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DE202004005755U1 - Reactor producing e.g. chlorine dioxide or peracetic acid solutions for disinfection in the food industry, is located in fluid line and has outlet remote from its supply lines - Google Patents

Reactor producing e.g. chlorine dioxide or peracetic acid solutions for disinfection in the food industry, is located in fluid line and has outlet remote from its supply lines Download PDF

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Publication number
DE202004005755U1
DE202004005755U1 DE202004005755U DE202004005755U DE202004005755U1 DE 202004005755 U1 DE202004005755 U1 DE 202004005755U1 DE 202004005755 U DE202004005755 U DE 202004005755U DE 202004005755 U DE202004005755 U DE 202004005755U DE 202004005755 U1 DE202004005755 U1 DE 202004005755U1
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Prior art keywords
reactor
chlorine dioxide
supply lines
fluid line
disinfection
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Expired - Lifetime
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DE202004005755U
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German (de)
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Priority to DE202004005755U priority Critical patent/DE202004005755U1/en
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Classifications

    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61L—METHODS OR APPARATUS FOR STERILISING MATERIALS OR OBJECTS IN GENERAL; DISINFECTION, STERILISATION OR DEODORISATION OF AIR; CHEMICAL ASPECTS OF BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES; MATERIALS FOR BANDAGES, DRESSINGS, ABSORBENT PADS OR SURGICAL ARTICLES
    • A61L2/00—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor
    • A61L2/16—Methods or apparatus for disinfecting or sterilising materials or objects other than foodstuffs or contact lenses; Accessories therefor using chemical substances
    • A61L2/18—Liquid substances or solutions comprising solids or dissolved gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/20—Mixing gases with liquids
    • B01F23/23—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids
    • B01F23/237—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids characterised by the physical or chemical properties of gases or vapours introduced in the liquid media
    • B01F23/2376—Mixing gases with liquids by introducing gases into liquid media, e.g. for producing aerated liquids characterised by the physical or chemical properties of gases or vapours introduced in the liquid media characterised by the gas being introduced
    • B01F23/23763—Chlorine or chlorine containing gases
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F23/00—Mixing according to the phases to be mixed, e.g. dispersing or emulsifying
    • B01F23/40—Mixing liquids with liquids; Emulsifying
    • B01F23/45—Mixing liquids with liquids; Emulsifying using flow mixing
    • B01F23/451—Mixing liquids with liquids; Emulsifying using flow mixing by injecting one liquid into another
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30—Injector mixers
    • B01F25/31—Injector mixers in conduits or tubes through which the main component flows
    • B01F25/313—Injector mixers in conduits or tubes through which the main component flows wherein additional components are introduced in the centre of the conduit
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F25/00—Flow mixers; Mixers for falling materials, e.g. solid particles
    • B01F25/30—Injector mixers
    • B01F25/32—Injector mixers wherein the additional components are added in a by-pass of the main flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/2204—Mixing chemical components in generals in order to improve chemical treatment or reactions, independently from the specific application
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01F—MIXING, e.g. DISSOLVING, EMULSIFYING OR DISPERSING
    • B01F2101/00—Mixing characterised by the nature of the mixed materials or by the application field
    • B01F2101/305—Treatment of water, waste water or sewage

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • General Chemical & Material Sciences (AREA)
  • Epidemiology (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Public Health (AREA)
  • Veterinary Medicine (AREA)
  • Treatment Of Water By Oxidation Or Reduction (AREA)

Abstract

The mixing vessel (1) has two supply lines (6a, 6b) for substances to be mixed. It is located inside a fluid line (5) and has a mixture outlet opening (1a) remote from the supply lines. The reactor (1) is combined with an arrangement in which the mixture is used, all occupying a common space. In a development based on the arrangement described, the main fluid line (5) includes a bypass (8) in which the mixing vessel (1) is located. In the branches to the bypass, 3/2-way valves (7a, 7b) are included.

Description

Die vorliegende Erfindung betrifft einen beweglichen Reaktor, insbesondere zur Herstellung aggressiver Mischungen, wie z.B. chlordioxidhaltige Lösungen oder peressigsäurehaltige Lösungen.The present invention relates to a movable reactor, especially for the production of aggressive Mixtures such as solutions containing chlorine dioxide or peracetic acid Solutions.

