DE1000223B - Freeze-drying process of meat - Google Patents
Freeze-drying process of meatInfo
- Publication number
- DE1000223B DE1000223B DEL23316A DEL0023316A DE1000223B DE 1000223 B DE1000223 B DE 1000223B DE L23316 A DEL23316 A DE L23316A DE L0023316 A DEL0023316 A DE L0023316A DE 1000223 B DE1000223 B DE 1000223B
- Authority
- DE
- Germany
- Prior art keywords
- meat
- residual moisture
- freeze
- drying process
- packaging
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 235000013372 meat Nutrition 0.000 title claims description 25
- 238000000034 method Methods 0.000 title claims description 24
- 238000004108 freeze drying Methods 0.000 title claims description 12
- 238000001035 drying Methods 0.000 claims description 12
- 235000013305 food Nutrition 0.000 claims description 7
- 238000007710 freezing Methods 0.000 claims description 6
- 230000008014 freezing Effects 0.000 claims description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 3
- 239000000126 substance Substances 0.000 claims description 2
- 238000004806 packaging method and process Methods 0.000 claims 6
- 238000012360 testing method Methods 0.000 claims 3
- 230000015572 biosynthetic process Effects 0.000 claims 2
- 230000006866 deterioration Effects 0.000 claims 2
- 238000004519 manufacturing process Methods 0.000 claims 2
- 239000004033 plastic Substances 0.000 claims 2
- 229920003023 plastic Polymers 0.000 claims 2
- 238000011156 evaluation Methods 0.000 claims 1
- 230000008020 evaporation Effects 0.000 claims 1
- 238000001704 evaporation Methods 0.000 claims 1
- 239000005022 packaging material Substances 0.000 claims 1
- 238000012372 quality testing Methods 0.000 claims 1
- 230000000717 retained effect Effects 0.000 claims 1
- 108090000790 Enzymes Proteins 0.000 description 2
- 102000004190 Enzymes Human genes 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 235000015177 dried meat Nutrition 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108010074860 Factor Xa Proteins 0.000 description 1
- 241000287828 Gallus gallus Species 0.000 description 1
- 102000003505 Myosin Human genes 0.000 description 1
- 108060008487 Myosin Proteins 0.000 description 1
- 230000000721 bacterilogical effect Effects 0.000 description 1
- 230000001413 cellular effect Effects 0.000 description 1
- 238000001246 colloidal dispersion Methods 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 230000006378 damage Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000002255 enzymatic effect Effects 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 230000005923 long-lasting effect Effects 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 235000016709 nutrition Nutrition 0.000 description 1
- 230000035764 nutrition Effects 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 235000013324 preserved food Nutrition 0.000 description 1
- 238000000859 sublimation Methods 0.000 description 1
- 230000008022 sublimation Effects 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVATION OF FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES; CHEMICAL RIPENING OF FRUIT OR VEGETABLES
- A23B4/00—Preservation of meat, sausages, fish or fish products
- A23B4/03—Drying; Subsequent reconstitution
- A23B4/037—Freeze-drying, i.e. cryodesiccation or lyophilisation; Apparatus therefor
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Meat, Egg Or Seafood Products (AREA)
- Freezing, Cooling And Drying Of Foods (AREA)
Description
DEUTSCHESGERMAN
Für die Haltbarmachung von Lebensmitteln ist Trocknung das bevorzugte Verfahren. Bakteriologische oder enzymatische Zersetzungsprozesse können hierbei unter geeigneten Bedingungen ausgeschaltet werden. Außerdem stellt der Gewichtsverlust des Produktes einen weiteren Vorteil dar.Drying is the preferred method for preserving food. Bacteriological or enzymatic decomposition processes can be switched off under suitable conditions will. In addition, the weight loss of the product is another benefit.
Fast alle Lebensmittel haben sich bisher mit Erfolg trocknen lassen. Eine Ausnahme bildet jedoch das Fleisch. Die Ursache für die schlechten Resultate liegen vor allem in der Eiweißnatur der zellulären wie der faserigen Bauelemente der Muskulatur. Sie bedingt die Tendenz vor allem der Myosinmoleküle, bei den gebräuchlichen Trocknungsverfahren ihre kolloidale Dispersion zu verlieren und zu koagulieren. Es gelingt daher nicht, wie bei den meisten anderen Lebensmitteln, die Diffusion des Wassers wahrend der Trocknung so zu beeinflussen, daß es an der Oberfläche verdampft, ohne zur Entstehung eines harten, zusammengeschrumpften und nur schwer wieder mit Wasser zu durchfeuchtenden Produktes zu führen. Vielmehr tritt eine Denaturierung der Eiweißmoleküle ein, wobei das Trocknungsprodukt neben der Zerstörung von Enzymen weitere chemische Veränderungen erleidet. Es ist demnach äußerst wichtig, ein wirtschaftliches Verfahren zu finden, welches eine Überführung von Fleisch in eine lagerfähige Trockenform unter Erhaltung seiner wichtigsten Eigenschaften als Lebensmittel ermöglicht.Almost all foods have been able to be dried successfully so far. However, this is an exception Meat. The main reason for the poor results is the protein nature of the cellular like the fibrous components of the muscles. It causes the tendency, above all, of the myosin molecules, to lose their colloidal dispersion and coagulate with the usual drying processes. As is the case with most other foods, the diffusion of the water does not succeed to influence the drying process in such a way that it evaporates on the surface without creating a hard, shrunk product that is difficult to re-moisten with water to lead. Rather, the protein molecules are denatured, with the drying product as well the destruction of enzymes suffers further chemical changes. It is therefore extremely important to find an economical process that converts meat into a storable dry form while maintaining its most important properties as a food.
