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DE19581926T1 - Verfahren und Vorrichtung zur Reinigung durch Vakuumdestillation zum Herstellen von Magnesium ultra-hoher Reinheit - Google Patents

Verfahren und Vorrichtung zur Reinigung durch Vakuumdestillation zum Herstellen von Magnesium ultra-hoher Reinheit

Info

Publication number
DE19581926T1
DE19581926T1 DE19581926T DE19581926T DE19581926T1 DE 19581926 T1 DE19581926 T1 DE 19581926T1 DE 19581926 T DE19581926 T DE 19581926T DE 19581926 T DE19581926 T DE 19581926T DE 19581926 T1 DE19581926 T1 DE 19581926T1
Authority
DE
Germany
Prior art keywords
cleaning
high purity
vacuum distillation
purity magnesium
produce ultra
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE19581926T
Other languages
English (en)
Inventor
Raymond K F Lam
Daniel R Marx
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Materials Research Corp
Original Assignee
Materials Research Corp
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Materials Research Corp filed Critical Materials Research Corp
Publication of DE19581926T1 publication Critical patent/DE19581926T1/de
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B26/00—Obtaining alkali, alkaline earth metals or magnesium
    • C22B26/20—Obtaining alkaline earth metals or magnesium
    • C22B26/22—Obtaining magnesium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10—Vacuum distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/42—Regulation; Control
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
    • C22B9/02—Refining by liquating, filtering, centrifuging, distilling, or supersonic wave action including acoustic waves
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B9/00—General processes of refining or remelting of metals; Apparatus for electroslag or arc remelting of metals
    • C22B9/04—Refining by applying a vacuum
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00—Technologies related to metal processing
    • Y02P10/20—Recycling

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Metallurgy (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Organic Chemistry (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Physics & Mathematics (AREA)
  • Acoustics & Sound (AREA)
  • Manufacture And Refinement Of Metals (AREA)
DE19581926T 1995-02-21 1995-11-09 Verfahren und Vorrichtung zur Reinigung durch Vakuumdestillation zum Herstellen von Magnesium ultra-hoher Reinheit Withdrawn DE19581926T1 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US08/391,047 US5582630A (en) 1995-02-21 1995-02-21 Ultra high purity magnesium vacuum distillation purification method
PCT/US1995/014434 WO1996026297A1 (en) 1995-02-21 1995-11-09 Ultra high purity magnesium and vacuum distillation purification method and apparatus

Publications (1)

Publication Number Publication Date
DE19581926T1 true DE19581926T1 (de) 1998-02-12

Family

ID=23544997

Family Applications (1)

Application Number Title Priority Date Filing Date
DE19581926T Withdrawn DE19581926T1 (de) 1995-02-21 1995-11-09 Verfahren und Vorrichtung zur Reinigung durch Vakuumdestillation zum Herstellen von Magnesium ultra-hoher Reinheit

Country Status (8)

Country Link
US (2) US5582630A (de)
JP (1) JPH11502565A (de)
AU (1) AU4147996A (de)
CH (1) CH689865A5 (de)
DE (1) DE19581926T1 (de)
LU (1) LU90125B1 (de)
TW (1) TW328550B (de)
WO (1) WO1996026297A1 (de)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2730309C2 (ru) * 2012-01-19 2020-08-21 Етх Цюрих Способ и устройство для получения высокочистого магния

Families Citing this family (35)