In vielen Anwendungsweisen der Lebensmittelindustrie werden Desinfektionsmittel, wie Peressigsäure oder Chlordioxid, zu Desinfektionszwecken vor Ort im Betrieb erzeugt, um dann ihrer Anwendung zugeführt zu werden.In many applications in the food industry disinfectants such as peracetic acid or chlorine dioxide are used for disinfection purposes Generated location in the company, in order to then be used for their application.

Speziell in Getränkebetrieben gibt es wegen der einschlägigen gesetzlichen Vorschriften im allgemeinen ein Chemikalienlager, von dem aus die Maschinen des Lebensmittelbetriebes mit den verschiedensten Chemikalien versorgt werden.Especially in beverage companies there are because of relevant legal regulations generally a chemical warehouse, from from which the machines of the food business with the most varied Chemicals are supplied.

Zum Beispiel werden Flaschenwaschmaschinen aus dem Chemikalienraum (Chemikalienlager) mit Natronlauge zur Flaschenwäsche versorgt; zusätzlich werden Härtestabilisierungsmittel, Desinfektionsmittel und Schaumbremsen aus dem Chemikalienraum dosiert zugegeben. Mittels einer Dosiervorrichtung (Dosierpumpe) wird aus dem Vorratsbehälter das Reinigungs- oder Desinfektionsmittel angesaugt und über eine Schlauchleitung durch das ganze Gebäude zur jeweiligen Anwendung transportiert, beispielsweise zur Flaschenwaschmaschine.For example, bottle washers supplied with sodium hydroxide solution for bottle washing from the chemical room (chemical store); in addition Hardness stabilizer, Disinfectant and foam brakes dosed from the chemical room added. A metering device (metering pump) turns off the reservoir the cleaning agent or disinfectant sucked in and over a Hose line through the entire building for the respective application transported, for example to the bottle washing machine.

Bei aggressiven oder giftigen Stoffen, wie z.B. Chlordioxid oder Peressigsäure, muss nachteiligerweise die Flüssigkeit über viele Meter und sehr teure hochwertige Leitungen durch den Betrieb transportiert werden; dies stellt eine gewisse Unfallgefahr dar, die durch den Vorschlag vorliegender Erfindung deutlich verringert wird.With aggressive or toxic substances, such as. Chlorine dioxide or peracetic acid, disadvantageously the liquid over many Meters and very expensive high quality lines transported through the operation become; this represents a certain risk of accident caused by the Proposal of the present invention is significantly reduced.

Wässrige Lösungen von Chlordioxid werden z.B. durch die Vermischung von zwei Komponenten in einem Reaktor hergestellt.aqueous solutions of chlorine dioxide are e.g. by mixing two components in manufactured in a reactor.

Vorliegende Erfindung schafft nun die Möglichkeit, die Herstellung der Mischungen aus zwei oder mehr hochreaktiven Flüssigkeiten an den Ort ihrer Anwendung zu verlagern, wobei die oben geschilderten Nachteile vermieden werden.The present invention now creates the possibility, the preparation of the mixtures from two or more highly reactive liquids to the place of their application, the ones described above Disadvantages are avoided.

Die Ausgangsstoffe werden nämlich beispielsweise mittels Pumpen und Dosierleitungen bis direkt zum Anwendungsort einzeln und gesondert gefördert und erst kurz vor oder am Ort der Anwendung, beispielsweise in Flaschenwaschmaschinen, einem Vermischungsprozess mit anderen Flüssigkeiten, beispielsweise Wasser, vermischt. Diese Vermischung findet in dem erfindungsgemäßen Reaktor statt.The starting materials are namely, for example using pumps and dosing lines directly to the application site funded individually and separately and only shortly before or at the point of use, for example in bottle washing machines Mixing process with other liquids, for example Water, mixed. This mixing takes place in the reactor according to the invention.

Die Erfindung schlägt also einen Reaktor zum Vermischen von mindestens zwei insbesondere reaktiven Flüssigkeiten, insbesondere Lösungen vor, der dadurch gekennzeichnet ist, dass er aus mindestens einem Mischgefäß mit mindestens zwei Zuleitungen für die zu vermischenden Stoffe besteht, wobei dieses Mischgefäß innerhalb einer Flüssigkeitsleitung angeordnet ist und mindestens eine Austrittsöffnung für die Mischung in dem den Zuleitungen abgewandten Bereich umfasst.The invention therefore strikes a reactor for mixing at least two in particular reactive Liquids, especially solutions which is characterized in that it consists of at least one Mixing vessel with at least two leads for consists of the substances to be mixed, this mixing vessel inside a liquid line is arranged and at least one outlet opening for the mixture in which the feed lines area facing away.