An sich erscheint das Verfahren der Gefriertrocknung geeignet, die hinsichtlich Geschmacksqualität, Aromagehalt und vor allem an die Wiederdurchfeuchtbarkeit des getrockneten Fleiches zu stellenden Anforderungen zu erfüllen. Der entscheidende Nachteil dieses Verfahrens in seiner bisherigen Form ist die lange Dauer des Trocknungsprozesses, die das Verfahren so verteuert, daß es trotz seiner allgemein anerkannten Vorzüge praktisch schwer realisierbar ist. Dies wird in der Fachliteratur an verschiedenen Stellen ausführlich dargelegt. So z. B. in R. Gane: Freeze-drying of foodstuffs. Tn: Freezing and drying, report of a Symposion Held, June 1951.In itself, the process of freeze-drying appears suitable, which in terms of taste quality, Aroma content and, above all, the ability to rewet the dried meat To meet requirements. The main disadvantage of this method in its previous form is the long duration of the drying process, which makes the process so expensive that it is general in spite of it recognized advantages are difficult to achieve in practice. This is stated at various points in the specialist literature Set out in detail. So z. B. R. Gane: Freeze-drying of foodstuffs. Tn: Freezing and drying, report of a Symposion Held, June 1951.
Als allgemein anerkannte Lehre gilt demnach, daß bei der Gefriertrocknung von Lebensmitteln ein lagerfähiges Produkt nur entsteht, wenn die Trocknung bis zu einem Restfeuchtigkeitsgehalt von 1 °/o oder maximal 2% fortgeführt wird. Diese Regel ist durch zahlreiche Untersuchungen bestätigt worden. In USA ist durch Gesetz festgelegt, daß getrocknete Lebensmittel, also auch Fleisch, keine kleinere Restfeuchtigkeit als ι °/o aufweisen dürfen.As a generally accepted teaching is therefore that in the freeze-drying of food a storable Product only arises when drying to a residual moisture content of 1% or a maximum of 2% is continued. This rule has been confirmed by numerous studies. In USA is stipulated by law that dried food, including meat, has no minor residual moisture than ι ° / o may show.
Eigene Untersuchungen haben gezeigt, daß eine solche Vorschrift für die meisten Lebensmittel sinnvoll ist, während Fleisch eine Sonderstellung einnimmt. Versuche mit Thrombokinaseextrakten liefer-Gefriertrocknungsverfahren von FleischOur own studies have shown that such a rule makes sense for most foods is, while meat has a special position. Experiments with thrombokinase extracts delivery freeze-drying process of meat
Anmelder: Leybold-Hochvakuum-Anlagen Gesellschaft mit beschränkter Haftung,
Köln-Bayenthal, Bonner Str. 504Applicant: Leybold high vacuum systems limited liability company,
Cologne-Bayenthal, Bonner Str. 504
Dr. med. Karlheinz Neumann, Köln-Bayenthal
ist als Erfinder genannt wordenDr. med. Karlheinz Neumann, Cologne-Bayenthal
has been named as the inventor
ten beispielsweise das Ergebnis, daß bei einem Feuchtigkeitsgehalt zwischen 2 und 3°/o die Enzym-the result, for example, that with a moisture content between 2 and 3 ° / o the enzyme
ao Präparate schon nach wenigen Monaten unbrauchbar wurden und bei einer Restfeuchtigkeit von 8%> nach wenigen Wochen bereits unbrauchbar waren.ao preparations became unusable after just a few months and with a residual moisture content of 8%> were unusable after a few weeks.