* Cited by examiner, † Cited by third party
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US6627149B1 (en) 1996-06-21 2003-09-30 Dowa Mining Co., Ltd. High-purity silver wires for use in recording, acoustic or image transmission applications
JP3725621B2 (ja) * 1996-06-21 2005-12-14 同和鉱業株式会社 記録用または音響もしくは画像送信用高純度銀線
JP3857589B2 (ja) * 2002-01-28 2006-12-13 同和鉱業株式会社 高純度金属の精製方法及び精製装置
RU2222623C1 (ru) * 2002-05-18 2004-01-27 Открытое акционерное общество "Российский научно-исследовательский и проектный институт титана и магния" Печь для рафинирования магния
WO2005009729A2 (en) 2003-07-24 2005-02-03 Tecomet, Inc. Assembled non-random foams
UA74941C2 (en) * 2004-04-26 2006-02-15 Fos Internat S A A metal-thermal process for producing magnesium and vacuum induction furnace for realizing the same
RU2283886C1 (ru) * 2004-12-30 2006-09-20 Открытое Акционерное Общество "Корпорация Всмпо-Ависма" Печь для рафинирования магния
CN1317405C (zh) * 2005-09-28 2007-05-23 中国科学院物理研究所 一种高纯材料的高真空原位两步精炼方法
CN1302133C (zh) * 2005-09-30 2007-02-28 中国科学院物理研究所 一种用于提炼高纯材料的高真空原位精炼装置
CN101386919B (zh) * 2008-10-24 2011-12-28 贵阳铝镁设计研究院有限公司 一种高纯镁的制备方法及装置
EP2493523B1 (de) * 2009-10-30 2014-06-18 Acrostak Corp BVI, Tortola Biologisch abbaubare implantierbare medizinische vorrichtungen aus superreinem material auf magnesiumbasis
CN101948958A (zh) * 2009-12-30 2011-01-19 陈静 一种有色金属真空电磁悬浮蒸馏精炼方法及设备
CN101948957B (zh) * 2010-10-14 2012-07-04 宁波翔博机械有限公司 一种镁合金的真空蒸馏方法
JP5290387B2 (ja) * 2011-12-07 2013-09-18 Ｊｘ日鉱日石金属株式会社 高純度カルシウムの製造方法
CN103184348B (zh) * 2011-12-28 2014-09-17 广东先导稀材股份有限公司 高纯锌的制备方法及设备
EP2864514B1 (de) 2012-06-26 2020-04-29 Biotronik AG Implantat aus einer magnesiumlegierung, verfahren zur herstellung davon und verwendung davon
EP3896181A1 (de) * 2012-06-26 2021-10-20 Biotronik AG Magnesiumlegierung, verfahren zur herstellung davon und verwendung davon
AU2013283537A1 (en) * 2012-06-26 2014-11-06 Biotronik Ag Magnesium-zinc-calcium alloy, method for production thereof, and use thereof
SG11201406026TA (en) * 2012-06-26 2014-10-30 Biotronik Ag Magnesium-zinc-calcium alloy, method for production thereof, and use thereof
KR101391422B1 (ko) * 2012-10-09 2014-05-12 김주영 환원물질의 배출 성능이 개선된 마그네슘 제련용 수직형 레토르트
CN103526036B (zh) * 2013-11-04 2014-12-10 柳州英格尔金属有限责任公司 一种铟脱杂用竖式真空蒸馏系统
US11513042B2 (en) * 2015-01-26 2022-11-29 SPEX SamplePrep, LLC Power-compensated fusion furnace
RU2635117C2 (ru) * 2015-12-25 2017-11-09 Общество с ограниченной ответственностью "СМВ Инжиниринг" (ООО "СМВ Инжиниринг") Способ рафинирования магния и его сплавов
JP6865067B2 (ja) * 2017-03-06 2021-04-28 高周波熱錬株式会社 マグネシウムの精製方法及びマグネシウムの精製装置
EP3388539A1 (de) * 2017-04-11 2018-10-17 Biotronik AG Vorrichtung und verfahren zur erzeugung von gereinigtem, insbesondere hochreinem, magnesium
CN110538478B (zh) * 2018-10-29 2024-07-26 天津包钢稀土研究院有限责任公司 一种高品质无水稀土卤化物提纯装置
US11045742B2 (en) 2019-11-22 2021-06-29 Jaxon Technologies, LLC Temperature controlled purification module and method
CN110894065B (zh) * 2019-12-18 2023-04-07 中南大学 一种制备高纯碲的设备及方法
CN111097920B (zh) * 2020-01-03 2021-02-02 四川万邦胜辉新能源科技有限公司 一种气态共冷凝法生产镁锂合金的方法
CN111424184B (zh) * 2020-04-17 2022-04-22 包头稀土研究院 一次连续还原蒸馏制备高纯金属镱的方法
CN112195348B (zh) * 2020-09-14 2021-09-07 昆明理工大学 一种半连续制备不同纯度高纯镁的设备及方法
CN113649531B (zh) * 2021-08-16 2023-07-14 江西中晶新材料有限公司 一种5n锌锭的生产方法
CN115401206B (zh) * 2022-08-25 2024-04-16 昆明理工大学 一种制备高纯球形镁和/或高纯镁粉的设备及方法
CN115449648A (zh) * 2022-08-30 2022-12-09 昆明理工大学 一种煅白真空碳热还原炼镁设备及方法
CN115821069B (zh) * 2022-12-07 2023-06-16 云南国钛金属股份有限公司 一种转子级海绵钛倒u型蒸馏工序温度控制方法

Family Cites Families (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1143644B (de) * 1960-10-12 1963-02-14 Knapsack Ag Verfahren zur Gewinnung von Magnesium durch elektrothermische Reduktion von Dolomit
US3767381A (en) * 1971-07-28 1973-10-23 Alco Standard Corp Furnace and method of using the same for reclaiming metal
JPS537886B2 (de) * 1972-07-19 1978-03-23
JPS58221242A (ja) * 1982-06-17 1983-12-22 Japan Metals & Chem Co Ltd 金属マグネシウム製造装置
US5078789A (en) * 1990-10-31 1992-01-07 Westinghouse Electric Corp. Continuous vacuum distillation and furnace therefor

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2730309C2 (ru) * 2012-01-19 2020-08-21 Етх Цюрих Способ и устройство для получения высокочистого магния

Also Published As

Publication number Publication date
AU4147996A (en) 1996-09-11
WO1996026297A1 (en) 1996-08-29
US5698158A (en) 1997-12-16
CH689865A5 (de) 1999-12-31
US5582630A (en) 1996-12-10
LU90125B1 (fr) 1997-11-13
TW328550B (en) 1998-03-21
JPH11502565A (ja) 1999-03-02

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Legal Events

Date Code Title Description
OP8 Request for examination as to paragraph 44 patent law
8125 Change of the main classification

Ipc: C22B 26/22

8607 Notification of search results after publication
8136 Disposal/non-payment of the fee for publication/grant