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DE102004023249A1 - Process to insert selected catalyst rings into battery of reactor tubes followed by manual removal as required - Google Patents

Process to insert selected catalyst rings into battery of reactor tubes followed by manual removal as required Download PDF

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Publication number
DE102004023249A1
DE102004023249A1 DE102004023249A DE102004023249A DE102004023249A1 DE 102004023249 A1 DE102004023249 A1 DE 102004023249A1 DE 102004023249 A DE102004023249 A DE 102004023249A DE 102004023249 A DE102004023249 A DE 102004023249A DE 102004023249 A1 DE102004023249 A1 DE 102004023249A1
Authority
DE
Germany
Prior art keywords
battery
reactor tubes
manual removal
selected catalyst
insert selected
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE102004023249A
Other languages
German (de)
Inventor
Martin Dieterle
Knut Eger
Klaus Joachim Mueller-Engel
Ulrich Hammon
Volker Schliephake
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
BASF SE
Original Assignee
BASF SE
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by BASF SE filed Critical BASF SE
Priority to DE102004023249A priority Critical patent/DE102004023249A1/en
Publication of DE102004023249A1 publication Critical patent/DE102004023249A1/en
Priority to BRPI0509632A priority patent/BRPI0509632B1/en
Priority to JP2007511930A priority patent/JP4768726B2/en
Priority to KR1020127028080A priority patent/KR101431365B1/en
Priority to CN201410148068.4A priority patent/CN103908927A/en
Priority to EP05737721.0A priority patent/EP1748839B1/en
Priority to KR1020067025734A priority patent/KR101237662B1/en
Priority to RU2006143086/15A priority patent/RU2393915C2/en
Priority to PCT/EP2005/004351 priority patent/WO2005113123A1/en
Priority to CN201410148505.2A priority patent/CN103894117A/en
Priority to CNA2005800146017A priority patent/CN1956773A/en
Priority to US11/118,433 priority patent/US7731916B2/en
Priority to MYPI20052014A priority patent/MY139283A/en
Priority to TW094114787A priority patent/TWI360436B/en
Priority to ZA200610181A priority patent/ZA200610181B/en
Priority to US12/756,424 priority patent/US20100197489A1/en
Withdrawn legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B01J8/003—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor in a downward flow
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/002—Mixed oxides other than spinels, e.g. perovskite
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/0015—Feeding of the particles in the reactor; Evacuation of the particles out of the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
    • B01J8/02—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds
    • B01J8/06—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes with stationary particles, e.g. in fixed beds in tube reactors; the solid particles being arranged in tubes
    • B01J8/067—Heating or cooling the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00008—Controlling the process
    • B01J2208/00017—Controlling the temperature
    • B01J2208/00106—Controlling the temperature by indirect heat exchange
    • B01J2208/00168—Controlling the temperature by indirect heat exchange with heat exchange elements outside the bed of solid particles
    • B01J2208/00212—Plates; Jackets; Cylinders
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00752—Feeding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00743—Feeding or discharging of solids
    • B01J2208/00769—Details of feeding or discharging
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/00796—Details of the reactor or of the particulate material
    • B01J2208/00805—Details of the particulate material
    • B01J2208/00814—Details of the particulate material the particulate material being provides in prefilled containers
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2208/00—Processes carried out in the presence of solid particles; Reactors therefor
    • B01J2208/02—Processes carried out in the presence of solid particles; Reactors therefor with stationary particles
    • B01J2208/023—Details
    • B01J2208/024—Particulate material
    • B01J2208/025—Two or more types of catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/30—Details relating to random packing elements
    • B01J2219/308—Details relating to random packing elements filling or discharging the elements into or from packed columns
    • B01J2219/3086—Filling of the packing elements into the column or vessel, e.g. using a tube
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/70—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper
    • B01J23/76—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36
    • B01J23/84—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of the iron group metals or copper combined with metals, oxides or hydroxides provided for in groups B01J23/02 - B01J23/36 with arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/85—Chromium, molybdenum or tungsten
    • B01J23/888—Tungsten
    • B01J23/8885—Tungsten containing also molybdenum
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2523/00—Constitutive chemical elements of heterogeneous catalysts
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/19—Catalysts containing parts with different compositions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/50—Catalysts, in general, characterised by their form or physical properties characterised by their shape or configuration
    • B01J35/55—Cylinders or rings

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Devices And Processes Conducted In The Presence Of Fluids And Solid Particles (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

Ein Verfahren der strukturierten Befüllung von Kontaktrohren eines Kontaktrohrbündels, bei dem zur Erzeugung eines Befüllungsabschnitts einheitlich vorportionierte Zusammenstellungen von Katalysatorformkörpern verwendet werden.A method of structured filling of contact tubes of a catalyst tube bundle, in which uniformly pre-portioned assemblies of shaped catalyst bodies are used to produce a filling section.

