (de)
BR (1) BR0003117A (de)
DE (1) DE60013970T2 (de)
MX (1) MXPA00007106A (de)
TW (1) TWI226326B (de)

Families Citing this family (27)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003040079A1 (en) * 2001-11-06 2003-05-15 Mitsubishi Chemical Corporation Method of collecting acrylic acid
JP3908118B2 (ja) 2002-08-08 2007-04-25 株式会社日本触媒 アクリル酸の製造方法
US20040104108A1 (en) 2002-12-03 2004-06-03 Mason Robert Michael High capacity purification of thermally unstable compounds
DE10351269A1 (de) 2003-10-31 2005-06-02 Basf Ag Verfahren zum Langzeitbetrieb einer heterogen katalysierten Gasphasenpartialoxidation von Propen zu Acrylsäure
US7393976B2 (en) 2003-11-26 2008-07-01 Rohm And Haas Company Process for manufacturing reduced water content (meth)acrylic acid
US20050137422A1 (en) * 2003-12-19 2005-06-23 Saudi Basic Industries Corporation Process for producing an unsaturated carboxylic acid from an alkane
JP5006507B2 (ja) * 2004-01-30 2012-08-22 株式会社日本触媒 アクリル酸の製造方法
US7592483B2 (en) 2004-07-01 2009-09-22 Basf Aktiengesellschaft Preparation of acrolein or acrylic acid or a mixture thereof by heterogeneously catalyzed partial gas phase oxidation of propylene
US7414149B2 (en) * 2004-11-22 2008-08-19 Rohm And Haas Company Non-routine reactor shutdown method
DE102005019911A1 (de) 2005-04-27 2006-11-02 Basf Ag Verfahren der rektifikativen Auftrennung einer Acrylsäure und/oder Methacrylsäure enthaltenden Flüssigkeit
DE102006022014A1 (de) * 2006-05-10 2007-11-15 Degussa Gmbh Verfahren zur Herstellung von Cyclododecatrien
DE102006036177B4 (de) * 2006-07-21 2013-05-08 Evonik Degussa Gmbh Vorrichtung und Verfahren zur Herstellung von Acrylsäure mit verminderter Autoxidationsneigung
JP5407486B2 (ja) * 2008-03-31 2014-02-05 三菱化学株式会社 （メタ）アクリル酸および／または（メタ）アクロレインの製造方法
JP2009263351A (ja) * 2008-03-31 2009-11-12 Mitsubishi Chemicals Corp （メタ）アクリル酸の製造方法
JP5507111B2 (ja) * 2008-05-30 2014-05-28 ローム アンド ハース カンパニー 水性（メタ）アクリル酸の製造方法
US9156769B2 (en) * 2008-10-15 2015-10-13 Arkema Inc. Method of recovering carboxylic acids from dilute aqueous streams
WO2010044990A1 (en) * 2008-10-15 2010-04-22 Arkema Inc. Method of recovering carboxylic acids from dilute aqueous streams
JP2011121048A (ja) 2009-12-09 2011-06-23 Rohm & Haas Co 固体触媒物質をブレンドし、管状構造物に装填する方法
CA2781246A1 (en) * 2011-07-14 2013-01-14 Rohm And Haas Company Method for removal of organic compounds from waste water streams in a process for production of (meth)acrylic acid
US9440903B2 (en) 2012-09-24 2016-09-13 Arkema Inc. Shell and tube oxidation reactor with improved resistance to fouling
EP3122714A4 (de) * 2014-03-24 2017-11-01 Arkema, Inc. Verfahren zur rückgewinnung von carboxylsäuren aus verdünnten wässrigen strömen
CN105061193B (zh) * 2015-08-10 2017-03-22 蓝星（北京）技术中心有限公司 蛋氨酸生产废水处理中回收有机物的方法
WO2019182713A1 (en) * 2018-03-21 2019-09-26 Rohm And Haas Company Method for preparing acrylic acid
CN110551020A (zh) * 2018-05-30 2019-12-10 中国石油集团东北炼化工程有限公司吉林设计院 一种回收废水中丙烯酸的方法
KR102690124B1 (ko) * 2020-12-03 2024-07-30 주식회사 엘지화학 아크릴산의 제조 공정
CN113582830A (zh) * 2021-09-30 2021-11-02 山东蓝湾新材料有限公司 一种高效剥离杂质提纯丙烯酸的方法
EP4234531A1 (de) * 2022-02-25 2023-08-30 Evonik Superabsorber GmbH Abtrennung von acrylsäure mit hilfe von membrankontaktoren