Eine Ausführungsform ist ferner dadurch gekennzeichnet, dass der Reaktor mit einer Anordnung, in der die Mischung angewendet wird, räumlich kombiniert wird.An embodiment is further characterized characterized in that the reactor with an arrangement in which the Mixture is applied spatially is combined.

Das Material für die Dosierleitung kann aus einfachem PVC bestehen, während bei chlordioxidhaltigen Lösungen die Leitungen aus FEP genommen werden müssen, einem sehr hochwertigen und teuren Rohstoff.The material for the dosing line can be made from simple PVC exist while with solutions containing chlorine dioxide the lines have to be taken out of FEP, a very high quality and expensive raw material.

Weiterhin sind chlordioxidhaltige Lösungen nicht beständig und damit ist die erzeugte Flüssigkeit, die in den Leitungen steht, verloren. Bei der vorliegenden Erfindung sind die Verlustmengen sehr gering.They also contain chlorine dioxide Solutions don't resistant and so the liquid produced is that in the lines is lost. In the present invention the losses are very small.

Durch den Einbau des Reaktors unterhalb des Wasserspiegels einer Flüssigkeit ist die Gefahr des Austretens von gasförmigem Chlordioxid erheblich gemindert, da sich eventuell gebildetes Chlordioxid in dem Wasser lösen würde.By installing the reactor below the Water level of a liquid the risk of gaseous chlorine dioxide escaping is considerable diminished because there is possibly formed chlorine dioxide in the water would solve.

Bei einer speziellen Ausführung für die Wasserdesinfektion wird der Reaktor in die Wasserleitung eingebaut, so dass im Leckagefall Chlordioxid im Wasser gebunden wird.In a special version for water disinfection the reactor is installed in the water pipe, so that in the event of a leak Chlorine dioxide is bound in the water.

Das Wesen vorliegender Erfindung wird im folgenden an Hand von drei Ausführungsbeispielen weiterhin erläutert.The essence of the present invention will continue in the following using three exemplary embodiments explained.

1 zeigt eine Ausführungsform des erfindungsgemäßen Reaktors in Kombination mit zwei Vorratsgefäßen für die zu vermischenden Chemikalien, wobei der eigentliche Mischreaktor in einer Flüssigkeitsleitung angeordnet ist. Der eigentliche Mischreaktor trägt die Bezugsziffer 1, die beiden Dosierleitungen sind mit 6a und 6b, die entsprechenden Dosierpumpen mit 3a und 3b und die Vorratsgefäße mit 2a und 2b bezeichnet. Mit der Bezugsziffer 5 ist eine Flüssigkeitsleitung bezeichnet, wobei die Strömungsrichtung mit 5a gekennzeichnet ist. Der eigentliche Vermischungsreaktor 1 hat ein Austrittsende 1a, das in dem Endbereich angeordnet ist, das den Zuleitungen 6a und 6b abgewandt ist. 1 shows an embodiment of the reactor according to the invention in combination with two storage vessels for the chemicals to be mixed, the actual mixing reactor being arranged in a liquid line. The actual mixing reactor bears the reference number 1 , the two dosing lines are with 6a and 6b , the corresponding metering pumps with 3a and 3b and the storage vessels with 2a and 2 B designated. With the reference number 5 is a liquid line, the flow direction with 5a is marked. The actual mixing reactor 1 has an exit end 1a , which is arranged in the end region which the feed lines 6a and 6b is turned away.

Die gesamte Anordnung der 1 wird als Reaktor bezeichnet; die eigentliche Vermischung der Komponenten findet im Mischreaktor 1 statt.The entire arrangement of the 1 is referred to as a reactor; the actual mixing of the components takes place in the mixing reactor 1 instead of.

In 2 wird eine weitere Ausführungsform vorliegender Erfindung beschrieben. Mit den Bezugsziffern 2a und 2b sind die jeweiligen Vorratsbehälter der Chemikalien, insbesondere der Chemikalienlösungen bezeichnet, die jeweils über die Dosierpumpen 3a und 3b von den Dosierleitungen in den eigentlichen Mischreaktor 1 eingeleitet werden, der seinerseits in einer kastenähnlichen Umhüllung 5 angeordnet ist, die ihrerseits räumlich mit der Flaschenwaschmaschine 4 kombiniert ist. Der kastenähnliche Behälter 5 ist in der Regel ein Kaltwasserbehälter.In 2 Another embodiment of the present invention is described. With the reference numbers 2a and 2 B are the respective storage containers of the chemicals, in particular the chemical solutions, each of which is designated via the metering pumps 3a and 3b from the metering lines into the actual mixing reactor 1 be introduced, which in turn in a box-like envelope 5 is arranged, which in turn spatially with the bottle washing machine 4 is combined. The box-like container 5 is usually a cold water tank.