DE102004023249A 2004-05-07 2004-05-07 Process to insert selected catalyst rings into battery of reactor tubes followed by manual removal as required Withdrawn DE102004023249A1 (en)

Priority Applications (16)

Application Number Priority Date Filing Date Title
DE102004023249A DE102004023249A1 (en) 2004-05-07 2004-05-07 Process to insert selected catalyst rings into battery of reactor tubes followed by manual removal as required
CNA2005800146017A CN1956773A (en) 2004-05-07 2005-04-22 Method for packing catalyst tubes in a catalyst tube bundle in a structured manner
KR1020067025734A KR101237662B1 (en) 2004-05-07 2005-04-22 Method for structurally filling contact tubes of a bank of contact tubes
PCT/EP2005/004351 WO2005113123A1 (en) 2004-05-07 2005-04-22 Method for structurally filling contact tubes of a bank of contact tubes
KR1020127028080A KR101431365B1 (en) 2004-05-07 2005-04-22 Method for structurally filling contact tubes of a bank of contact tubes
CN201410148068.4A CN103908927A (en) 2004-05-07 2005-04-22 Process to fill catalyst tube into catalyst ring in structural manner
EP05737721.0A EP1748839B1 (en) 2004-05-07 2005-04-22 Method for structurally filling contact tubes of a bank of contact tubes
BRPI0509632A BRPI0509632B1 (en) 2004-05-07 2005-04-22 process for loading contact tubes from a contact tube bundle in a structured manner
RU2006143086/15A RU2393915C2 (en) 2004-05-07 2005-04-22 Method of structured filling of contact tubes of contact tube bundle and package produced on wrapping by quantitative portion of formed catalyst product composition
JP2007511930A JP4768726B2 (en) 2004-05-07 2005-04-22 Method for structurally filling contact tubes of a contact tube bundle
CN201410148505.2A CN103894117A (en) 2004-05-07 2005-04-22 Method for structurally filing contact tubes of a bank of contact tubes
US11/118,433 US7731916B2 (en) 2004-05-07 2005-05-02 Method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion
MYPI20052014A MY139283A (en) 2004-05-07 2005-05-05 Method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion
TW094114787A TWI360436B (en) 2004-05-07 2005-05-06 Method of charging catalyst tubes of a bundle of c
ZA200610181A ZA200610181B (en) 2004-05-07 2006-12-05 Method for structurally filing contact tubes of a bank of contact tubes
US12/756,424 US20100197489A1 (en) 2004-05-07 2010-04-08 Method of charging catalyst tubes of a bundle of catalyst tubes in a structured fashion

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE102004023249A DE102004023249A1 (en) 2004-05-07 2004-05-07 Process to insert selected catalyst rings into battery of reactor tubes followed by manual removal as required

Publications (1)

Publication Number Publication Date
DE102004023249A1 true DE102004023249A1 (en) 2005-03-10

Family

ID=34178117

Family Applications (1)

Application Number Title Priority Date Filing Date
DE102004023249A Withdrawn DE102004023249A1 (en) 2004-05-07 2004-05-07 Process to insert selected catalyst rings into battery of reactor tubes followed by manual removal as required

Country Status (6)

Country Link
JP (1) JP4768726B2 (en)
KR (1) KR101431365B1 (en)
CN (3) CN103908927A (en)
DE (1) DE102004023249A1 (en)
RU (1) RU2393915C2 (en)
ZA (1) ZA200610181B (en)

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007028332A1 (en) 2007-06-15 2008-12-18 Basf Se A method for feeding a reactor with a fixed catalyst bed comprising at least annular shaped catalyst bodies K.
DE102007028333A1 (en) 2007-06-15 2008-12-18 Basf Se Method for introducing a subset taken from at least one production batch of annular shell catalysts K into a reaction tube of a tube bundle reactor
DE202008004922U1 (en) 2008-04-10 2009-08-20 Süd-Chemie AG Feeding system for tube bundle reactors
DE102014016203A1 (en) 2014-11-03 2016-05-19 Clariant International Ltd. Feeding system for feeding a tube bundle reactor
EP3112014A1 (en) * 2015-06-30 2017-01-04 Shell Internationale Research Maatschappij B.V. Method of loading a particulate material into a reactor
WO2021048373A1 (en) * 2019-09-13 2021-03-18 Hte Gmbh The High Throughput Experimentation Company Method for filling reactors and for examining catalytic reactors

