DE1003385B - Lubricants and lubricants - Google Patents
Lubricants and lubricantsInfo
- Publication number
- DE1003385B DE1003385B DEB38243A DEB0038243A DE1003385B DE 1003385 B DE1003385 B DE 1003385B DE B38243 A DEB38243 A DE B38243A DE B0038243 A DEB0038243 A DE B0038243A DE 1003385 B DE1003385 B DE 1003385B
- Authority
- DE
- Germany
- Prior art keywords
- lubricants
- disulfide
- ammonium
- molybdenum
- grain size
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000000314 lubricant Substances 0.000 title claims description 13
- CWQXQMHSOZUFJS-UHFFFAOYSA-N molybdenum disulfide Chemical compound S=[Mo]=S CWQXQMHSOZUFJS-UHFFFAOYSA-N 0.000 claims description 13
- 229910052982 molybdenum disulfide Inorganic materials 0.000 claims description 9
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims description 6
- 239000000203 mixture Substances 0.000 claims description 6
- ITRNXVSDJBHYNJ-UHFFFAOYSA-N tungsten disulfide Chemical compound S=[W]=S ITRNXVSDJBHYNJ-UHFFFAOYSA-N 0.000 claims description 5
- BWGNESOTFCXPMA-UHFFFAOYSA-N Dihydrogen disulfide Chemical compound SS BWGNESOTFCXPMA-UHFFFAOYSA-N 0.000 claims description 2
- 238000005979 thermal decomposition reaction Methods 0.000 claims 1
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 4
- 150000002019 disulfides Chemical class 0.000 description 3
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 2
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 2
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- 229910021529 ammonia Inorganic materials 0.000 description 2
- 239000007864 aqueous solution Substances 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 230000001050 lubricating effect Effects 0.000 description 2
- 229920000642 polymer Polymers 0.000 description 2
- ZYECOAILUNWEAL-NUDFZHEQSA-N (4z)-4-[[2-methoxy-5-(phenylcarbamoyl)phenyl]hydrazinylidene]-n-(3-nitrophenyl)-3-oxonaphthalene-2-carboxamide Chemical compound COC1=CC=C(C(=O)NC=2C=CC=CC=2)C=C1N\N=C(C1=CC=CC=C1C=1)/C(=O)C=1C(=O)NC1=CC=CC([N+]([O-])=O)=C1 ZYECOAILUNWEAL-NUDFZHEQSA-N 0.000 description 1
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- 239000004952 Polyamide Substances 0.000 description 1
- 241000589614 Pseudomonas stutzeri Species 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical compound [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 description 1
- 229940010552 ammonium molybdate Drugs 0.000 description 1
- 235000018660 ammonium molybdate Nutrition 0.000 description 1
- 239000011609 ammonium molybdate Substances 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 229910002092 carbon dioxide Inorganic materials 0.000 description 1
- 239000001569 carbon dioxide Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- VLAPMBHFAWRUQP-UHFFFAOYSA-L molybdic acid Chemical compound O[Mo](O)(=O)=O VLAPMBHFAWRUQP-UHFFFAOYSA-L 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 229920002647 polyamide Polymers 0.000 description 1
- 229920000915 polyvinyl chloride Polymers 0.000 description 1
- 239000004800 polyvinyl chloride Substances 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000002244 precipitate Substances 0.000 description 1
- 229920006395 saturated elastomer Polymers 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000000243 solution Substances 0.000 description 1
- 150000004763 sulfides Chemical class 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M7/00—Solid or semi-solid compositions essentially based on lubricating components other than mineral lubricating oils or fatty oils and their use as lubricants; Use as lubricants of single solid or semi-solid substances
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/04—Elements
- C10M2201/041—Carbon; Graphite; Carbon black
- C10M2201/042—Carbon; Graphite; Carbon black halogenated, i.e. graphite fluoride
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/06—Metal compounds
- C10M2201/065—Sulfides; Selenides; Tellurides
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2201/00—Inorganic compounds or elements as ingredients in lubricant compositions
- C10M2201/06—Metal compounds
- C10M2201/065—Sulfides; Selenides; Tellurides
- C10M2201/066—Molybdenum sulfide
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2205/00—Organic macromolecular hydrocarbon compounds or fractions, whether or not modified by oxidation as ingredients in lubricant compositions
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2211/00—Organic non-macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2211/06—Perfluorinated compounds