Die Gesamtheit der Elemente dieses Reaktors kann bevorzugtermaßen aus starrem Material bestehen, wobei ein Transport, d.h. eine Ortsveränderung ohne Zerlegung in Einzelteile möglich ist.The entirety of the elements of this Reactor can preferably consist of rigid material, whereby a transport, i.e. a change of location possible without disassembly into individual parts is.

In 3 wird eine weitere Ausführungsform vorliegender Erfindung beschrieben, bei der parallel zur Wasserleitung ein Bypass eingesetzt wird, der den Reaktor enthält. Der Bypass kann mittels zweier 3/2-Wege-Ventile zu- oder abgeschaltet werden.In 3 becomes another embodiment The present invention described, in which a bypass is used in parallel to the water pipe, which contains the reactor. The bypass can be switched on or off using two 3/2-way valves.

Steuerungstechnisch kann die Anlage so geschaltet werden, dass die Chlordioxid produzierende Anlage nur dosiert, wenn die 3/2-Wege-Ventile den Bypass aktiviert haben.In terms of control technology, the system can be switched so that the chlorine dioxide producing plant only dosed when the 3/2-way valves have activated the bypass.

In die Trinkwasserleitung können nach dem Bypass Mess- und Regeleinheiten eingebaut sein, die die Chlordioxid-Anlage bei Fehlfunktion oder Produktmangel deaktivieren, indem sie den Bypass deaktivieren.After in the drinking water pipe the bypass measuring and control units built into the chlorine dioxide system in the event of malfunction or product deficiency, deactivate it by pressing the Deactivate bypass.

Der Bypass kann als komplette Einheit in die Wasserversorgung eingeschraubt oder eingeklebt werden.The bypass can be a complete unit screwed or glued into the water supply.

Mit der Bezugsziffer 1 ist der Reaktor (Mischreaktor), mit 1a dessen Austrittsöffnung, mit 6a und 6b die Zuleitungen, mit 7a und 7b die beiden 3/2-Wege-Ventile, mit 5 die Trinkwasserleitung und mit der Bezugsziffer 8 der Bypass bezeichnet.With the reference number 1 is the reactor (mixed reactor) with 1a its outlet opening, with 6a and 6b the leads, with 7a and 7b the two 3/2-way valves, with 5 the drinking water pipe and with the reference number 8th called the bypass.

11
den Mischreaktorthe mixing reactor
1a1a
die Austrittsöffnung desthe outlet opening of
Mischreaktorsmixing reactor
2a, 2b2a, 2 B
den Vorratsbehälterthe reservoir
3a, 3b3a, 3b
die Dosierpumpenthe dosing
44
die Flaschenwaschmaschinethe bottle Washer
55
die Flüssigkeitsleitungthe liquid line
(Kaltwasserbehälter)(Cold water tank)
5a5a
die Strömungsrichtung in derthe flow direction in the
Flüssigkeitsleitungliquid line
6a, 6b6a, 6b
die Zuleitungenthe leads
7a, 7b7a, 7b
die 3/2-Wege-Ventilethe 3/2-way valves
88th
den Bypassthe bypass

Claims (4)