Das neue Verfahren gemäß der Erfindung vermeidet die aufgezeigten Nachteile und liefert durch Gefrier-The new method according to the invention avoids the disadvantages indicated and provides by freezing
s5 trocknung ein haltbares und für die Ernährung geeignetes Trockenfleisch mit einem Restfeuchtigkeitsgehalt zwischen 6 und 15%. Hierzu wird das rohe oder gekochte Frischfleisch zunächst rasch eingefroren, wobei der kritische Temperaturbereich zwisehen + 2 und — 40C in kürzester Zeit (unter 15 Min.) durchfahren werden muß. Daran anschließend erfolgt unter Vakuumeinwirkung eine Absublimation des Eises aus dem gefrorenen Fleisch bis zu einer Restfeuchtigkeit des Trockengutes von 6 bis 15%. Es ist ferner möglich, das Fleisch ohne vorheriges Einfrieren der Vakuumeinwirkung auszusetzen. In diesem Fall führt die bei der Druckerniedrigung auftretende Verdunstungskälte zu der gewünschten raschen Unterkühlung des Fleisches.s5 drying a long-lasting dried meat suitable for nutrition with a residual moisture content between 6 and 15%. To this end, the raw or cooked fresh meat is first frozen rapidly, the critical temperature range zwisehen + 2, and - (. Less than 15 minutes) 4 0 C in a short time must be passed through. This is followed by a sublimation of the ice from the frozen meat under the action of a vacuum until the dry goods have a residual moisture content of 6 to 15%. It is also possible to expose the meat to the effect of vacuum without first freezing it. In this case, the evaporative cooling that occurs when the pressure is reduced leads to the desired rapid undercooling of the meat.
Es war sehr überraschend, daß entgegen den bisherigen Ansichten auch eine Restfeuchtigkeit von 6 bis 15% die Lagerfähigkeit und den Geschmack des gefriergetrockneten Fleisches nicht beeinträchtigt, so daß das Verfahren nach Erreichen dieser Restfeudhtigkeitswerte abgebrochen werden kann.It was very surprising that, contrary to previous views, a residual moisture of 6 up to 15% does not affect the shelf life and taste of the freeze-dried meat, so that the process can be terminated after these residual moisture levels have been reached.
Dadurch ergibt sich aber ein wesentlicher technischer Fortschritt, da gerade zur Erreichung der kleinen Restfeuchtigkeit von etwa 1 bis 2% lange zusätzliche Trocknungszeiten benötigt werden. Dies zeigt die graphische Darstellung in Fig. 1, wobei über der Trocknungszeit die Restfeuchtigkeit für eine bestimmte Fleischsorte (Hühnerfleisch) aufgetragen ist.However, this results in a significant technical advance, since it is precisely to achieve the small residual moisture of around 1 to 2%, long additional drying times are required. this shows the graph in FIG. 1, with the residual moisture for a certain types of meat (chicken) are served.
Das erfindungsgemäße Verfahren erlaubt daher eineThe inventive method therefore allows a
wesentlich bessere Ausnutzung der Gefriertfockmings-significantly better utilization of the freezing jib
Claims (5)
M. W. Tuchschneid, »Die Kältebehandlung schnell verderblicher Lebensmittel«, 189 bis 191, 1951.Considered publications:
MW Tuchschneid, "The Cold Treatment of Perishable Foods", 189 to 191, 1951.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEL23316A DE1000223B (en) | 1955-10-31 | 1955-10-31 | Freeze-drying process of meat |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEL23316A DE1000223B (en) | 1955-10-31 | 1955-10-31 | Freeze-drying process of meat |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1000223B true DE1000223B (en) | 1957-01-03 |
Family
ID=7262684
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEL23316A Pending DE1000223B (en) | 1955-10-31 | 1955-10-31 | Freeze-drying process of meat |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE1000223B (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1231535B (en) * | 1960-04-26 | 1966-12-29 | Truman Benjamin Wayne | Process for the production of dehydrated, gelatinized rice products |
| DE1243503B (en) * | 1959-10-16 | 1967-06-29 | Maggi Ag | Process for preventing foodstuffs from crumbling, which are in the form of cubes, slices or in another form, dried, in particular freeze-dried, and device for carrying out the process |
| EP0223887A1 (en) * | 1983-11-04 | 1987-06-03 | Bonanza Enterprises Ltd. | Method and equipment for producing dried food |
-
1955
- 1955-10-31 DE DEL23316A patent/DE1000223B/en active Pending
Non-Patent Citations (1)
| Title |
|---|
| None * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1243503B (en) * | 1959-10-16 | 1967-06-29 | Maggi Ag | Process for preventing foodstuffs from crumbling, which are in the form of cubes, slices or in another form, dried, in particular freeze-dried, and device for carrying out the process |
| DE1231535B (en) * | 1960-04-26 | 1966-12-29 | Truman Benjamin Wayne | Process for the production of dehydrated, gelatinized rice products |
| EP0223887A1 (en) * | 1983-11-04 | 1987-06-03 | Bonanza Enterprises Ltd. | Method and equipment for producing dried food |
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