DE456019C - Process for the production of water-soluble pest repellants in solid form - Google Patents
Process for the production of water-soluble pest repellants in solid formInfo
- Publication number
- DE456019C DE456019C DEA39052D DEA0039052D DE456019C DE 456019 C DE456019 C DE 456019C DE A39052 D DEA39052 D DE A39052D DE A0039052 D DEA0039052 D DE A0039052D DE 456019 C DE456019 C DE 456019C
- Authority
- DE
- Germany
- Prior art keywords
- water
- solid form
- production
- soluble
- parts
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 6
- 239000007787 solid Substances 0.000 title claims description 6
- 238000004519 manufacturing process Methods 0.000 title claims description 3
- 241000607479 Yersinia pestis Species 0.000 title description 3
- 239000002253 acid Substances 0.000 claims description 8
- 150000007513 acids Chemical class 0.000 claims description 5
- 230000003647 oxidation Effects 0.000 claims description 4
- 238000007254 oxidation reaction Methods 0.000 claims description 4
- 239000002803 fossil fuel Substances 0.000 claims description 2
- 229910052752 metalloid Inorganic materials 0.000 claims description 2
- 150000002738 metalloids Chemical class 0.000 claims description 2
- 239000000575 pesticide Substances 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 239000003513 alkali Substances 0.000 description 3
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000011593 sulfur Substances 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- LAISNASYKAIAIK-UHFFFAOYSA-N [S].[As] Chemical compound [S].[As] LAISNASYKAIAIK-UHFFFAOYSA-N 0.000 description 1
- 150000004645 aluminates Chemical class 0.000 description 1
- DIZPMCHEQGEION-UHFFFAOYSA-H aluminium sulfate (anhydrous) Chemical compound [Al+3].[Al+3].[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O.[O-]S([O-])(=O)=O DIZPMCHEQGEION-UHFFFAOYSA-H 0.000 description 1
- HIVLDXAAFGCOFU-UHFFFAOYSA-N ammonium hydrosulfide Chemical compound [NH4+].[SH-] HIVLDXAAFGCOFU-UHFFFAOYSA-N 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 239000000417 fungicide Substances 0.000 description 1
- 239000003077 lignite Substances 0.000 description 1
- 150000002737 metalloid compounds Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 239000003415 peat Substances 0.000 description 1
- 229920001021 polysulfide Polymers 0.000 description 1
- 239000005077 polysulfide Substances 0.000 description 1
- 150000008117 polysulfides Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 235000011121 sodium hydroxide Nutrition 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
Landscapes
- Life Sciences & Earth Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Health & Medical Sciences (AREA)
- Environmental Sciences (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Agronomy & Crop Science (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Description
Verfahren zur Herstellung von wasserlöslichen Schädlingsbekämpfungsmitteln in fester Form. In dem Patent 43 0 7 12, Anspruch 3, ist ein Verfahren zur Herstellung für die Schädlingsbekämpfung geeigneter Staffe beschrieben, das dadurch gekennzeichnet ist, daß man Lösungen von Metalloidverbindungen in durch Säure zersetzbarer Form mit den Alkaliverbindungen solcher hochmolekularen Säuren versetzt, welche aus fossilen Brennstoffen, gegebenenfalls nach deren Oxydation, nach bekannten Methoden gewonnen werden.Process for the preparation of water-soluble pesticides in solid form. Patent 43 0 7 12, claim 3, describes a process for the production of pest control suitable stuffing, which is characterized in that solutions of metalloid compounds in acid-decomposable form are mixed with the alkali compounds of such high molecular weight acids, which are derived from fossil fuels , optionally after their oxidation, are obtained by known methods.
Bei der weiteren Bearbeitung hat sich nun gezeigt, daß man an Stelle der dort genannten unlöslichen Produkte wasserlösliche Produkte in fester Form gewinnen kann, welche die Metalloide enthalten, wenn man statt der Alkaliverbindungen der genannten hochmolekularen Säuren diese Säuren selbst ohne Zusatz einer stärkeren Säure verwendet.In further processing it has now been shown that one in place of the insoluble products mentioned there obtain water-soluble products in solid form can, which contain the metalloids if, instead of the alkali compounds, the called high molecular acids these acids themselves without the addition of a stronger one Acid used.
So kann man z. B. aus Alkalipolysulfiden mittels dieser Säure Schwefel, aus Sulfoarseniaten Schwefelarsen, aus Aluminaten Alunüniurnoxydhydrat in wasserlöslicher Form gewinnen. Die so gewonnenen Produkte sind in fester Form luftbeständig und im kalten Wasser leicht löslich. Sie eignen sich in vorzüglicher Weise zur Bekämpfung von Schädlingen aller Art. B eis pi el i. Eine Lösung von 34 Teilen Schwefelammonium in 2ooTeilen Wasser wird mit Schwefel gesättigt, hierauf mit 5 5 Teilen einer durch Oxydation von Braunkohle erhältlichen hochmolekularen Säure versetzt und zur Trockne gedampft. Der feste braune Rückstand löst sich leicht in Wasser und ist ein sehr wirksames Fungizid. Beispiel 2. 55Teile Aluminiumsulfat werden in 1500 Teilen Wasser gelöst und 4oTeile Atznatron in 5oo Teilen Wasser zugefügt. In der erhaltenen Natriumaltiminatlösung werden unter gutem Rühren 6oTeile der durch Extraktion (nach vorheriger Oxydation) von Torf erhaltenen hochmolekularen Säuren gelöst und die Masse zur Trockne verdampft. DerRückstand löst sich leicht in Wasser. So you can z. B. from alkali polysulfides by means of this acid sulfur, from sulfoarseniates arsenic sulfur, from aluminates Alunüniurnoxydhydrat in water-soluble form. The products obtained in this way are air-resistant in solid form and easily soluble in cold water. They are particularly suitable for combating pests of all kinds. B eis pi el i. A solution of 34 parts of sulfur ammonium in 2oo parts of water is saturated with sulfur, 5 5 parts of a high molecular acid obtainable by oxidation of lignite are then added and the mixture is evaporated to dryness. The solid brown residue dissolves easily in water and is a very effective fungicide. Example 2. 55 parts of aluminum sulfate are dissolved in 1500 parts of water and 40 parts of caustic soda in 500 parts of water are added. 60 parts of the high molecular weight acids obtained by extraction (after previous oxidation) of peat are dissolved in the sodium aliminate solution obtained, and the mass is evaporated to dryness. The residue easily dissolves in water.
Claims (1)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEA39052D DE456019C (en) | 1922-12-22 | 1922-12-22 | Process for the production of water-soluble pest repellants in solid form |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEA39052D DE456019C (en) | 1922-12-22 | 1922-12-22 | Process for the production of water-soluble pest repellants in solid form |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE456019C true DE456019C (en) | 1928-02-14 |
Family
ID=6931155
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEA39052D Expired DE456019C (en) | 1922-12-22 | 1922-12-22 | Process for the production of water-soluble pest repellants in solid form |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE456019C (en) |
-
1922
- 1922-12-22 DE DEA39052D patent/DE456019C/en not_active Expired
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