Reaktor zum Vermischen von mindestens zwei, insbesondere reaktiven Flüssigkeiten, insbesondere Lösungen, dadurch gekennzeichnet, dass er aus mindestens einem Mischgefäß (1) mit mindestens zwei Zuleitungen (6a, 6b) für die zu vermischenden Stoffe besteht, wobei dieses Mischgefäß (1) innerhalb einer Flüssigkeitsleitung (5) angeordnet ist und mindestens eine Austrittsöffnung (1a) für die Mischung in dem den Zuleitungen (6a, 6b) abgewandten Bereich aufweist.Reactor for mixing at least two, in particular reactive liquids, in particular solutions, characterized in that it consists of at least one mixing vessel ( 1 ) with at least two supply lines ( 6a . 6b ) exists for the substances to be mixed, this mixing vessel ( 1 ) within a liquid line ( 5 ) is arranged and at least one outlet opening ( 1a ) for the mixture in which the feed lines ( 6a . 6b ) facing away from the area. Reaktor nach Anspruch 1, dadurch gekennzeichnet, dass der Reaktor (1) mit einer Anordnung, in der die Mischung angewendet wird, räumlich kombiniert ist.Reactor according to claim 1, characterized in that the reactor ( 1 ) is spatially combined with an arrangement in which the mixture is used. Reaktor nach Anspruch 1, dadurch gekennzeichnet, dass in die Flüssigkeitsleitung (5) ein Bypass (8) eingebaut ist, in dem sich das Mischgefäß (1) befindet.Reactor according to claim 1, characterized in that in the liquid line ( 5 ) a bypass ( 8th ) is installed in which the mixing vessel ( 1 ) is located. Reaktor nach Anspruch 3, dadurch gekennzeichnet, dass an den Verzweigungspunkten 3/2-Wege-Ventile (7a, 7b) angeordnet sind.Reactor according to claim 3, characterized in that 3/2-way valves ( 7a . 7b ) are arranged.
DE202004005755U 2004-04-13 2004-04-13 Reactor producing e.g. chlorine dioxide or peracetic acid solutions for disinfection in the food industry, is located in fluid line and has outlet remote from its supply lines Expired - Lifetime DE202004005755U1 (en)

Priority Applications (1)

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DE202004005755U DE202004005755U1 (en) 2004-04-13 2004-04-13 Reactor producing e.g. chlorine dioxide or peracetic acid solutions for disinfection in the food industry, is located in fluid line and has outlet remote from its supply lines

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE202004005755U DE202004005755U1 (en) 2004-04-13 2004-04-13 Reactor producing e.g. chlorine dioxide or peracetic acid solutions for disinfection in the food industry, is located in fluid line and has outlet remote from its supply lines

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2011128137A2 (en) 2010-04-16 2011-10-20 Infracor Gmbh Immersion reactor
DE102010027908A1 (en) 2010-04-19 2011-10-20 Infracor Gmbh tubular reactor
DE202010017478U1 (en) 2010-04-19 2012-03-14 Infracor Gmbh tubular reactor
DE202012006932U1 (en) 2012-07-18 2012-08-31 Infracor Gmbh Radial tubular reactor
EP2581340A1 (en) 2011-10-14 2013-04-17 Infracor Gmbh Improved method for treating water with chlorine dioxide
US8486276B2 (en) 2008-12-19 2013-07-16 Infracor Gmbh Method of treating water and aqueous systems in pipes with chlorine dioxide
US8663481B2 (en) 2007-12-19 2014-03-04 Infracor Gmbh Method of treating water with chlorine dioxide
DE102013015552A1 (en) * 2013-09-10 2015-03-12 AMS Albrecht & Graul GmbH lance
US9156717B2 (en) 2012-07-20 2015-10-13 Infracor Gmbh Radial pipe reactor
US10508031B2 (en) 2016-12-30 2019-12-17 International Dioxcide, Inc. Chlorine dioxide generation

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8663481B2 (en) 2007-12-19 2014-03-04 Infracor Gmbh Method of treating water with chlorine dioxide
US8486276B2 (en) 2008-12-19 2013-07-16 Infracor Gmbh Method of treating water and aqueous systems in pipes with chlorine dioxide
DE102010027840A1 (en) 2010-04-16 2011-10-20 Infracor Gmbh diving reactor
WO2011128137A2 (en) 2010-04-16 2011-10-20 Infracor Gmbh Immersion reactor
DE202010017479U1 (en) 2010-04-16 2012-02-16 Infracor Gmbh diving reactor
WO2011131389A1 (en) 2010-04-19 2011-10-27 Infracor Gmbh Tube reactor
DE202010017478U1 (en) 2010-04-19 2012-03-14 Infracor Gmbh tubular reactor
DE102010027908A1 (en) 2010-04-19 2011-10-20 Infracor Gmbh tubular reactor
EP2581340A1 (en) 2011-10-14 2013-04-17 Infracor Gmbh Improved method for treating water with chlorine dioxide
WO2013053789A1 (en) 2011-10-14 2013-04-18 Infracor Gmbh Improved method for the treatment of water with chlorine dioxide
DE202012006932U1 (en) 2012-07-18 2012-08-31 Infracor Gmbh Radial tubular reactor
US9156717B2 (en) 2012-07-20 2015-10-13 Infracor Gmbh Radial pipe reactor
DE102013015552A1 (en) * 2013-09-10 2015-03-12 AMS Albrecht & Graul GmbH lance
US10508031B2 (en) 2016-12-30 2019-12-17 International Dioxcide, Inc. Chlorine dioxide generation

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