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2213/00—Organic macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2213/02—Organic macromolecular compounds containing halogen as ingredients in lubricant compositions obtained from monomers containing carbon, hydrogen and halogen only
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2213/00—Organic macromolecular compounds containing halogen as ingredients in lubricant compositions
- C10M2213/06—Perfluoro polymers
- C10M2213/062—Polytetrafluoroethylene [PTFE]
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/04—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2217/042—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds between the nitrogen-containing monomer and an aldehyde or ketone
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/04—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2217/043—Mannich bases
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/04—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2217/044—Polyamides
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10M—LUBRICATING COMPOSITIONS; USE OF CHEMICAL SUBSTANCES EITHER ALONE OR AS LUBRICATING INGREDIENTS IN A LUBRICATING COMPOSITION
- C10M2217/00—Organic macromolecular compounds containing nitrogen as ingredients in lubricant compositions
- C10M2217/04—Macromolecular compounds from nitrogen-containing monomers obtained otherwise than by reactions only involving carbon-to-carbon unsaturated bonds
- C10M2217/045—Polyureas; Polyurethanes
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2050/00—Form in which the lubricant is applied to the material being lubricated
- C10N2050/08—Solids
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2050/00—Form in which the lubricant is applied to the material being lubricated
- C10N2050/10—Form in which the lubricant is applied to the material being lubricated semi-solid; greasy
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Lubricants (AREA)
Description
Schmier- und Gleitmittel Zusatz zur Patentanmeldung B 31055 IVc / 23 c Gegenstand derHauptpatentanmeldungB 31055 IVc/23c ist die Verwendung von in bekannter Weise aus Ammoniumsulfomolybdaten oder Ammoniumsulfowolframaten erhältlichem Molybdändisulfid oder Wolframdisulfid als Schmier- und Gleitmittel.Lubricants and lubricants addendum to patent application B 31055 IVc / 23 c The subject of the main patent application B 31055 IVc / 23c is the use of in known manner from ammonium sulfomolybdates or ammonium sulfotungstates obtainable Molybdenum disulfide or tungsten disulfide as a lubricant and lubricant.
Es wurde gefunden, daß man besonders gute Schmier-und Gleitmittel erhält, wenn man ein Molybdändisulfid oder Wolframdisulfid gemäß der Hauptpatentanmeldung B 31055 I V c/23 c in Mischung mit einem natürlichen Molybdändisulfid verwendet, wobei das synthetische Disulfid in einer Korngröße unterhalb 40,u und das natürliche Molybdändisulfid in einer Körnung zwischen 40 und 80,u vorliegen muß.It has been found that particularly good lubricants and lubricants are obtained if a molybdenum disulfide or tungsten disulfide according to the main patent application B 31055 IV c / 23 c is used in a mixture with a natural molybdenum disulfide, the synthetic disulfide having a grain size below 40, u and the natural molybdenum disulphide must be present in a grain size between 40 and 80 u.
Die nach der Hauptpatentanmeldung B 31055IV c/23 c als Schmier- und Gleitmittel verwendeten Molybdän- und Wolframdisulfide werden in bekannter Weise, z. B. aus durch Behandlung wäßriger Lösungen von Ammoniummolybdat bzw. Ammoniumwolframat mit Schwefelwasserstoff oder geeigneten Sulfiden erhaltenen Ammoniumsulfomolybdaten bzw. -wolframaten durch deren Erhitzen auf Temperaturen von oberhalb 250°, insbesondere 400 bis 600°, in einem Gasstrom von z. B. Stickstoff, Ammoniak, Kohlendioxyd, insbesondere aber Wasserstoff, erhalten.According to the main patent application B 31055IV c / 23 c as lubricating and Molybdenum and tungsten disulfides used in lubricants are used in a known manner, z. B. from by treating aqueous solutions of ammonium molybdate or ammonium tungstate ammonium sulfomolybdates obtained with hydrogen sulfide or suitable sulfides or tungstates by heating them to temperatures above 250 °, in particular 400 to 600 °, in a gas stream of z. B. nitrogen, ammonia, carbon dioxide, in particular but get hydrogen.