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007017080A1 (en) * 2007-04-10 2008-10-16 Basf Se Method for feeding a longitudinal section of a contact tube

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NL62754C (en) * 1941-01-27
IT955185B (en) * 1972-04-29 1973-09-29 Saes Getter Spa CATALYTIC CARTRIDGE
KR830000312B1 (en) * 1978-03-13 1983-03-02 유씨비, 에스. 에이. Plastic container body for pressurized carbonated beverage
US4402643A (en) * 1981-02-18 1983-09-06 Ppg Industries, Inc. Catalyst loader
JPS63197533A (en) * 1987-12-28 1988-08-16 ケミカル・リサーチ・アンド・ライセンシング・カンパニー Catalytic distillation catalyst structure
EP0396650B2 (en) * 1988-09-02 1995-04-12 GebràœDer Sulzer Aktiengesellschaft Device for carrying out catalytic reactions
JPH0784400B2 (en) * 1990-04-03 1995-09-13 株式会社日本触媒 Process for producing unsaturated aldehyde and unsaturated acid
WO1992002348A1 (en) * 1990-08-01 1992-02-20 H.B. Fuller Licensing And Financing Inc. Method of packaging an adhesive composition and corresponding packaged article
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US5266546A (en) * 1992-06-22 1993-11-30 Chemical Research & Licensing Company Catalytic distillation machine
EP0631813B1 (en) * 1993-06-30 1998-01-07 Sulzer Chemtech AG Catalysing fixed-bed reactor
DE4442346A1 (en) * 1994-11-29 1996-05-30 Basf Ag Process for producing a catalyst consisting of a support body and a catalytically active oxide mass applied to the surface of the support body
WO1998014392A1 (en) * 1996-10-22 1998-04-09 Comardo Mathis P Catalytic reactor charging system and method
JP3891726B2 (en) * 1999-04-12 2007-03-14 三井化学株式会社 Filling method of organopolymer siloxane catalyst
DE19934324A1 (en) * 1999-07-21 2000-09-07 Basf Ag Apparatus for filling tubular reactors with catalyst particles comprises a filling tube that can be moved in a frame structure in two directions
WO2001094006A2 (en) * 2000-06-07 2001-12-13 Abb Lummus Global, Inc. Heat exchanger/reactor apparatus
CN1172823C (en) * 2001-05-30 2004-10-27 中国石油化工股份有限公司 A kind of packaging bag and its application in catalyst packaging
JP4092090B2 (en) * 2001-06-26 2008-05-28 株式会社日本触媒 Solid particle packed reactor and catalytic gas phase oxidation method using the reactor
US7182778B2 (en) * 2001-11-01 2007-02-27 Gel Tech Solutions, Inc. Conforming thermal pack

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE102007028332A1 (en) 2007-06-15 2008-12-18 Basf Se A method for feeding a reactor with a fixed catalyst bed comprising at least annular shaped catalyst bodies K.
DE102007028333A1 (en) 2007-06-15 2008-12-18 Basf Se Method for introducing a subset taken from at least one production batch of annular shell catalysts K into a reaction tube of a tube bundle reactor
DE202008004922U1 (en) 2008-04-10 2009-08-20 Süd-Chemie AG Feeding system for tube bundle reactors
DE102014016203A1 (en) 2014-11-03 2016-05-19 Clariant International Ltd. Feeding system for feeding a tube bundle reactor
EP3112014A1 (en) * 2015-06-30 2017-01-04 Shell Internationale Research Maatschappij B.V. Method of loading a particulate material into a reactor
WO2021048373A1 (en) * 2019-09-13 2021-03-18 Hte Gmbh The High Throughput Experimentation Company Method for filling reactors and for examining catalytic reactors
US11738316B2 (en) 2019-09-13 2023-08-29 Hte Gmbh The High Throughput Experimentation Method for filling reactors and for examining catalytic reactors

Also Published As

Publication number Publication date
RU2393915C2 (en) 2010-07-10
CN103908927A (en) 2014-07-09
CN103894117A (en) 2014-07-02
JP2007536078A (en) 2007-12-13
JP4768726B2 (en) 2011-09-07
ZA200610181B (en) 2008-05-28
CN1956773A (en) 2007-05-02
KR20120134146A (en) 2012-12-11
RU2006143086A (en) 2008-06-20
KR101431365B1 (en) 2014-08-18

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