Family Cites Families (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS5129124B1 (de) 1971-04-27 1976-08-24
BE783549A (fr) * 1972-05-16 1972-09-18 Mines Fond Zinc Vieille Procede de purification de solutions de sulfate de zinc provenant de lalixiviation des minerais de zinc.
US3893951A (en) 1973-02-22 1975-07-08 Standard Oil Co Catalysts for oxidation reactions
JPS5246208B2 (de) 1973-03-22 1977-11-22
JPS5223589A (en) 1975-08-18 1977-02-22 Mitsubishi Petrochem Co Ltd Catalyst for producing alpha,beta-unsaturaded carboxylic acid
US4203906A (en) 1977-07-13 1980-05-20 Nippon Shokubai Kagaku Kogyo Co., Ltd. Process for catalytic vapor phase oxidation
JPS6054939B2 (ja) * 1977-08-04 1985-12-03 住友化学工業株式会社 粗製アクリル酸の精製方法
JPS55102536A (en) 1979-01-30 1980-08-05 Mitsubishi Petrochem Co Ltd Preparation of acrylic acid
JPS5673041A (en) * 1979-11-19 1981-06-17 Mitsubishi Petrochem Co Ltd Preparation of acrylic acid
US5198578A (en) 1986-07-17 1993-03-30 Union Carbide Chemicals Anhydrous diluents for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid
CA1299193C (en) * 1986-07-17 1992-04-21 Gordon Gene Harkreader Anhydrous diluents for the propylene oxidation reaction to acrolein and acrolein oxidation to acrylic acid
JPH0813777B2 (ja) * 1986-12-11 1996-02-14 三菱化学株式会社 アクリル酸の製造法
JPH0686399B2 (ja) * 1987-05-27 1994-11-02 株式会社日本触媒 アクリル酸の製造方法
AU606160B2 (en) * 1987-05-27 1991-01-31 Nippon Shokubai Kagaku Kogyo Co. Ltd. Process for production of acrylic acid
RU2024296C1 (ru) 1989-11-06 1994-12-15 Ниппон Сокубаи Кагаку Когио Ко., Лтд. Способ получения акриловой кислоты и катализатор для его осуществления
DE4023239A1 (de) 1990-07-21 1992-01-23 Basf Ag Verfahren zur katalytischen gasphasenoxidation von propen oder iso-buten zu acrolein oder methacrolein
EP0487900A1 (de) * 1990-11-27 1992-06-03 Kabushiki Kaisha Toshiba Tragbarer Rechner für Rückstellung eines Wiederaufnahmefehlers, verursacht durch Veränderung einer HDD-geladenen Bedingung und BS-Start
DE4132263A1 (de) * 1991-09-27 1993-04-01 Basf Ag Verfahren zur katalytischen gasphasenoxidation von acrolein zu acrylsaeure
DE4302991A1 (de) 1993-02-03 1994-08-04 Basf Ag Multimetalloxidmassen
JP3937462B2 (ja) * 1994-08-04 2007-06-27 三菱化学株式会社 アクリル酸精製法
DE4431949A1 (de) 1994-09-08 1995-03-16 Basf Ag Verfahren zur katalytischen Gasphasenoxidation von Acrolein zu Acrylsäure
JP3299424B2 (ja) * 1994-11-14 2002-07-08 株式会社日本触媒 アクリル酸製造用触媒およびその製造法
DE69518547T2 (de) 1994-11-14 2001-01-11 Nippon Shokubai Co. Ltd., Osaka Verfahren zur Herstellung von Acrylsäure
WO1997036849A1 (en) 1996-04-01 1997-10-09 Union Carbide Chemicals & Plastics Technology Corporation Processes for the oxidation of alkanes
KR20010104053A (ko) * 2000-05-12 2001-11-24 성재갑 프로필렌의 기상 산화 반응에 의한 아크롤레인의 제조 방법

Also Published As

Publication number Publication date
MXPA00007106A (es) 2002-06-04
BR0003117A (pt) 2001-03-13
CN1269787C (zh) 2006-08-16
JP2001064227A (ja) 2001-03-13
EP1070700A3 (de) 2003-01-02
TWI226326B (en) 2005-01-11
US6639106B1 (en) 2003-10-28
EP1070700B1 (de) 2004-09-22
CN1282727A (zh) 2001-02-07
DE60013970T2 (de) 2005-03-31
EP1070700A2 (de) 2001-01-24
KR20010049838A (ko) 2001-06-15
KR100735873B1 (ko) 2007-07-06

Similar Documents

Publication Publication Date Title
DE60013970D1 (de) Verfahren mit verbesserter Kapazität zur Herstellung und Reinigung von Acrylsäure aus Propylen
DE60002793D1 (de) Verfahren zur Herstellung von Acrolein und Acrylsäure
DE69902139D1 (de) Verfahren zur Herstellung von Salpetersäure
DE60110497D1 (de) Verfahren zur Herstellung von Acrylsäure
DE60107987D1 (de) Verfahren zur Herstellung von Acrolein und Acrylsäure
AT7109U3 (de) Verfahren zur herstellung von amlodipinmaleat
DE60133445D1 (de) Verfahren zur Herstellung von Harnstoff
DE60005870D1 (de) Verfahren zur Herstellung von Acrylsäure
DE60017237D1 (de) Verfahren zur mikrobiellen Herstellung von Polyestern
DE60024210D1 (de) Verfahren zur Herstellung von Zahnrädern
DE60038560D1 (de) Verfahren zur fermentativen Herstellung von L-Arginin
DE69903698D1 (de) Verfahren zur Herstellung von Acrylsäure
DE69909181D1 (de) Verfahren zur Herstellung von Acrolein und Acrylsäure
DE50015943D1 (de) Verfahren zur Herstellung von Düngemittelpressgranulaten
DE60131954D1 (de) Verfahren zur herstellung von 2-hydroxy-4-methylthiobutansäure
DE60121649D1 (de) Kontinuierliches Verfahren zur Herstellung von Polyolefinschaumteilchen
DE60020048D1 (de) Verfahren zur Herstellung von Methacrylsäure
DE60131562D1 (de) Verfahren zur herstellung von benztriazolen
EP1320367A4 (de) Verfahren zur herstellung von dinapsolin
DE69906607D1 (de) Verfahren zur Herstellung von optisch aktiven Chrysanthemumsäure
DE60034843D1 (de) Verfahren zur Herstellung von L-arginin
DE60019606D1 (de) Verfahren zur herstellung von substituierten pyrimidinen
DE69916332D1 (de) Verfahren zur herstellung von etheraminalkoxylaten
DE60105734D1 (de) Verfahren zur Herstellung von 4-Cyano-4-Oxobuttersäureester und 4-Cyano-3-Hydroxybuttersäureester
DE60012337D1 (de) Verfahren zur herstellung von fluorcarbonsäureanyhydriden

Legal Events

Date Code Title Description
8363 Opposition against the patent
8331 Complete revocation