Diese synthetischen Disulfide werden durch Zerkleinerung in an sich bekannten Mahlvorrichtungen auf eine Korngröße von unterhalb 40,u, zweckmäßig zwischen 1 und 30,u, vorteilhaft 1 und 10,u, gebracht, während für das natürliche Molybdändisulfid im allgemeinen Korngrößen zwischen 40 und 80,u, insbesondere 50 und 70,u gewählt werden. Nur bei Mischungen der beiden Komponenten in den genannten Korngrößen wird die verbesserte Schmierwirkung erzielt. Die synthetischen Disulfide werden dem natürlichen Molybdändisulfid in einer Menge von 5 bis 50 Gewichtsprozent, vorteilhaft von 15 bis 40 Gewichtsprozent, zugegeben.These synthetic disulfides are broken down by crushing in themselves known grinding devices to a grain size of below 40, u, expediently between 1 and 30, u, advantageously 1 and 10, u, while for the natural molybdenum disulfide generally grain sizes between 40 and 80, u, in particular 50 and 70, u are selected will. Only when the two components are mixed in the specified grain sizes the improved lubricating effect achieved. The synthetic disulfides become the natural ones Molybdenum disulfide in an amount of 5 to 50 percent by weight, advantageously 15 up to 40 percent by weight, added.
Diese Gemische können gegebenenfalls auch unter Zusatz von Graphit und/oder festen hochmolekularen temperaturbeständigen Polymerisaten wie Polyvinylchlorid, Polyamiden, polymerisierten Olefinen, Harnstoffpolymerisaten als Schmier- und Gleitmittel verwendet werden.These mixtures can optionally also with the addition of graphite and / or solid, high molecular weight, temperature-resistant polymers such as polyvinyl chloride, Polyamides, polymerized olefins, urea polymers as lubricants and lubricants be used.
Beispiel In eine wäßrige Lösung, die 200/, Molybdänsäure und 15 % Ammoniak enthält, wird bei 50° Schwefelwasserstoff bis zur Sättigung eingeleitet. Die Lösung wird anschließend auf Zimmertemperatur abgekühlt. Die dabei ausfallenden rotvioletten Nadeln des Ammoniumsulfomolybdats werden abgesaugt, mit Stickstoff abgeblasen, langsam getrocknet und schließlich im trockenen Wasserstoffstrom bei 600° zu Molybdändisulfid zersetzt. Dieses Disulfid wird dann auf eine Körnung von 1 bis 5,u gemahlen.EXAMPLE In an aqueous solution containing 200 % molybdic acid and 15% ammonia, hydrogen sulphide is passed at 50 ° until it is saturated. The solution is then cooled to room temperature. The red-violet needles of ammonium sulfomolybdate which precipitate out are filtered off with suction, blown off with nitrogen, slowly dried and finally decomposed in a stream of dry hydrogen at 600 ° to form molybdenum disulfide. This disulfide is then ground to a grain size of 1 to 5 microns.
Das so erzeugte Pulver wird in einer Menge von 25 Gewichtsprozent einem natürlichen Molybdändisulfid von einer Körnung von 50 bis 70,u zugegeben.The powder thus produced is used in an amount of 25 percent by weight a natural molybdenum disulphide with a grain size of 50 to 70 µ added.
In der Almen-Wieland-Maschine ergibt die Mischung eine Endbelastung von 2300 kg bei 350 kg Reibungskraft. Bei derselben Reibungskraft verträgt das natürliche Molybdändisulfid für sich allein nur eine Belastung von 2000 kg. Die Mischung ermöglicht also eine höhere Belastung und gibt einen niederen Reibungskoeffizienten von 0,152 gegen 0,175.In the Almen-Wieland machine, the mixture results in a final load of 2300 kg at 350 kg friction force. The natural can tolerate the same frictional force Molybdenum disulphide alone only carries a load of 2000 kg. The mix makes it possible thus a higher load and gives a lower coefficient of friction of 0.152 against 0.175.
Claims (2)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEB38243A DE1003385B (en) | 1955-12-10 | 1955-12-10 | Lubricants and lubricants |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEB38243A DE1003385B (en) | 1955-12-10 | 1955-12-10 | Lubricants and lubricants |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1003385B true DE1003385B (en) | 1957-02-28 |
Family
ID=6965436
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEB38243A Pending DE1003385B (en) | 1955-12-10 | 1955-12-10 | Lubricants and lubricants |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE1003385B (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1288220B (en) * | 1962-04-19 | 1969-01-30 | Acheson Ind Inc | Thread lubricant |
-
1955
- 1955-12-10 DE DEB38243A patent/DE1003385B/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1288220B (en) * | 1962-04-19 | 1969-01-30 | Acheson Ind Inc | Thread lubricant |
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